In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging

Electron Beam Powder Bed Fusion (PBF-EB) is an Additive Manufacturing (AM) method that utilizes an electron beam to melt and consolidate metal powder. The beam, combined with a backscattered electron detector, enables advanced process monitoring, a method termed Electron Optical Imaging (ELO). ELO i...

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Main Authors: Martin Gardfjell, Marcel Reith, Martin Franke, Carolin Körner
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/12/4220
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author Martin Gardfjell
Marcel Reith
Martin Franke
Carolin Körner
author_facet Martin Gardfjell
Marcel Reith
Martin Franke
Carolin Körner
author_sort Martin Gardfjell
collection DOAJ
description Electron Beam Powder Bed Fusion (PBF-EB) is an Additive Manufacturing (AM) method that utilizes an electron beam to melt and consolidate metal powder. The beam, combined with a backscattered electron detector, enables advanced process monitoring, a method termed Electron Optical Imaging (ELO). ELO is already known to provide great topographical information, but its capabilities regarding material contrast are less studied. In this article the extents of material contrast using ELO are investigated, focusing mainly on identifying powder contamination. It will be shown that an ELO detector is capable of distinguishing a single 100 μ<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mi mathvariant="normal">m</mi></semantics></math></inline-formula> foreign powder particle, during an PBF-EB process, if the backscattering coefficient of the inclusion is sufficiently higher than its surroundings. Additionally, it is investigated how the material contrast can be used for material characterization. A mathematical framework is provided to describe the relationship between the signal intensity in the detector and the effective atomic number <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><msup><mi mathvariant="normal">Z</mi><mi>eff</mi></msup></semantics></math></inline-formula> of the imaged alloy. The approach is verified with empirical data from twelve different materials, demonstrating that the effective atomic number of an alloy can be predicted to within one atomic number from its ELO intensity.
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spelling doaj.art-59b3df2fa36f43a5bd74870b1da3cd9f2023-11-18T11:23:10ZengMDPI AGMaterials1996-19442023-06-011612422010.3390/ma16124220In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical ImagingMartin Gardfjell0Marcel Reith1Martin Franke2Carolin Körner3Neue Materialien Fürth GmbH, 90762 Fürth, GermanyNeue Materialien Fürth GmbH, 90762 Fürth, GermanyNeue Materialien Fürth GmbH, 90762 Fürth, GermanyMaterials Science and Engineering for Metals (WTM), Martensstr. 5., 91058 Erlangen, GermanyElectron Beam Powder Bed Fusion (PBF-EB) is an Additive Manufacturing (AM) method that utilizes an electron beam to melt and consolidate metal powder. The beam, combined with a backscattered electron detector, enables advanced process monitoring, a method termed Electron Optical Imaging (ELO). ELO is already known to provide great topographical information, but its capabilities regarding material contrast are less studied. In this article the extents of material contrast using ELO are investigated, focusing mainly on identifying powder contamination. It will be shown that an ELO detector is capable of distinguishing a single 100 μ<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mi mathvariant="normal">m</mi></semantics></math></inline-formula> foreign powder particle, during an PBF-EB process, if the backscattering coefficient of the inclusion is sufficiently higher than its surroundings. Additionally, it is investigated how the material contrast can be used for material characterization. A mathematical framework is provided to describe the relationship between the signal intensity in the detector and the effective atomic number <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><msup><mi mathvariant="normal">Z</mi><mi>eff</mi></msup></semantics></math></inline-formula> of the imaged alloy. The approach is verified with empirical data from twelve different materials, demonstrating that the effective atomic number of an alloy can be predicted to within one atomic number from its ELO intensity.https://www.mdpi.com/1996-1944/16/12/4220Additive ManufacturingElectron Beam Powder Bed FusionProcess MonitoringBackscattered Electron DetectionElectron Optical ImagingPowder Contamination
spellingShingle Martin Gardfjell
Marcel Reith
Martin Franke
Carolin Körner
In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
Materials
Additive Manufacturing
Electron Beam Powder Bed Fusion
Process Monitoring
Backscattered Electron Detection
Electron Optical Imaging
Powder Contamination
title In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
title_full In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
title_fullStr In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
title_full_unstemmed In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
title_short In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using Electron Optical Imaging
title_sort in situ inclusion detection and material characterization in an electron beam powder bed fusion process using electron optical imaging
topic Additive Manufacturing
Electron Beam Powder Bed Fusion
Process Monitoring
Backscattered Electron Detection
Electron Optical Imaging
Powder Contamination
url https://www.mdpi.com/1996-1944/16/12/4220
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