A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation

The objectives of this study were to experimentally determine the effects of the stress relaxation of a cyanate-ester-based composite, derive and integrate constitutive equations into commercial FEM software, and apply this approach to understand the formation of residual stress in a typical aerospa...

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Main Authors: Nicolas Gort, Fabian Schadt, Martin Liebisch, Christian Brauner, Tobias Wille
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/15/19/6675
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author Nicolas Gort
Fabian Schadt
Martin Liebisch
Christian Brauner
Tobias Wille
author_facet Nicolas Gort
Fabian Schadt
Martin Liebisch
Christian Brauner
Tobias Wille
author_sort Nicolas Gort
collection DOAJ
description The objectives of this study were to experimentally determine the effects of the stress relaxation of a cyanate-ester-based composite, derive and integrate constitutive equations into commercial FEM software, and apply this approach to understand the formation of residual stress in a typical aerospace structure—namely, a stiffened panel. In preliminary studies, a cyanate-ester-based composite with increased fracture toughness for high-temperature applications was developed. High curing temperatures up to 260 °C will inevitably lead to high process-induced stresses. To assess the magnitude of impact on the development of internal stresses, the relaxation behavior of the neat resin was measured and characterized. The system was toughened, and the effect of stress relaxation increased as the temperature got closer to the glass transition temperature of the toughener, which was approximately 240 °C. With the use of an incremental linear viscoelastic model, the relaxation behavior was integrated into a process model with a holistic approach. A stiffened panel was manufactured and used as the validation use case. The displacement field was validated with an optical 3D measuring system, and good agreement was found between the simulated and experimental results. The maximum difference between the elastic and the viscoelastic solution was found to be 15%. Furthermore, the stress magnitude in the transverse material direction resulted in a more critical value higher than the material strength.
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spelling doaj.art-5ff0f0ab75f0425a82d130dc6a766b842023-11-23T20:54:48ZengMDPI AGMaterials1996-19442022-09-011519667510.3390/ma15196675A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress RelaxationNicolas Gort0Fabian Schadt1Martin Liebisch2Christian Brauner3Tobias Wille4Institute of Polymer Engineering, FHNW University of Applied Sciences and Arts Northwestern Switzerland, Klosterzelgstrasse 2, 5210 Windisch, SwitzerlandInstitute of Polymer Engineering, FHNW University of Applied Sciences and Arts Northwestern Switzerland, Klosterzelgstrasse 2, 5210 Windisch, SwitzerlandInstitute of Composite Structures and Adaptive Systems, German Aerospace Center, Lilienthalplatz 7, 38108 Braunschweig, GermanyInstitute of Polymer Engineering, FHNW University of Applied Sciences and Arts Northwestern Switzerland, Klosterzelgstrasse 2, 5210 Windisch, SwitzerlandInstitute of Composite Structures and Adaptive Systems, German Aerospace Center, Lilienthalplatz 7, 38108 Braunschweig, GermanyThe objectives of this study were to experimentally determine the effects of the stress relaxation of a cyanate-ester-based composite, derive and integrate constitutive equations into commercial FEM software, and apply this approach to understand the formation of residual stress in a typical aerospace structure—namely, a stiffened panel. In preliminary studies, a cyanate-ester-based composite with increased fracture toughness for high-temperature applications was developed. High curing temperatures up to 260 °C will inevitably lead to high process-induced stresses. To assess the magnitude of impact on the development of internal stresses, the relaxation behavior of the neat resin was measured and characterized. The system was toughened, and the effect of stress relaxation increased as the temperature got closer to the glass transition temperature of the toughener, which was approximately 240 °C. With the use of an incremental linear viscoelastic model, the relaxation behavior was integrated into a process model with a holistic approach. A stiffened panel was manufactured and used as the validation use case. The displacement field was validated with an optical 3D measuring system, and good agreement was found between the simulated and experimental results. The maximum difference between the elastic and the viscoelastic solution was found to be 15%. Furthermore, the stress magnitude in the transverse material direction resulted in a more critical value higher than the material strength.https://www.mdpi.com/1996-1944/15/19/6675composite materialscyanate estertougheninghigh-temperature applicationprocess-induced deformation/stressviscoelastic
spellingShingle Nicolas Gort
Fabian Schadt
Martin Liebisch
Christian Brauner
Tobias Wille
A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
Materials
composite materials
cyanate ester
toughening
high-temperature application
process-induced deformation/stress
viscoelastic
title A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
title_full A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
title_fullStr A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
title_full_unstemmed A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
title_short A Manufacturing Process Simulation of Toughened Cyanate-Ester-Based Composite Structures with Respect to Stress Relaxation
title_sort manufacturing process simulation of toughened cyanate ester based composite structures with respect to stress relaxation
topic composite materials
cyanate ester
toughening
high-temperature application
process-induced deformation/stress
viscoelastic
url https://www.mdpi.com/1996-1944/15/19/6675
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