Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis

Nickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of pol...

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Main Authors: V. Helan, J. Joseph Prince, Naif Abdullah Al-Dhabi, Mariadhas Valan Arasu, A. Ayeshamariam, G. Madhumitha, Selvaraj Mohana Roopan, M. Jayachandran
Format: Article
Language:English
Published: Elsevier 2016-01-01
Series:Results in Physics
Online Access:http://www.sciencedirect.com/science/article/pii/S2211379716302455
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author V. Helan
J. Joseph Prince
Naif Abdullah Al-Dhabi
Mariadhas Valan Arasu
A. Ayeshamariam
G. Madhumitha
Selvaraj Mohana Roopan
M. Jayachandran
author_facet V. Helan
J. Joseph Prince
Naif Abdullah Al-Dhabi
Mariadhas Valan Arasu
A. Ayeshamariam
G. Madhumitha
Selvaraj Mohana Roopan
M. Jayachandran
author_sort V. Helan
collection DOAJ
description Nickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of polycrystalline nature of samples (0 1 0), (0 1 1) and (0 1 2) with hexagonal crystal phase. Morphological studies using Transmission Electron Microscope (TEM) reveals that the biosynthesized NiO NPs were in shape of oblong with 12 nm in size. Elemental analysis (EDAX) confirms the quantity of Ni is present at 51% and remaining O as 49% as well as the mass magnetization values of 61 emu/g are also recorded for NiO NPs and its coercivity values in the range of 0.2–0.4 of nanoparticles respectively. Finally the NiO NPs was studied for bacterial activity against Staphylococcus aureus (MTCC 1430) and followed by Escherichia coli (MTCC 739) by agar diffusion assay. Keywords: Neem seed, NiO NPs, Coercivity, Magnetic properties, Bacterial activities
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spelling doaj.art-615387c65f514899b7d9b3f8de27f14e2022-12-22T02:05:05ZengElsevierResults in Physics2211-37972016-01-016712718Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysisV. Helan0J. Joseph Prince1Naif Abdullah Al-Dhabi2Mariadhas Valan Arasu3A. Ayeshamariam4G. Madhumitha5Selvaraj Mohana Roopan6M. Jayachandran7Research and Development Centre, BIT Campus, Anna University of Technology, Tiruchirappalli 623024, IndiaResearch and Development Centre, BIT Campus, Anna University of Technology, Tiruchirappalli 623024, India; Corresponding authors.Department of Botany and Microbiology, Addiriyah Chair for Environmental Studies, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi ArabiaDepartment of Botany and Microbiology, Addiriyah Chair for Environmental Studies, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi ArabiaDepartment of Physics, Khadir Mohideen College, Adirampattinam 614701, India; Corresponding authors.Chemistry of Heterocycles and Natural Product Research Laboratory, Department of Chemistry, School of Advanced Sciences, VIT University, Vellore 632014, Tamil Nadu, IndiaChemistry of Heterocycles and Natural Product Research Laboratory, Department of Chemistry, School of Advanced Sciences, VIT University, Vellore 632014, Tamil Nadu, India; Corresponding authors.Department of Physics, Sree Sevugan Annamalai College, Devakottai, 630303, IndiaNickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of polycrystalline nature of samples (0 1 0), (0 1 1) and (0 1 2) with hexagonal crystal phase. Morphological studies using Transmission Electron Microscope (TEM) reveals that the biosynthesized NiO NPs were in shape of oblong with 12 nm in size. Elemental analysis (EDAX) confirms the quantity of Ni is present at 51% and remaining O as 49% as well as the mass magnetization values of 61 emu/g are also recorded for NiO NPs and its coercivity values in the range of 0.2–0.4 of nanoparticles respectively. Finally the NiO NPs was studied for bacterial activity against Staphylococcus aureus (MTCC 1430) and followed by Escherichia coli (MTCC 739) by agar diffusion assay. Keywords: Neem seed, NiO NPs, Coercivity, Magnetic properties, Bacterial activitieshttp://www.sciencedirect.com/science/article/pii/S2211379716302455
spellingShingle V. Helan
J. Joseph Prince
Naif Abdullah Al-Dhabi
Mariadhas Valan Arasu
A. Ayeshamariam
G. Madhumitha
Selvaraj Mohana Roopan
M. Jayachandran
Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
Results in Physics
title Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
title_full Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
title_fullStr Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
title_full_unstemmed Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
title_short Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
title_sort neem leaves mediated preparation of nio nanoparticles and its magnetization coercivity and antibacterial analysis
url http://www.sciencedirect.com/science/article/pii/S2211379716302455
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