1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione
In the title compound, C13H15ClN2S, the dihydropyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydropyrimidine and benzene rings...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2011-02-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810054292 |
| _version_ | 1819280228511383552 |
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| author | Bohari M. Yamin Halima Farag Salem |
| author_facet | Bohari M. Yamin Halima Farag Salem |
| author_sort | Bohari M. Yamin |
| collection | DOAJ |
| description | In the title compound, C13H15ClN2S, the dihydropyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydropyrimidine and benzene rings is 86.62 (13)°. The crystal structure is stabilized by intermolecular N—H...S hydrogen bonds, which form centrosymmetric dimers arranged along the c axis. |
| first_indexed | 2024-12-24T00:40:28Z |
| format | Article |
| id | doaj.art-5a53d77a78ab4d7197713b24219a5c30 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-24T00:40:28Z |
| publishDate | 2011-02-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-5a53d77a78ab4d7197713b24219a5c302022-12-21T17:23:58ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-02-01672o282o28210.1107/S16005368100542921-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thioneBohari M. YaminHalima Farag SalemIn the title compound, C13H15ClN2S, the dihydropyrimidine ring is essentially planar, with a maximum deviation from the least-squares plane of 0.122 (3) Å for the unsubstitued olefinic C atom. The dihedral angle between the dihydropyrimidine and benzene rings is 86.62 (13)°. The crystal structure is stabilized by intermolecular N—H...S hydrogen bonds, which form centrosymmetric dimers arranged along the c axis.http://scripts.iucr.org/cgi-bin/paper?S1600536810054292 |
| spellingShingle | Bohari M. Yamin Halima Farag Salem 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione Acta Crystallographica Section E |
| title | 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione |
| title_full | 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione |
| title_fullStr | 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione |
| title_full_unstemmed | 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione |
| title_short | 1-(3-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione |
| title_sort | 1 3 chlorophenyl 4 4 6 trimethyl 3 4 dihydropyrimidine 2 1h thione |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810054292 |
| work_keys_str_mv | AT boharimyamin 13chlorophenyl446trimethyl34dihydropyrimidine21hthione AT halimafaragsalem 13chlorophenyl446trimethyl34dihydropyrimidine21hthione |