THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory

The characterization of simplisia, phytochemical screening, extraction, isolation and identification of chemical constituens  from thallus Turbinaria decurrens Bory have been carried out. The examination of simplisia characteristics gave the water soluble extract the value of 10.59%, ethanol soluble...

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Main Author: Irma Sari
Format: Article
Language:English
Published: Universitas Syiah Kuala, Faculty of Mathematics and Natural Science 2015-09-01
Series:Jurnal Natural
Online Access:http://www.jurnal.unsyiah.ac.id/natural/article/view/5063
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author Irma Sari
author_facet Irma Sari
author_sort Irma Sari
collection DOAJ
description The characterization of simplisia, phytochemical screening, extraction, isolation and identification of chemical constituens  from thallus Turbinaria decurrens Bory have been carried out. The examination of simplisia characteristics gave the water soluble extract the value of 10.59%, ethanol soluble extract valued at 0.93%, total ash valued at 15.64%, the acid insoluble ash value 0.79% and the water content valued at 8.66%. The result of phytochemical screening showed that there was triterpens/steroids present. The extraction process was carried out by percolation and then was separated by liquid vacum column chromatography. Then by preparative thin layer chromatography isolate B1 was obtained. The analysis of isolate B1 by infra red spectrophotometry showed hydroxyl, aliphatic C-H bond, C=O bond, double bond of C=C, C=O bond, C=H bond of CH3 and CH2, were present. Ultra violet spectrophotometry exhibited a maximum absorption at 242 nm and mass spectrometric fragmentation pattern exhibited that the molecular weight of isolate B1 was 394, it was suspected ergosta -4,7,22 –trien -3 one.
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spelling doaj.art-56ad7060a9c84a23b74ce5f56cef802a2024-04-02T06:08:54ZengUniversitas Syiah Kuala, Faculty of Mathematics and Natural ScienceJurnal Natural1411-85132541-40622015-09-011524265THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens BoryIrma SariThe characterization of simplisia, phytochemical screening, extraction, isolation and identification of chemical constituens  from thallus Turbinaria decurrens Bory have been carried out. The examination of simplisia characteristics gave the water soluble extract the value of 10.59%, ethanol soluble extract valued at 0.93%, total ash valued at 15.64%, the acid insoluble ash value 0.79% and the water content valued at 8.66%. The result of phytochemical screening showed that there was triterpens/steroids present. The extraction process was carried out by percolation and then was separated by liquid vacum column chromatography. Then by preparative thin layer chromatography isolate B1 was obtained. The analysis of isolate B1 by infra red spectrophotometry showed hydroxyl, aliphatic C-H bond, C=O bond, double bond of C=C, C=O bond, C=H bond of CH3 and CH2, were present. Ultra violet spectrophotometry exhibited a maximum absorption at 242 nm and mass spectrometric fragmentation pattern exhibited that the molecular weight of isolate B1 was 394, it was suspected ergosta -4,7,22 –trien -3 one.http://www.jurnal.unsyiah.ac.id/natural/article/view/5063
spellingShingle Irma Sari
THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
Jurnal Natural
title THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
title_full THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
title_fullStr THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
title_full_unstemmed THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
title_short THE CHARACTERIZATION OF SIMPLISIA, ISOLATION AND IDENTIFICATION OF CHEMICAL CONSTITUENS FROM THALLUS Turbinaria decurrens Bory
title_sort characterization of simplisia isolation and identification of chemical constituens from thallus turbinaria decurrens bory
url http://www.jurnal.unsyiah.ac.id/natural/article/view/5063
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