One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour

We present one-pot colloidal synthesis of copper indium telluride (CITe) from respective metal salts with sodium tellurite in 1-octadecene with variation in surfactant and the reaction temperature between 200 and 300 °C. Oleic acid and/or oleyl amine are employed to initially, generate tellurides of...

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Main Authors: Naeem Mohammad, Pawan K. Khanna
Format: Article
Language:English
Published: Elsevier 2024-04-01
Series:Hybrid Advances
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2773207X24000307
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author Naeem Mohammad
Pawan K. Khanna
author_facet Naeem Mohammad
Pawan K. Khanna
author_sort Naeem Mohammad
collection DOAJ
description We present one-pot colloidal synthesis of copper indium telluride (CITe) from respective metal salts with sodium tellurite in 1-octadecene with variation in surfactant and the reaction temperature between 200 and 300 °C. Oleic acid and/or oleyl amine are employed to initially, generate tellurides of individual element at intermediate stage. The tuning of reaction parameter including temperature variations play important role for the formation of phase-pure CuInTe2 nanocrystals with a band-gap of about 1.15 eV. The phase-purity was confirmed by XRD. EMI Shielding efficiency of CITe/PVA film can be enhanced to the tune of −8.84 dB by use of silver nano-particles. The composite can be suitable for X-band applications.
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spelling doaj.art-56e4a42436884e5ca412ff77f6a504d22024-04-16T04:10:09ZengElsevierHybrid Advances2773-207X2024-04-015100169One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviourNaeem Mohammad0Pawan K. Khanna1Quantum Dots/Nanomaterials Laboratory, Department of Applied Chemistry, Defence Institute of Advanced Technology (DIAT), Pune, 411025, IndiaCorresponding author.; Quantum Dots/Nanomaterials Laboratory, Department of Applied Chemistry, Defence Institute of Advanced Technology (DIAT), Pune, 411025, IndiaWe present one-pot colloidal synthesis of copper indium telluride (CITe) from respective metal salts with sodium tellurite in 1-octadecene with variation in surfactant and the reaction temperature between 200 and 300 °C. Oleic acid and/or oleyl amine are employed to initially, generate tellurides of individual element at intermediate stage. The tuning of reaction parameter including temperature variations play important role for the formation of phase-pure CuInTe2 nanocrystals with a band-gap of about 1.15 eV. The phase-purity was confirmed by XRD. EMI Shielding efficiency of CITe/PVA film can be enhanced to the tune of −8.84 dB by use of silver nano-particles. The composite can be suitable for X-band applications.http://www.sciencedirect.com/science/article/pii/S2773207X24000307SynthesisNanoparticlesElectronic materialTernary metal tellurideEMI shielding
spellingShingle Naeem Mohammad
Pawan K. Khanna
One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
Hybrid Advances
Synthesis
Nanoparticles
Electronic material
Ternary metal telluride
EMI shielding
title One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
title_full One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
title_fullStr One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
title_full_unstemmed One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
title_short One-pot solvothermal synthesis of copper indium telluride (CuInTe2) and its X-band EMI shielding behaviour
title_sort one pot solvothermal synthesis of copper indium telluride cuinte2 and its x band emi shielding behaviour
topic Synthesis
Nanoparticles
Electronic material
Ternary metal telluride
EMI shielding
url http://www.sciencedirect.com/science/article/pii/S2773207X24000307
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