Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life
In this study, the extraction process of fennel essential oil was optimized by response surface methodology. Fennel essential oil was used as oil phase, Tween 80+40 as surfactant and glycerol as cosurfactant to prepare fennel essential oil microemulsion system. The structure, particle size, total re...
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| Format: | Article |
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The editorial department of Science and Technology of Food Industry
2022-09-01
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| Series: | Shipin gongye ke-ji |
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| Online Access: | http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021110199 |
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| author | Bing HAN Tianqi ZHANG Ye ZHENG Xue HAN Xiaohan JIANG Chunran HAN Gensheng ZHANG Shiyou YU |
| author_facet | Bing HAN Tianqi ZHANG Ye ZHENG Xue HAN Xiaohan JIANG Chunran HAN Gensheng ZHANG Shiyou YU |
| author_sort | Bing HAN |
| collection | DOAJ |
| description | In this study, the extraction process of fennel essential oil was optimized by response surface methodology. Fennel essential oil was used as oil phase, Tween 80+40 as surfactant and glycerol as cosurfactant to prepare fennel essential oil microemulsion system. The structure, particle size, total reducing power and storage property of fennel essential oil microemulsion were investigated by rheology, particle size analyzer and reduction reaction. The results showed that the yield of essential oil of fennel was as high as 15.99%±0.10% when the ratio of material to liquid was 1:8.40 g/mL, the extraction time was 4.09 h, the particle size was 80 mesh, and the extraction temperature 80 ℃. The diameter of fennel essential oil microemulsion was 30.92±0.13 nm, and when the moisture content was higher than 60%, it was a stable O/W microemulsion. The emulsification of fennel essential oil significantly improved the total reducing power of fennel essential oil. According to the principle of chemical reaction kinetics, the Arrhenius equation was established as k=2518.85·e−35583.09/RT. The model predicted that the fennel essential oil microemulsion could store 1899.18, 932.03, 492.94 and 271.51 h at 20, 35, 50 and 65 ℃, the maximum relative error was 8.73%, and the error was small, which could accurately predict the shelf life of the microemulsion. |
| first_indexed | 2024-04-11T06:52:22Z |
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| id | doaj.art-57beca50a51045009656715a278b708b |
| institution | Directory Open Access Journal |
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| language | zho |
| last_indexed | 2024-04-11T06:52:22Z |
| publishDate | 2022-09-01 |
| publisher | The editorial department of Science and Technology of Food Industry |
| record_format | Article |
| series | Shipin gongye ke-ji |
| spelling | doaj.art-57beca50a51045009656715a278b708b2022-12-22T04:39:08ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062022-09-01431720321110.13386/j.issn1002-0306.20211101992021110199-17Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf LifeBing HAN0Tianqi ZHANG1Ye ZHENG2Xue HAN3Xiaohan JIANG4Chunran HAN5Gensheng ZHANG6Shiyou YU7College of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaCollege of Food Engineering, Harbin University of Commerce, Harbin 150028, ChinaIn this study, the extraction process of fennel essential oil was optimized by response surface methodology. Fennel essential oil was used as oil phase, Tween 80+40 as surfactant and glycerol as cosurfactant to prepare fennel essential oil microemulsion system. The structure, particle size, total reducing power and storage property of fennel essential oil microemulsion were investigated by rheology, particle size analyzer and reduction reaction. The results showed that the yield of essential oil of fennel was as high as 15.99%±0.10% when the ratio of material to liquid was 1:8.40 g/mL, the extraction time was 4.09 h, the particle size was 80 mesh, and the extraction temperature 80 ℃. The diameter of fennel essential oil microemulsion was 30.92±0.13 nm, and when the moisture content was higher than 60%, it was a stable O/W microemulsion. The emulsification of fennel essential oil significantly improved the total reducing power of fennel essential oil. According to the principle of chemical reaction kinetics, the Arrhenius equation was established as k=2518.85·e−35583.09/RT. The model predicted that the fennel essential oil microemulsion could store 1899.18, 932.03, 492.94 and 271.51 h at 20, 35, 50 and 65 ℃, the maximum relative error was 8.73%, and the error was small, which could accurately predict the shelf life of the microemulsion.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021110199fennel essential oilresponse surface optimizationmicroemulsion propertiesmodelshelf life |
| spellingShingle | Bing HAN Tianqi ZHANG Ye ZHENG Xue HAN Xiaohan JIANG Chunran HAN Gensheng ZHANG Shiyou YU Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life Shipin gongye ke-ji fennel essential oil response surface optimization microemulsion properties model shelf life |
| title | Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life |
| title_full | Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life |
| title_fullStr | Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life |
| title_full_unstemmed | Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life |
| title_short | Optimization of Extraction Process of Fennel Essential Oil by Response Surface Methodology and Its Microemulsion Characteristics and Shelf Life |
| title_sort | optimization of extraction process of fennel essential oil by response surface methodology and its microemulsion characteristics and shelf life |
| topic | fennel essential oil response surface optimization microemulsion properties model shelf life |
| url | http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2021110199 |
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