Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork

To avoid fraudulent practices, LC-Orbitrap and FT-NIRS combined with multivariate analysis was used to distinguish between 53 Korean and foreign Boston butt samples; forty were used to establish the calibration model and 13 were used as an external validation set. Twenty metabolites were determined...

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Main Authors: Lee Ji Hye, An Jae Min, Kang Dong Jin, Kim Ho Jin, Lee Seong Hun
Format: Article
Language:English
Published: Taylor & Francis Group 2022-12-01
Series:International Journal of Food Properties
Subjects:
Online Access:http://dx.doi.org/10.1080/10942912.2022.2027962
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author Lee Ji Hye
An Jae Min
Kang Dong Jin
Kim Ho Jin
Lee Seong Hun
author_facet Lee Ji Hye
An Jae Min
Kang Dong Jin
Kim Ho Jin
Lee Seong Hun
author_sort Lee Ji Hye
collection DOAJ
description To avoid fraudulent practices, LC-Orbitrap and FT-NIRS combined with multivariate analysis was used to distinguish between 53 Korean and foreign Boston butt samples; forty were used to establish the calibration model and 13 were used as an external validation set. Twenty metabolites were determined to be good indicators of geographic origin. Both LC-Orbitrap with CDA model based on 20 metabolites and FT-NIRS with PLS achieved 100% efficiency in identifying Korean and foreign samples; overall predictive rates for LC-Orbitrap (94.9%) and FT-NIRS (100%). Thus, combined use of LC-Orbitrap and FT-NIRS could be proposed to determine reliably discriminate geographic origins of pork samples.
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spelling doaj.art-59a4f2e5dbfb4362b7afe4c07a54e7852022-12-22T04:10:09ZengTaylor & Francis GroupInternational Journal of Food Properties1094-29121532-23862022-12-0125112814310.1080/10942912.2022.20279622027962Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt porkLee Ji Hye0An Jae Min1Kang Dong Jin2Kim Ho Jin3Lee Seong Hun4Experiment Research Institute, National Agricultural Products Quality Management ServiceExperiment Research Institute, National Agricultural Products Quality Management ServiceExperiment Research Institute, National Agricultural Products Quality Management ServiceExperiment Research Institute, National Agricultural Products Quality Management ServiceExperiment Research Institute, National Agricultural Products Quality Management ServiceTo avoid fraudulent practices, LC-Orbitrap and FT-NIRS combined with multivariate analysis was used to distinguish between 53 Korean and foreign Boston butt samples; forty were used to establish the calibration model and 13 were used as an external validation set. Twenty metabolites were determined to be good indicators of geographic origin. Both LC-Orbitrap with CDA model based on 20 metabolites and FT-NIRS with PLS achieved 100% efficiency in identifying Korean and foreign samples; overall predictive rates for LC-Orbitrap (94.9%) and FT-NIRS (100%). Thus, combined use of LC-Orbitrap and FT-NIRS could be proposed to determine reliably discriminate geographic origins of pork samples.http://dx.doi.org/10.1080/10942912.2022.2027962porkboston buttlc-orbitrapft-nirsgeographical originmultivariate analysis
spellingShingle Lee Ji Hye
An Jae Min
Kang Dong Jin
Kim Ho Jin
Lee Seong Hun
Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
International Journal of Food Properties
pork
boston butt
lc-orbitrap
ft-nirs
geographical origin
multivariate analysis
title Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
title_full Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
title_fullStr Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
title_full_unstemmed Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
title_short Use of LC-Orbitrap MS and FT-NIRS with multivariate analysis to determine geographic origin of Boston butt pork
title_sort use of lc orbitrap ms and ft nirs with multivariate analysis to determine geographic origin of boston butt pork
topic pork
boston butt
lc-orbitrap
ft-nirs
geographical origin
multivariate analysis
url http://dx.doi.org/10.1080/10942912.2022.2027962
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