Effect of Heat Treatment on Microstructure, Tensile Properties and High-Temperature Corrosion Resistance of the FeCrMnNi High Entropy Alloy

FeCrMnNi high-entropy alloys prepared by vacuum induction melting were tested and characterized using an X-ray diffractometer, a scanning electron microscope, a micro hardness tester and a universal tensile tester to investigate the effects of the heat treatment temperature on the microstructure and...

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Bibliographic Details
Main Authors: Zhen Cai, Na Wei, Yaolei Han, Fang Si, Lei Mi, Chenhui Zhang, Xiaohua Liu, Fengyang Jiang, Tiandong Wu
Format: Article
Language:English
Published: MDPI AG 2022-09-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/12/9/1537
Description
Summary:FeCrMnNi high-entropy alloys prepared by vacuum induction melting were tested and characterized using an X-ray diffractometer, a scanning electron microscope, a micro hardness tester and a universal tensile tester to investigate the effects of the heat treatment temperature on the microstructure and mechanical properties of the alloys and the heat-resistant corrosion properties of FeCrMnNi alloy after annealing at 800 °C. It is a high-entropy alloy with a typical dendritic (DR) morphology. With the increase in the heat-treatment temperature, the amount of ultrafine precipitates with the BCC structure in the matrix increased; furthermore, the amount of ultrafine precipitates started to decrease at temperatures above 900 °C, and the DR structure gradually weakened. After heat treatment at temperatures above 800 °C, the alloy showed a tensile strength of 721.1 MPa and an elongation at break of 26.7%, which indicates improved strength of the alloy while maintaining good plasticity, mainly because a large amount of nanoscale particles precipitated between the DR structures and enabled fine grain strengthening. Therefore, an appropriate heat-treatment temperature helps to improve the overall mechanical properties of the high-entropy alloy.
ISSN:2075-4701