Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM
In this work, polycrystalline samples of hard-magnetic materials of (Nd1– xPrx)2Fe14B general formula have been prepared and subjected to severe plastic deformation (SPD). Thereafter the features of nanostructure formation in the compounds were investigated before and after SPD using atomic force mi...
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Format: | Article |
Language: | English |
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Peter the Great St.Petersburg Polytechnic University
2022-06-01
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Series: | St. Petersburg Polytechnical University Journal: Physics and Mathematics |
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Online Access: | https://physmath.spbstu.ru/article/2022.56.04/ |
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author | Tereshina Irina Politova Galina Kaminskaya Tatiana Popov Vladimir Gunderov Dmitry Filimonov Alexey Pelevin Ivan |
author_facet | Tereshina Irina Politova Galina Kaminskaya Tatiana Popov Vladimir Gunderov Dmitry Filimonov Alexey Pelevin Ivan |
author_sort | Tereshina Irina |
collection | DOAJ |
description | In this work, polycrystalline samples of hard-magnetic materials of (Nd1– xPrx)2Fe14B general formula have been prepared and subjected to severe plastic deformation (SPD). Thereafter the features of nanostructure formation in the compounds were investigated before and after SPD using atomic force microscopy and magnetic force one (AFM & MFM). The differences in texture formation were revealed when studying the surface microstructure of both the initial and deformed samples. The initial ones prepared by the Czochralski method, exhibited the columnar structure, while the SPD samples exhibited the concentric rings containing elongated nanosized crystallites. The magnetic domain structure was visualized using the MFM that clearly demonstrated the relationship between the microstructural features and the magnetic domains’ configuration. |
first_indexed | 2024-04-13T22:38:52Z |
format | Article |
id | doaj.art-58eba260610a4ebe8aef6018662d4c97 |
institution | Directory Open Access Journal |
issn | 2405-7223 |
language | English |
last_indexed | 2024-04-13T22:38:52Z |
publishDate | 2022-06-01 |
publisher | Peter the Great St.Petersburg Polytechnic University |
record_format | Article |
series | St. Petersburg Polytechnical University Journal: Physics and Mathematics |
spelling | doaj.art-58eba260610a4ebe8aef6018662d4c972022-12-22T02:26:40ZengPeter the Great St.Petersburg Polytechnic UniversitySt. Petersburg Polytechnical University Journal: Physics and Mathematics2405-72232022-06-0115210.18721/JPM.1520420714726Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFMTereshina Irina0https://orcid.org/0000-0003-3633-3440Politova Galina1https://orcid.org/0000-0003-1908-9677Kaminskaya Tatiana2https://orcid.org/0000-0002-3667-0837Popov Vladimir3https://orcid.org/0000-0003-1191-3860Gunderov Dmitry4https://orcid.org/0000-0001-5925-4513Filimonov Alexey5https://orcid.org/0000-0002-2793-5717Pelevin Ivan6https://orcid.org/0000-0003-1592-3062Lomonosov Moscow State UniversityBaikov Institute of Metallurgy Materials Science Imet RASLomonosov Moscow State UniversityLomonosov Moscow State UniversityInstitute of Molecule and Crystal Physics - Subdivision of the Ufa Federal Research Centre of the Russian Academy of SciencesPeter the Great St. Petersburg Polytechnic UniversityNational University of Science and Technology "MISIS" (MISIS)In this work, polycrystalline samples of hard-magnetic materials of (Nd1– xPrx)2Fe14B general formula have been prepared and subjected to severe plastic deformation (SPD). Thereafter the features of nanostructure formation in the compounds were investigated before and after SPD using atomic force microscopy and magnetic force one (AFM & MFM). The differences in texture formation were revealed when studying the surface microstructure of both the initial and deformed samples. The initial ones prepared by the Czochralski method, exhibited the columnar structure, while the SPD samples exhibited the concentric rings containing elongated nanosized crystallites. The magnetic domain structure was visualized using the MFM that clearly demonstrated the relationship between the microstructural features and the magnetic domains’ configuration.https://physmath.spbstu.ru/article/2022.56.04/atomic force microscopymagnetic force microscopyhard-magnetic materialnanostructure |
spellingShingle | Tereshina Irina Politova Galina Kaminskaya Tatiana Popov Vladimir Gunderov Dmitry Filimonov Alexey Pelevin Ivan Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM St. Petersburg Polytechnical University Journal: Physics and Mathematics atomic force microscopy magnetic force microscopy hard-magnetic material nanostructure |
title | Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM |
title_full | Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM |
title_fullStr | Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM |
title_full_unstemmed | Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM |
title_short | Features of the nanostructure formation in the Nd-Pr-Fe-B-system alloys: a study by AFM and MFM |
title_sort | features of the nanostructure formation in the nd pr fe b system alloys a study by afm and mfm |
topic | atomic force microscopy magnetic force microscopy hard-magnetic material nanostructure |
url | https://physmath.spbstu.ru/article/2022.56.04/ |
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