Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment

Ti–6Al–4V alloy was subjected to cryogenic treatment at −196 °C followed by single and multiple treatment cycles. Compression tests revealed that, despite a decrease in yield strength, cryogenically treated samples (especially by multiple cryogenic treatment) exhibited noteworthy improvements, with...

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Main Authors: Hyun-Hak Kang, Seung-Chang Han, Min-Ki Ji, Jeong-Rim Lee, Tea-Sung Jun
Format: Article
Language:English
Published: Elsevier 2024-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424005039
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author Hyun-Hak Kang
Seung-Chang Han
Min-Ki Ji
Jeong-Rim Lee
Tea-Sung Jun
author_facet Hyun-Hak Kang
Seung-Chang Han
Min-Ki Ji
Jeong-Rim Lee
Tea-Sung Jun
author_sort Hyun-Hak Kang
collection DOAJ
description Ti–6Al–4V alloy was subjected to cryogenic treatment at −196 °C followed by single and multiple treatment cycles. Compression tests revealed that, despite a decrease in yield strength, cryogenically treated samples (especially by multiple cryogenic treatment) exhibited noteworthy improvements, with a 10.2% failure strain and 9.4% rise in compressive strength compared to the as-received state. The cryogenically treated samples were further refined and exhibited a reduced β-phase volume fraction, showed higher dislocation density and microstrain in X-ray diffraction results. Remarkably, the surface hardness was significantly improved by the cryogenic treatment, leading to enhanced wear resistance with lower coefficients of friction. This was attributed to the formation of smaller wear debris and a decrease in abrasive wear under sliding conditions. Electron backscatter diffraction (EBSD) findings demonstrate that the friction-induced localized deformation layers exhibit the high density of low angle grain boundaries (LAGBs) with deformation-induced sub-grains. The synergistic improvement of wear resistance and mechanical properties is ascribed to the intricate microstructural alterations induced during cryogenic treatment, particularly accentuated in multiple cryogenic treatment. These findings highlight the efficacy of cryogenic treatment in improving both mechanical and wear properties of Ti–6Al–4V alloy.
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spelling doaj.art-5d1c82be8c29450aa36ef413947effd32024-03-24T06:58:42ZengElsevierJournal of Materials Research and Technology2238-78542024-03-012951185125Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatmentHyun-Hak Kang0Seung-Chang Han1Min-Ki Ji2Jeong-Rim Lee3Tea-Sung Jun4Department of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of KoreaDepartment of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of KoreaDepartment of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of KoreaDepartment of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of KoreaDepartment of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of Korea; Research Institute for Engineering and Technology, Incheon National University, Incheon 22012, Republic of Korea; Corresponding author. Department of Mechanical Engineering, Incheon National University, Incheon 22012, Republic of Korea.Ti–6Al–4V alloy was subjected to cryogenic treatment at −196 °C followed by single and multiple treatment cycles. Compression tests revealed that, despite a decrease in yield strength, cryogenically treated samples (especially by multiple cryogenic treatment) exhibited noteworthy improvements, with a 10.2% failure strain and 9.4% rise in compressive strength compared to the as-received state. The cryogenically treated samples were further refined and exhibited a reduced β-phase volume fraction, showed higher dislocation density and microstrain in X-ray diffraction results. Remarkably, the surface hardness was significantly improved by the cryogenic treatment, leading to enhanced wear resistance with lower coefficients of friction. This was attributed to the formation of smaller wear debris and a decrease in abrasive wear under sliding conditions. Electron backscatter diffraction (EBSD) findings demonstrate that the friction-induced localized deformation layers exhibit the high density of low angle grain boundaries (LAGBs) with deformation-induced sub-grains. The synergistic improvement of wear resistance and mechanical properties is ascribed to the intricate microstructural alterations induced during cryogenic treatment, particularly accentuated in multiple cryogenic treatment. These findings highlight the efficacy of cryogenic treatment in improving both mechanical and wear properties of Ti–6Al–4V alloy.http://www.sciencedirect.com/science/article/pii/S2238785424005039Cryogenic treatmentEBSDWearBall-on-discTi–6Al–4V
spellingShingle Hyun-Hak Kang
Seung-Chang Han
Min-Ki Ji
Jeong-Rim Lee
Tea-Sung Jun
Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
Journal of Materials Research and Technology
Cryogenic treatment
EBSD
Wear
Ball-on-disc
Ti–6Al–4V
title Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
title_full Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
title_fullStr Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
title_full_unstemmed Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
title_short Achieving synergistic improvement of wear and mechanical properties in Ti–6Al–4V alloy by multiple cryogenic treatment
title_sort achieving synergistic improvement of wear and mechanical properties in ti 6al 4v alloy by multiple cryogenic treatment
topic Cryogenic treatment
EBSD
Wear
Ball-on-disc
Ti–6Al–4V
url http://www.sciencedirect.com/science/article/pii/S2238785424005039
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