High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds

In this study, TiC0·5N0.5–70 wt% W cermet specimens consisting of a core–rim grain structure with coherent interfaces and the binder phase were prepared by blending TiC0·5N0.5 and W powders with particle sizes of less than 1 μm and then spark plasma sintering the blended powders. The compression tes...

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Main Authors: Takashi Murakami, Masahito Katoh, Daisuke Matsukura, Kyosuke Yoshimi
Format: Article
Language:English
Published: Elsevier 2023-05-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785423009328
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author Takashi Murakami
Masahito Katoh
Daisuke Matsukura
Kyosuke Yoshimi
author_facet Takashi Murakami
Masahito Katoh
Daisuke Matsukura
Kyosuke Yoshimi
author_sort Takashi Murakami
collection DOAJ
description In this study, TiC0·5N0.5–70 wt% W cermet specimens consisting of a core–rim grain structure with coherent interfaces and the binder phase were prepared by blending TiC0·5N0.5 and W powders with particle sizes of less than 1 μm and then spark plasma sintering the blended powders. The compression tests of the cermet specimens were conducted in the temperature range of 1873 K–2073 K in a vacuum and under Ar gas flow conditions. At all testing temperatures, this cermet exhibited much higher yield stress than MoSiBTiC and MoNbTaVW high-entropy alloys, which are some of the structural materials showing the highest strength at temperatures exceeding 1873 K. After isothermal upset forging of commercially available solid-solution heat-treated Inconel 718 alloy specimens with a diameter of 5 mm and a height of 5 mm using cermet molds at loads of 40 kN and 10 kN at 1273 K and 1373 K in a vacuum, respectively, their average grain size (2 μm) was found to be much smaller than that before forging. Such fine microstructures were assumed to be formed by dynamic recrystallization during forging.
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spelling doaj.art-5ccfde6ffd8043d5acbb1942b2d194822023-06-21T06:57:15ZengElsevierJournal of Materials Research and Technology2238-78542023-05-012465786587High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet moldsTakashi Murakami0Masahito Katoh1Daisuke Matsukura2Kyosuke Yoshimi3Advanced Manufacturing Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Ibaraki, 305-8564, Japan; Corresponding author.Advanced Manufacturing Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Ibaraki, 305-8564, JapanDepartment of Materials Science and Engineering, School of Engineering, Tohoku University, Sendai, Miyagi, 980-8579, JapanDepartment of Materials Science and Engineering, School of Engineering, Tohoku University, Sendai, Miyagi, 980-8579, JapanIn this study, TiC0·5N0.5–70 wt% W cermet specimens consisting of a core–rim grain structure with coherent interfaces and the binder phase were prepared by blending TiC0·5N0.5 and W powders with particle sizes of less than 1 μm and then spark plasma sintering the blended powders. The compression tests of the cermet specimens were conducted in the temperature range of 1873 K–2073 K in a vacuum and under Ar gas flow conditions. At all testing temperatures, this cermet exhibited much higher yield stress than MoSiBTiC and MoNbTaVW high-entropy alloys, which are some of the structural materials showing the highest strength at temperatures exceeding 1873 K. After isothermal upset forging of commercially available solid-solution heat-treated Inconel 718 alloy specimens with a diameter of 5 mm and a height of 5 mm using cermet molds at loads of 40 kN and 10 kN at 1273 K and 1373 K in a vacuum, respectively, their average grain size (2 μm) was found to be much smaller than that before forging. Such fine microstructures were assumed to be formed by dynamic recrystallization during forging.http://www.sciencedirect.com/science/article/pii/S2238785423009328Cermet: high-temperature compression test: isothermal forging: Inconel 718Spark plasma sintering
spellingShingle Takashi Murakami
Masahito Katoh
Daisuke Matsukura
Kyosuke Yoshimi
High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
Journal of Materials Research and Technology
Cermet: high-temperature compression test: isothermal forging: Inconel 718
Spark plasma sintering
title High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
title_full High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
title_fullStr High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
title_full_unstemmed High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
title_short High-temperature compression tests of Ti(C, N)–70 wt% W cermet and isothermal forging of Inconel 718 alloys using cermet molds
title_sort high temperature compression tests of ti c n 70 wt w cermet and isothermal forging of inconel 718 alloys using cermet molds
topic Cermet: high-temperature compression test: isothermal forging: Inconel 718
Spark plasma sintering
url http://www.sciencedirect.com/science/article/pii/S2238785423009328
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