Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material

Thermochemical adsorption energy storage is a potential energy utilization technology. Among these technologies, the composite energy storage material prepared by K<sub>2</sub>CO<sub>3</sub> and expanded vermiculite (EVM) shows excellent performance. In this paper, the influe...

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Main Authors: Dequan Zou, Xiangji Yue, Tianyi He, Jianan Ding, Dechun Ba
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/10/3702
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author Dequan Zou
Xiangji Yue
Tianyi He
Jianan Ding
Dechun Ba
author_facet Dequan Zou
Xiangji Yue
Tianyi He
Jianan Ding
Dechun Ba
author_sort Dequan Zou
collection DOAJ
description Thermochemical adsorption energy storage is a potential energy utilization technology. Among these technologies, the composite energy storage material prepared by K<sub>2</sub>CO<sub>3</sub> and expanded vermiculite (EVM) shows excellent performance. In this paper, the influence of the preparation process using the impregnation method and vacuum impregnation method on K<sub>2</sub>CO<sub>3</sub>/EVM composite material is studied. The preparation plan is further optimized with the solution concentration and the expanded vermiculite particle size as variables. In the experiment, mercury intrusion porosimetry (MIP) is used to measure the porosity and other parameters. Additionally, with the help of scanning electron microscopy (SEM), the morphological characteristics of the materials are obtained from a microscopic point of view. The effects of different preparation parameters are evaluated by comparing the experimental results. The results show that the K<sub>2</sub>CO<sub>3</sub> specific gravity of the composite material increases with the increase of the vacuum degree, up to 70.440 wt.% (the vacuum degree is 6.7 kPa). Expanded vermiculite with a large particle size (3~6 mm) can carry more K<sub>2</sub>CO<sub>3</sub>, and content per cubic centimeter of K<sub>2</sub>CO<sub>3</sub> can be as high as 0.466 g.
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spelling doaj.art-5bd7b57e868a470fb817354269a726a02023-11-23T11:59:23ZengMDPI AGMaterials1996-19442022-05-011510370210.3390/ma15103702Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage MaterialDequan Zou0Xiangji Yue1Tianyi He2Jianan Ding3Dechun Ba4School of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, ChinaSchool of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, ChinaSchool of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, ChinaSchool of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, ChinaSchool of Mechanical Engineering and Automation, Northeastern University, Shenyang 110819, ChinaThermochemical adsorption energy storage is a potential energy utilization technology. Among these technologies, the composite energy storage material prepared by K<sub>2</sub>CO<sub>3</sub> and expanded vermiculite (EVM) shows excellent performance. In this paper, the influence of the preparation process using the impregnation method and vacuum impregnation method on K<sub>2</sub>CO<sub>3</sub>/EVM composite material is studied. The preparation plan is further optimized with the solution concentration and the expanded vermiculite particle size as variables. In the experiment, mercury intrusion porosimetry (MIP) is used to measure the porosity and other parameters. Additionally, with the help of scanning electron microscopy (SEM), the morphological characteristics of the materials are obtained from a microscopic point of view. The effects of different preparation parameters are evaluated by comparing the experimental results. The results show that the K<sub>2</sub>CO<sub>3</sub> specific gravity of the composite material increases with the increase of the vacuum degree, up to 70.440 wt.% (the vacuum degree is 6.7 kPa). Expanded vermiculite with a large particle size (3~6 mm) can carry more K<sub>2</sub>CO<sub>3</sub>, and content per cubic centimeter of K<sub>2</sub>CO<sub>3</sub> can be as high as 0.466 g.https://www.mdpi.com/1996-1944/15/10/3702thermochemical energy storagesalt hydratesvacuum impregnationK<sub>2</sub>CO<sub>3</sub>expanded vermiculite
spellingShingle Dequan Zou
Xiangji Yue
Tianyi He
Jianan Ding
Dechun Ba
Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
Materials
thermochemical energy storage
salt hydrates
vacuum impregnation
K<sub>2</sub>CO<sub>3</sub>
expanded vermiculite
title Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
title_full Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
title_fullStr Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
title_full_unstemmed Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
title_short Experimental Research on the Preparation of K<sub>2</sub>CO<sub>3</sub>/Expanded Vermiculite Composite Energy Storage Material
title_sort experimental research on the preparation of k sub 2 sub co sub 3 sub expanded vermiculite composite energy storage material
topic thermochemical energy storage
salt hydrates
vacuum impregnation
K<sub>2</sub>CO<sub>3</sub>
expanded vermiculite
url https://www.mdpi.com/1996-1944/15/10/3702
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