Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications
This work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystalli...
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Format: | Article |
Language: | English |
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EDP Sciences
2023-01-01
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Series: | MATEC Web of Conferences |
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Online Access: | https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdf |
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author | El-Habib Imroi Roynette Anne Morakchi-Goudjil Houda Lemarchand Alex Mielcarek Christine Azouani Rabah Traore Mamadou |
author_facet | El-Habib Imroi Roynette Anne Morakchi-Goudjil Houda Lemarchand Alex Mielcarek Christine Azouani Rabah Traore Mamadou |
author_sort | El-Habib Imroi |
collection | DOAJ |
description | This work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystallization of ZnO at low temperature (<110°C). Our experiments have also shown that these reagents exert an influence on the size of the NPs. The NPs after precipitation are recovered in the form of powders then characterized by different techniques: X-ray diffraction (XRD) and Raman spectroscopy. The crystalline domain size are calculated from Scherrer’s formula. The antimicrobial potential of these NPs has been studied. The technique applied for this evaluation consists in estimating the minimum inhibitory concentration (MIC) of the NPs by measuring the evolution of the optical density of the bacteria over time. The results showed that the synthesized ZnO NPs show efficacy on the Escherichia coli bacteria. |
first_indexed | 2024-03-13T06:24:41Z |
format | Article |
id | doaj.art-5d37dabdb62c4607b6f23b4c9cfff0b9 |
institution | Directory Open Access Journal |
issn | 2261-236X |
language | English |
last_indexed | 2024-03-13T06:24:41Z |
publishDate | 2023-01-01 |
publisher | EDP Sciences |
record_format | Article |
series | MATEC Web of Conferences |
spelling | doaj.art-5d37dabdb62c4607b6f23b4c9cfff0b92023-06-09T09:28:19ZengEDP SciencesMATEC Web of Conferences2261-236X2023-01-013790600310.1051/matecconf/202337906003matecconf_sfgp23_06003Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applicationsEl-Habib Imroi0Roynette Anne1Morakchi-Goudjil Houda2Lemarchand Alex3Mielcarek Christine4Azouani Rabah5Traore Mamadou6Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordEcole de Biologie Industrielle (EBI)Ecole de Biologie Industrielle (EBI)Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordEcole de Biologie Industrielle (EBI)Ecole de Biologie Industrielle (EBI)Laboratoire des Sciences de Procédés et des Matériaux (LSPM-CNRS), Institut Galilée, Université Sorbonne Paris NordThis work focuses on the synthesis of ZnO nanoparticles (NPs) by the sol-gel method for antimicrobial applications. The influence of synthesis parameters on the size of NPs is discussed. The addition of water and an alcoholamine (Monoethanolamine MEA) during the synthesis made possible the crystallization of ZnO at low temperature (<110°C). Our experiments have also shown that these reagents exert an influence on the size of the NPs. The NPs after precipitation are recovered in the form of powders then characterized by different techniques: X-ray diffraction (XRD) and Raman spectroscopy. The crystalline domain size are calculated from Scherrer’s formula. The antimicrobial potential of these NPs has been studied. The technique applied for this evaluation consists in estimating the minimum inhibitory concentration (MIC) of the NPs by measuring the evolution of the optical density of the bacteria over time. The results showed that the synthesized ZnO NPs show efficacy on the Escherichia coli bacteria.https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdfchimie doucesol-gelznonanoparticulesbactériesantimicrobien |
spellingShingle | El-Habib Imroi Roynette Anne Morakchi-Goudjil Houda Lemarchand Alex Mielcarek Christine Azouani Rabah Traore Mamadou Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications MATEC Web of Conferences chimie douce sol-gel zno nanoparticules bactéries antimicrobien |
title | Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications |
title_full | Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications |
title_fullStr | Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications |
title_full_unstemmed | Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications |
title_short | Synthesis by soft chemistry of size-controlled zinc oxide (ZnO) nanocrystals for antimicrobial applications |
title_sort | synthesis by soft chemistry of size controlled zinc oxide zno nanocrystals for antimicrobial applications |
topic | chimie douce sol-gel zno nanoparticules bactéries antimicrobien |
url | https://www.matec-conferences.org/articles/matecconf/pdf/2023/06/matecconf_sfgp23_06003.pdf |
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