Experimento utilizando grãos para explorar a calibração em análises químicas
The conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method...
Main Authors: | , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Sociedade Brasileira de Química
2014-01-01
|
Series: | Química Nova |
Subjects: | |
Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=en |
_version_ | 1818112925971251200 |
---|---|
author | Daniel Menezes Silvestre Juliana Naozuka Paulo Rogério Miranda Correia Cassiana Seimi Nomura |
author_facet | Daniel Menezes Silvestre Juliana Naozuka Paulo Rogério Miranda Correia Cassiana Seimi Nomura |
author_sort | Daniel Menezes Silvestre |
collection | DOAJ |
description | The conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method calibration is one of the most critical parameters that has to be grasped since most analytical techniques depend on it for quantitative analysis. The conceptual understanding of calibration is not trivial for undergraduate students. External calibration is widely discussed during instrumental analysis courses. However, the understanding of the limitations of external calibration to correct some systematic errors is not directly derived from laboratory examples. The conceptual understanding of other calibration methods (standard addition, matrix matching, and internal standard) is imperative. The aim of this work is to present a simple experiment using grains (beans, corn and chickpeas) to explore different types of calibration methods. |
first_indexed | 2024-12-11T03:26:41Z |
format | Article |
id | doaj.art-5dece9550c49417a864cabf262385f73 |
institution | Directory Open Access Journal |
issn | 1678-7064 |
language | English |
last_indexed | 2024-12-11T03:26:41Z |
publishDate | 2014-01-01 |
publisher | Sociedade Brasileira de Química |
record_format | Article |
series | Química Nova |
spelling | doaj.art-5dece9550c49417a864cabf262385f732022-12-22T01:22:29ZengSociedade Brasileira de QuímicaQuímica Nova1678-70642014-01-013791545154910.5935/0100-4042.20140209S0100-40422014000900020Experimento utilizando grãos para explorar a calibração em análises químicasDaniel Menezes Silvestre0Juliana Naozuka1Paulo Rogério Miranda Correia2Cassiana Seimi Nomura3Universidade de São PauloUniversidade Federal de São PauloUniversidade de São PauloUniversidade de São PauloThe conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method calibration is one of the most critical parameters that has to be grasped since most analytical techniques depend on it for quantitative analysis. The conceptual understanding of calibration is not trivial for undergraduate students. External calibration is widely discussed during instrumental analysis courses. However, the understanding of the limitations of external calibration to correct some systematic errors is not directly derived from laboratory examples. The conceptual understanding of other calibration methods (standard addition, matrix matching, and internal standard) is imperative. The aim of this work is to present a simple experiment using grains (beans, corn and chickpeas) to explore different types of calibration methods.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=encalibrationinstrumental analysisinternal standardstandard addition |
spellingShingle | Daniel Menezes Silvestre Juliana Naozuka Paulo Rogério Miranda Correia Cassiana Seimi Nomura Experimento utilizando grãos para explorar a calibração em análises químicas Química Nova calibration instrumental analysis internal standard standard addition |
title | Experimento utilizando grãos para explorar a calibração em análises químicas |
title_full | Experimento utilizando grãos para explorar a calibração em análises químicas |
title_fullStr | Experimento utilizando grãos para explorar a calibração em análises químicas |
title_full_unstemmed | Experimento utilizando grãos para explorar a calibração em análises químicas |
title_short | Experimento utilizando grãos para explorar a calibração em análises químicas |
title_sort | experimento utilizando graos para explorar a calibracao em analises quimicas |
topic | calibration instrumental analysis internal standard standard addition |
url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=en |
work_keys_str_mv | AT danielmenezessilvestre experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas AT juliananaozuka experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas AT paulorogeriomirandacorreia experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas AT cassianaseiminomura experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas |