Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition

Сobalt-based catalysts are one of the possible candidates for catalysts that accelerate the decomposition of water to produce energy. In this work, the one-dimension GeCo nanostructures have been prepared by electrochemical deposition in a three-electrode cell. The samples have been annealed in atmo...

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Main Authors: Martynova Irina, Gavrilin Ilya
Format: Article
Language:English
Published: Peter the Great St.Petersburg Polytechnic University 2022-10-01
Series:St. Petersburg Polytechnical University Journal: Physics and Mathematics
Subjects:
Online Access:https://physmath.spbstu.ru/article/2022.58.39/
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author Martynova Irina
Gavrilin Ilya
author_facet Martynova Irina
Gavrilin Ilya
author_sort Martynova Irina
collection DOAJ
description Сobalt-based catalysts are one of the possible candidates for catalysts that accelerate the decomposition of water to produce energy. In this work, the one-dimension GeCo nanostructures have been prepared by electrochemical deposition in a three-electrode cell. The samples have been annealed in atmosphere at various temperature (300 ºC, 450 ºC, 600 ºC). Effect of thermal annealing on the composition of Ge-Co nanostructure has been studied. The morphology of the obtained Ge-Co nanostructures has been investigated using scanning electron microscopy The method of X-ray diffraction analysis has been used to investigate composition changes of Ge-Co. Diffractograms show the presence of Co2GeO4 catalyst at an annealing temperature of 600 ºC. The sample with this annealing temperature shows the best properties as oxygen evolution catalyst.
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spelling doaj.art-5eac975b4956465e93070d1afe8b1aba2022-12-22T02:43:00ZengPeter the Great St.Petersburg Polytechnic UniversitySt. Petersburg Polytechnical University Journal: Physics and Mathematics2405-72232022-10-01153.110.18721/JPM.153.13920714726Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical depositionMartynova Irina0https://orcid.org/0000-0002-6128-5244Gavrilin Ilya1https://orcid.org/0000-0002-0278-1598National Research University of Electronic TechnologyNational Research University of Electronic TechnologyСobalt-based catalysts are one of the possible candidates for catalysts that accelerate the decomposition of water to produce energy. In this work, the one-dimension GeCo nanostructures have been prepared by electrochemical deposition in a three-electrode cell. The samples have been annealed in atmosphere at various temperature (300 ºC, 450 ºC, 600 ºC). Effect of thermal annealing on the composition of Ge-Co nanostructure has been studied. The morphology of the obtained Ge-Co nanostructures has been investigated using scanning electron microscopy The method of X-ray diffraction analysis has been used to investigate composition changes of Ge-Co. Diffractograms show the presence of Co2GeO4 catalyst at an annealing temperature of 600 ºC. The sample with this annealing temperature shows the best properties as oxygen evolution catalyst.https://physmath.spbstu.ru/article/2022.58.39/ge-co nanostructuresoxygen evolution catalystge nanowireselectrochemical deposition
spellingShingle Martynova Irina
Gavrilin Ilya
Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
St. Petersburg Polytechnical University Journal: Physics and Mathematics
ge-co nanostructures
oxygen evolution catalyst
ge nanowires
electrochemical deposition
title Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
title_full Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
title_fullStr Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
title_full_unstemmed Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
title_short Effect of thermal annealing on the composition of Ge-Co nanostructure obtained by electrochemical deposition
title_sort effect of thermal annealing on the composition of ge co nanostructure obtained by electrochemical deposition
topic ge-co nanostructures
oxygen evolution catalyst
ge nanowires
electrochemical deposition
url https://physmath.spbstu.ru/article/2022.58.39/
work_keys_str_mv AT martynovairina effectofthermalannealingonthecompositionofgeconanostructureobtainedbyelectrochemicaldeposition
AT gavrilinilya effectofthermalannealingonthecompositionofgeconanostructureobtainedbyelectrochemicaldeposition