Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process
In the present study, Inconel 718 (IN718) superalloy fabricated by laser powder bed fusion (LPBF) has been characterized focusing on the effect of both homogenization and solution treatment time on grains structure, crystallographic texture, precipitates formation/dissolution and material hardness....
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MDPI AG
2020-06-01
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| author | Eslam M. Fayed Davood Shahriari Mohammad Saadati Vladimir Brailovski Mohammad Jahazi Mamoun Medraj |
| author_facet | Eslam M. Fayed Davood Shahriari Mohammad Saadati Vladimir Brailovski Mohammad Jahazi Mamoun Medraj |
| author_sort | Eslam M. Fayed |
| collection | DOAJ |
| description | In the present study, Inconel 718 (IN718) superalloy fabricated by laser powder bed fusion (LPBF) has been characterized focusing on the effect of both homogenization and solution treatment time on grains structure, crystallographic texture, precipitates formation/dissolution and material hardness. For this purpose, a heat-treatment time window with a wide range of soaking times for both treatments was established aiming to develop the optimal post-treatment conditions for laser powder bed fused IN718. It was found that the as-printed IN718 is characterized by very fine columnar/cellular dendrites with Laves phase precipitating at the grain boundaries as well as inter-dendritic regions, which differs from the microstructure of wrought and cast materials and requires special heat-treatment conditions different from the standard treatments. The results reveal that the relatively short homogenization treatment at 1080 °C for 1 h was not enough to significantly change the as-printed grain structure and completely dissolve the segregates and Laves phase. However, a completely recrystallized IN718 material and more Laves phase dissolution were obtained after homogenization treatment for 4 h. A further increase in time of the homogenization treatment (7 h) resulted in grain growth and coarsening of carbides precipitates. The solution treatment time at 980 °C did not cause noticeable changes in the crystallographic texture and grain structure. Nevertheless, the amount of δ-phase precipitation was significantly affected by the solution treatment time. After applying the heat-treatment time window, the hardness increased by 51–72% of the as-printed condition depending on the treatment time due to the formation of γ′ and γ″ in the γ-matrix. The highest material hardness was obtained after 1 h homogenization, whereas the prolonged time treatments reduced the hardness. This study provides a comprehensive investigation of the post heat-treatments of the laser powder bed fused IN718 that can result in an optimized microstructure and mechanical behavior for particular applications. |
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| spelling | doaj.art-57a1d2393e974d0a8c9a62edcf7624652023-11-20T02:55:27ZengMDPI AGMaterials1996-19442020-06-011311257410.3390/ma13112574Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion ProcessEslam M. Fayed0Davood Shahriari1Mohammad Saadati2Vladimir Brailovski3Mohammad Jahazi4Mamoun Medraj5Department of Mechanical, Industrial and Aerospace Engineering, Concordia University, 15151 Rue Sainte Catherine West, Montreal, QC H3G 2W1, CanadaDepartment of Mechanical Engineering, École de Technologie Supérieure, 1100, Notre-Dame Street West, Montreal, QC H3C 1K3, CanadaDepartment of Mechanical Engineering, École de Technologie Supérieure, 1100, Notre-Dame Street West, Montreal, QC H3C 1K3, CanadaDepartment of Mechanical Engineering, École de Technologie Supérieure, 1100, Notre-Dame Street West, Montreal, QC H3C 1K3, CanadaDepartment of Mechanical Engineering, École de Technologie Supérieure, 1100, Notre-Dame Street West, Montreal, QC H3C 1K3, CanadaDepartment of Mechanical, Industrial and Aerospace Engineering, Concordia University, 15151 Rue Sainte Catherine West, Montreal, QC H3G 2W1, CanadaIn the present study, Inconel 718 (IN718) superalloy fabricated by laser powder bed fusion (LPBF) has been characterized focusing on the effect of both homogenization and solution treatment time on grains structure, crystallographic texture, precipitates formation/dissolution and material hardness. For this purpose, a heat-treatment time window with a wide range of soaking times for both treatments was established aiming to develop the optimal post-treatment conditions for laser powder bed fused IN718. It was found that the as-printed IN718 is characterized by very fine columnar/cellular dendrites with Laves phase precipitating at the grain boundaries as well as inter-dendritic regions, which differs from the microstructure of wrought and cast materials and requires special heat-treatment conditions different from the standard treatments. The results reveal that the relatively short homogenization treatment at 1080 °C for 1 h was not enough to significantly change the as-printed grain structure and completely dissolve the segregates and Laves phase. However, a completely recrystallized IN718 material and more Laves phase dissolution were obtained after homogenization treatment for 4 h. A further increase in time of the homogenization treatment (7 h) resulted in grain growth and coarsening of carbides precipitates. The solution treatment time at 980 °C did not cause noticeable changes in the crystallographic texture and grain structure. Nevertheless, the amount of δ-phase precipitation was significantly affected by the solution treatment time. After applying the heat-treatment time window, the hardness increased by 51–72% of the as-printed condition depending on the treatment time due to the formation of γ′ and γ″ in the γ-matrix. The highest material hardness was obtained after 1 h homogenization, whereas the prolonged time treatments reduced the hardness. This study provides a comprehensive investigation of the post heat-treatments of the laser powder bed fused IN718 that can result in an optimized microstructure and mechanical behavior for particular applications.https://www.mdpi.com/1996-1944/13/11/2574additive manufacturinglaser powder bed fusionmetal 3D printingnickel-based superalloyIN718microstructure |
| spellingShingle | Eslam M. Fayed Davood Shahriari Mohammad Saadati Vladimir Brailovski Mohammad Jahazi Mamoun Medraj Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process Materials additive manufacturing laser powder bed fusion metal 3D printing nickel-based superalloy IN718 microstructure |
| title | Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process |
| title_full | Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process |
| title_fullStr | Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process |
| title_full_unstemmed | Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process |
| title_short | Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process |
| title_sort | influence of homogenization and solution treatments time on the microstructure and hardness of inconel 718 fabricated by laser powder bed fusion process |
| topic | additive manufacturing laser powder bed fusion metal 3D printing nickel-based superalloy IN718 microstructure |
| url | https://www.mdpi.com/1996-1944/13/11/2574 |
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