Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
Abstract It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all 13C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with appl...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Wiley-VCH
2019-08-01
|
| Series: | ChemistryOpen |
| Subjects: | |
| Online Access: | https://doi.org/10.1002/open.201900136 |
| _version_ | 1818454414448394240 |
|---|---|
| author | Tamás Gyöngyösi Prof. Dr. Katalin E. Kövér Dr. Ole W. Sørensen |
| author_facet | Tamás Gyöngyösi Prof. Dr. Katalin E. Kövér Dr. Ole W. Sørensen |
| author_sort | Tamás Gyöngyösi |
| collection | DOAJ |
| description | Abstract It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all 13C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with applications to ibuprofen and strychnine. |
| first_indexed | 2024-12-14T21:54:30Z |
| format | Article |
| id | doaj.art-60bba7bdd50d40938a799d0f9b3c7be1 |
| institution | Directory Open Access Journal |
| issn | 2191-1363 |
| language | English |
| last_indexed | 2024-12-14T21:54:30Z |
| publishDate | 2019-08-01 |
| publisher | Wiley-VCH |
| record_format | Article |
| series | ChemistryOpen |
| spelling | doaj.art-60bba7bdd50d40938a799d0f9b3c7be12022-12-21T22:46:10ZengWiley-VCHChemistryOpen2191-13632019-08-01881048105110.1002/open.201900136Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range CorrelationTamás Gyöngyösi0Prof. Dr. Katalin E. Kövér1Dr. Ole W. Sørensen2Department of Inorganic and Analytical Chemistry University of Debrecen Egyetem tér 1 H-4032 Debrecen HungaryDepartment of Inorganic and Analytical Chemistry University of Debrecen Egyetem tér 1 H-4032 Debrecen HungaryCopenhagen DenmarkAbstract It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all 13C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with applications to ibuprofen and strychnine.https://doi.org/10.1002/open.201900136NMR spectroscopylong-range correlationabsorptive profilesresolution enhancement |
| spellingShingle | Tamás Gyöngyösi Prof. Dr. Katalin E. Kövér Dr. Ole W. Sørensen Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation ChemistryOpen NMR spectroscopy long-range correlation absorptive profiles resolution enhancement |
| title | Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation |
| title_full | Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation |
| title_fullStr | Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation |
| title_full_unstemmed | Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation |
| title_short | Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation |
| title_sort | resolution enhancement in sea xloc for heteronuclear nmr long range correlation |
| topic | NMR spectroscopy long-range correlation absorptive profiles resolution enhancement |
| url | https://doi.org/10.1002/open.201900136 |
| work_keys_str_mv | AT tamasgyongyosi resolutionenhancementinseaxlocforheteronuclearnmrlongrangecorrelation AT profdrkatalinekover resolutionenhancementinseaxlocforheteronuclearnmrlongrangecorrelation AT drolewsørensen resolutionenhancementinseaxlocforheteronuclearnmrlongrangecorrelation |