New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo
From the roots of Deguelia hatschbachii, the known flavonoids scandenin (1), methyl robustate (2) and 4',5- dihydroxy-6-(3,3-dimethylalyll)-7-methoxy flavanone (3) were isolated and characterized by comparison of their spectroscopic data with those found in the literature. Now the inclusion of...
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| Format: | Article |
| Language: | English |
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Sociedade Brasileira de Química
2003-01-01
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| Series: | Journal of the Brazilian Chemical Society |
| Subjects: | |
| Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000100022 |
| _version_ | 1818156119696080896 |
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| author | Magalhães Aderbal F. Tozzi Ana M. G. A. Magalhães Eva G. Moraes Valéria R. de S. |
| author_facet | Magalhães Aderbal F. Tozzi Ana M. G. A. Magalhães Eva G. Moraes Valéria R. de S. |
| author_sort | Magalhães Aderbal F. |
| collection | DOAJ |
| description | From the roots of Deguelia hatschbachii, the known flavonoids scandenin (1), methyl robustate (2) and 4',5- dihydroxy-6-(3,3-dimethylalyll)-7-methoxy flavanone (3) were isolated and characterized by comparison of their spectroscopic data with those found in the literature. Now the inclusion of 1D- and 2D-NMR and MS/MS data has allowed the complete assignment of all hydrogen and carbon chemical shifts in their NMR spectra, as well as the elucidation of the fragmentation pathways of 1-3 in the mass spectrometer. |
| first_indexed | 2024-12-11T14:53:14Z |
| format | Article |
| id | doaj.art-596ee9b572bd49c18088ca2be751f5fb |
| institution | Directory Open Access Journal |
| issn | 0103-5053 |
| language | English |
| last_indexed | 2024-12-11T14:53:14Z |
| publishDate | 2003-01-01 |
| publisher | Sociedade Brasileira de Química |
| record_format | Article |
| series | Journal of the Brazilian Chemical Society |
| spelling | doaj.art-596ee9b572bd49c18088ca2be751f5fb2022-12-22T01:01:22ZengSociedade Brasileira de QuímicaJournal of the Brazilian Chemical Society0103-50532003-01-01141133137New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. AzevedoMagalhães Aderbal F.Tozzi Ana M. G. A.Magalhães Eva G.Moraes Valéria R. de S.From the roots of Deguelia hatschbachii, the known flavonoids scandenin (1), methyl robustate (2) and 4',5- dihydroxy-6-(3,3-dimethylalyll)-7-methoxy flavanone (3) were isolated and characterized by comparison of their spectroscopic data with those found in the literature. Now the inclusion of 1D- and 2D-NMR and MS/MS data has allowed the complete assignment of all hydrogen and carbon chemical shifts in their NMR spectra, as well as the elucidation of the fragmentation pathways of 1-3 in the mass spectrometer.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000100022Deguelia hatschbachiiLeguminosae4-hydroxy-3-phenylcoumarinsflavanone |
| spellingShingle | Magalhães Aderbal F. Tozzi Ana M. G. A. Magalhães Eva G. Moraes Valéria R. de S. New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo Journal of the Brazilian Chemical Society Deguelia hatschbachii Leguminosae 4-hydroxy-3-phenylcoumarins flavanone |
| title | New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo |
| title_full | New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo |
| title_fullStr | New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo |
| title_full_unstemmed | New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo |
| title_short | New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo |
| title_sort | new spectral data of some flavonoids from deguelia hatschbachii a m g azevedo |
| topic | Deguelia hatschbachii Leguminosae 4-hydroxy-3-phenylcoumarins flavanone |
| url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532003000100022 |
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