Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications

This work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystalli...

Full description

Bibliographic Details
Main Authors: El-Habib Imroi, Roynette Anne, Morakchi-Goudjil Houda, Lemarchand Alex, Mielcarek Christine, Azouani Rabah, Traore Mamadou
Format: Article
Language:English
Published: EDP Sciences 2023-01-01
Series:MATEC Web of Conferences
Subjects:
Online Access:https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdf
_version_ 1797807579879964672
author El-Habib Imroi
Roynette Anne
Morakchi-Goudjil Houda
Lemarchand Alex
Mielcarek Christine
Azouani Rabah
Traore Mamadou
author_facet El-Habib Imroi
Roynette Anne
Morakchi-Goudjil Houda
Lemarchand Alex
Mielcarek Christine
Azouani Rabah
Traore Mamadou
author_sort El-Habib Imroi
collection DOAJ
description This work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystallization of ZnO at low temperature (<110°C). Our experiments have also shown that these reagents exert an influence on the size of the NPs. The NPs after precipitation are recovered in the form of powders then characterized by different techniques: X-ray diffraction (XRD) and Raman spectroscopy. The crystalline domain size are calculated from Scherrer’s formula. The antimicrobial potential of these NPs has been studied. The technique applied for this evaluation consists in estimating the minimum inhibitory concentration (MIC) of the NPs by measuring the evolution of the optical density of the bacteria over time. The results showed that the synthesized ZnO NPs show efficacy on the Escherichia coli bacteria.
first_indexed 2024-03-13T06:24:41Z
format Article
id doaj.art-5d37dabdb62c4607b6f23b4c9cfff0b9
institution Directory Open Access Journal
issn 2261-236X
language English
last_indexed 2024-03-13T06:24:41Z
publishDate 2023-01-01
publisher EDP Sciences
record_format Article
series MATEC Web of Conferences
spelling doaj.art-5d37dabdb62c4607b6f23b4c9cfff0b92023-06-09T09:28:19ZengEDP SciencesMATEC Web of Conferences2261-236X2023-01-013790600310.1051/matecconf/202337906003matecconf_sfgp23_06003Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applicationsEl-Habib Imroi0Roynette Anne1Morakchi-Goudjil Houda2Lemarchand Alex3Mielcarek Christine4Azouani Rabah5Traore Mamadou6Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordEcole de Biologie Industrielle (EBI)Ecole de Biologie Industrielle (EBI)Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordEcole de Biologie Industrielle (EBI)Ecole de Biologie Industrielle (EBI)Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordThis work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystallization of ZnO at low temperature (<110°C). Our experiments have also shown that these reagents exert an influence on the size of the NPs. The NPs after precipitation are recovered in the form of powders then characterized by different techniques: X-ray diffraction (XRD) and Raman spectroscopy. The crystalline domain size are calculated from Scherrer’s formula. The antimicrobial potential of these NPs has been studied. The technique applied for this evaluation consists in estimating the minimum inhibitory concentration (MIC) of the NPs by measuring the evolution of the optical density of the bacteria over time. The results showed that the synthesized ZnO NPs show efficacy on the Escherichia coli bacteria.https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdfchimie doucesol-gelznonanoparticulesbactériesantimicrobien
spellingShingle El-Habib Imroi
Roynette Anne
Morakchi-Goudjil Houda
Lemarchand Alex
Mielcarek Christine
Azouani Rabah
Traore Mamadou
Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
MATEC Web of Conferences
chimie douce
sol-gel
zno
nanoparticules
bactéries
antimicrobien
title Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
title_full Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
title_fullStr Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
title_full_unstemmed Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
title_short Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
title_sort synthesis by soft chemistry of size controlled zinc oxide zno nanocrystals for antimicrobial applications
topic chimie douce
sol-gel
zno
nanoparticules
bactéries
antimicrobien
url https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdf
work_keys_str_mv AT elhabibimroi synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT roynetteanne synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT morakchigoudjilhouda synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT lemarchandalex synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT mielcarekchristine synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT azouanirabah synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications
AT traoremamadou synthesisbysoftchemistryofsizecontrolledzincoxideznonanocrystalsforantimicrobialapplications