Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling

During the start-stop process of high-precision instruments in service, the critical materials of instruments undergo thermal cycling, resulting in changes in microstructure and dimension. In this paper, the evolution and coupling effects of dislocations and precipitates within 2024 Al alloy during...

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Main Authors: Youfang Cao, Longtao Jiang, Guwei Shen, Deng Gong, Jiancun Rao, Guoqin Chen
Format: Article
Language:English
Published: Elsevier 2024-01-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785423031988
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author Youfang Cao
Longtao Jiang
Guwei Shen
Deng Gong
Jiancun Rao
Guoqin Chen
author_facet Youfang Cao
Longtao Jiang
Guwei Shen
Deng Gong
Jiancun Rao
Guoqin Chen
author_sort Youfang Cao
collection DOAJ
description During the start-stop process of high-precision instruments in service, the critical materials of instruments undergo thermal cycling, resulting in changes in microstructure and dimension. In this paper, the evolution and coupling effects of dislocations and precipitates within 2024 Al alloy during 500 cycles were investigated, and their influence on the dimensional change was quantitatively characterized and decoupling analyzed. Transmission Electron Microscopy (TEM)/aberration-corrected scanning TEM (CS-TEM), X-ray diffraction (XRD), and Three-Dimensional Atom Probe Tomography (3D-APT) were used for microstructural evolution analysis and quantitative statistics. The dislocation density increased from 3.32 × 1014 m−2 to 5.75 × 1014 m−2 after 500 cycles, which accelerated elemental diffusion and provided nucleation sites of precipitates, contributing to an increase in the number density of the S'/S phase from 1.04 × 1024 m−3 to 1.41 × 1024 m−3. Based on the quantitative statistics of precipitate types and corresponding volume fractions, the dimensional change induced by precipitate evolution was −1.25 × 10−4. The dimensional change caused by the free volume introduced by dislocation density was 3.32 × 10−6. Comparing these values with the experimental value of −1.94 × 10−4, it is clear that the precipitate evolution is the main factor that triggers the dimensional change.
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spelling doaj.art-5c716d166e104d33a2ad1f4c01f220462024-01-31T05:43:43ZengElsevierJournal of Materials Research and Technology2238-78542024-01-012823132325Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cyclingYoufang Cao0Longtao Jiang1Guwei Shen2Deng Gong3Jiancun Rao4Guoqin Chen5School of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, ChinaSchool of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, China; State Key Laboratory of Advanced Welding Production Technology, Harbin Institute of Technology, Harbin, 150001, China; Corresponding author. School of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, China.School of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, China; Corresponding author.School of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, China; Aero Engine Control System Institute, Aero Engine Corporation of China, Wuxi, 214063, ChinaAIM Lab, Maryland NanoCenter, University of Maryland, MD, 20742, USASchool of Materials and Engineering, Harbin Institute of Technology, Harbin, 150001, China; Corresponding author.During the start-stop process of high-precision instruments in service, the critical materials of instruments undergo thermal cycling, resulting in changes in microstructure and dimension. In this paper, the evolution and coupling effects of dislocations and precipitates within 2024 Al alloy during 500 cycles were investigated, and their influence on the dimensional change was quantitatively characterized and decoupling analyzed. Transmission Electron Microscopy (TEM)/aberration-corrected scanning TEM (CS-TEM), X-ray diffraction (XRD), and Three-Dimensional Atom Probe Tomography (3D-APT) were used for microstructural evolution analysis and quantitative statistics. The dislocation density increased from 3.32 × 1014 m−2 to 5.75 × 1014 m−2 after 500 cycles, which accelerated elemental diffusion and provided nucleation sites of precipitates, contributing to an increase in the number density of the S'/S phase from 1.04 × 1024 m−3 to 1.41 × 1024 m−3. Based on the quantitative statistics of precipitate types and corresponding volume fractions, the dimensional change induced by precipitate evolution was −1.25 × 10−4. The dimensional change caused by the free volume introduced by dislocation density was 3.32 × 10−6. Comparing these values with the experimental value of −1.94 × 10−4, it is clear that the precipitate evolution is the main factor that triggers the dimensional change.http://www.sciencedirect.com/science/article/pii/S2238785423031988Aluminum alloyDimensional stabilityThermal cyclingPrecipitateDislocation
spellingShingle Youfang Cao
Longtao Jiang
Guwei Shen
Deng Gong
Jiancun Rao
Guoqin Chen
Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
Journal of Materials Research and Technology
Aluminum alloy
Dimensional stability
Thermal cycling
Precipitate
Dislocation
title Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
title_full Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
title_fullStr Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
title_full_unstemmed Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
title_short Quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 Al alloy during long-term thermal cycling
title_sort quantitative study on the microstructural evolution and dimensional stability mechanism of 2024 al alloy during long term thermal cycling
topic Aluminum alloy
Dimensional stability
Thermal cycling
Precipitate
Dislocation
url http://www.sciencedirect.com/science/article/pii/S2238785423031988
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