Experimento utilizando grãos para explorar a calibração em análises químicas

The conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method...

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Main Authors: Daniel Menezes Silvestre, Juliana Naozuka, Paulo Rogério Miranda Correia, Cassiana Seimi Nomura
Format: Article
Language:English
Published: Sociedade Brasileira de Química 2014-01-01
Series:Química Nova
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=en
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author Daniel Menezes Silvestre
Juliana Naozuka
Paulo Rogério Miranda Correia
Cassiana Seimi Nomura
author_facet Daniel Menezes Silvestre
Juliana Naozuka
Paulo Rogério Miranda Correia
Cassiana Seimi Nomura
author_sort Daniel Menezes Silvestre
collection DOAJ
description The conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method calibration is one of the most critical parameters that has to be grasped since most analytical techniques depend on it for quantitative analysis. The conceptual understanding of calibration is not trivial for undergraduate students. External calibration is widely discussed during instrumental analysis courses. However, the understanding of the limitations of external calibration to correct some systematic errors is not directly derived from laboratory examples. The conceptual understanding of other calibration methods (standard addition, matrix matching, and internal standard) is imperative. The aim of this work is to present a simple experiment using grains (beans, corn and chickpeas) to explore different types of calibration methods.
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spelling doaj.art-5dece9550c49417a864cabf262385f732022-12-22T01:22:29ZengSociedade Brasileira de QuímicaQuímica Nova1678-70642014-01-013791545154910.5935/0100-4042.20140209S0100-40422014000900020Experimento utilizando grãos para explorar a calibração em análises químicasDaniel Menezes Silvestre0Juliana Naozuka1Paulo Rogério Miranda Correia2Cassiana Seimi Nomura3Universidade de São PauloUniversidade Federal de São PauloUniversidade de São PauloUniversidade de São PauloThe conventional curriculum of Analytical Chemistry undergraduate courses emphasizes the introduction of techniques, methods and procedures used for instrumental analysis. All these concepts must be integrated into a sound conceptual framework to allow students to make appropriate decisions. Method calibration is one of the most critical parameters that has to be grasped since most analytical techniques depend on it for quantitative analysis. The conceptual understanding of calibration is not trivial for undergraduate students. External calibration is widely discussed during instrumental analysis courses. However, the understanding of the limitations of external calibration to correct some systematic errors is not directly derived from laboratory examples. The conceptual understanding of other calibration methods (standard addition, matrix matching, and internal standard) is imperative. The aim of this work is to present a simple experiment using grains (beans, corn and chickpeas) to explore different types of calibration methods.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=encalibrationinstrumental analysisinternal standardstandard addition
spellingShingle Daniel Menezes Silvestre
Juliana Naozuka
Paulo Rogério Miranda Correia
Cassiana Seimi Nomura
Experimento utilizando grãos para explorar a calibração em análises químicas
Química Nova
calibration
instrumental analysis
internal standard
standard addition
title Experimento utilizando grãos para explorar a calibração em análises químicas
title_full Experimento utilizando grãos para explorar a calibração em análises químicas
title_fullStr Experimento utilizando grãos para explorar a calibração em análises químicas
title_full_unstemmed Experimento utilizando grãos para explorar a calibração em análises químicas
title_short Experimento utilizando grãos para explorar a calibração em análises químicas
title_sort experimento utilizando graos para explorar a calibracao em analises quimicas
topic calibration
instrumental analysis
internal standard
standard addition
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000900020&lng=en&tlng=en
work_keys_str_mv AT danielmenezessilvestre experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas
AT juliananaozuka experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas
AT paulorogeriomirandacorreia experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas
AT cassianaseiminomura experimentoutilizandograosparaexploraracalibracaoemanalisesquimicas