Syntheses and Study of a Pyrroline Nitroxide Condensed Phospholene Oxide and a Pyrroline Nitroxide Attached Diphenylphosphine

Syntheses and Study of a Pyrroline Nitroxide Condensed Phospholene Oxide and a Pyrroline Nitroxide Attached Diphenylphosphine

The reaction of a diene nitroxide precursor with dichlorophenylphosphine in a McCormac procedure afforded 1,1,3,3-tetramethyl-5-phenyl-1,2,3,4,5,6-hexahydrophospholo[3,4-c]pyrrole-5-oxide-2-oxyl. Lithiation of the protected 3-iodo-pyrroline nitroxide followed by treatment with chlorodiphenylphosphin...

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Bibliographic Details
Main Authors: Mostafa Isbera, Balázs Bognár, Ferenc Gallyas, Attila Bényei, József Jekő, Tamás Kálai
Format: Article
Language:English
Published: MDPI AG 2021-07-01
Series:Molecules
Subjects:
lithiation
McCormac reaction
nitroxides
protecting groups
reduction
Online Access:https://www.mdpi.com/1420-3049/26/14/4366

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