Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis
Nickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of pol...
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Elsevier
2016-01-01
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Series: | Results in Physics |
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author | V. Helan J. Joseph Prince Naif Abdullah Al-Dhabi Mariadhas Valan Arasu A. Ayeshamariam G. Madhumitha Selvaraj Mohana Roopan M. Jayachandran |
author_facet | V. Helan J. Joseph Prince Naif Abdullah Al-Dhabi Mariadhas Valan Arasu A. Ayeshamariam G. Madhumitha Selvaraj Mohana Roopan M. Jayachandran |
author_sort | V. Helan |
collection | DOAJ |
description | Nickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of polycrystalline nature of samples (0 1 0), (0 1 1) and (0 1 2) with hexagonal crystal phase. Morphological studies using Transmission Electron Microscope (TEM) reveals that the biosynthesized NiO NPs were in shape of oblong with 12 nm in size. Elemental analysis (EDAX) confirms the quantity of Ni is present at 51% and remaining O as 49% as well as the mass magnetization values of 61 emu/g are also recorded for NiO NPs and its coercivity values in the range of 0.2–0.4 of nanoparticles respectively. Finally the NiO NPs was studied for bacterial activity against Staphylococcus aureus (MTCC 1430) and followed by Escherichia coli (MTCC 739) by agar diffusion assay. Keywords: Neem seed, NiO NPs, Coercivity, Magnetic properties, Bacterial activities |
first_indexed | 2024-04-14T07:54:49Z |
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institution | Directory Open Access Journal |
issn | 2211-3797 |
language | English |
last_indexed | 2024-04-14T07:54:49Z |
publishDate | 2016-01-01 |
publisher | Elsevier |
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series | Results in Physics |
spelling | doaj.art-615387c65f514899b7d9b3f8de27f14e2022-12-22T02:05:05ZengElsevierResults in Physics2211-37972016-01-016712718Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysisV. Helan0J. Joseph Prince1Naif Abdullah Al-Dhabi2Mariadhas Valan Arasu3A. Ayeshamariam4G. Madhumitha5Selvaraj Mohana Roopan6M. Jayachandran7Research and Development Centre, BIT Campus, Anna University of Technology, Tiruchirappalli 623024, IndiaResearch and Development Centre, BIT Campus, Anna University of Technology, Tiruchirappalli 623024, India; Corresponding authors.Department of Botany and Microbiology, Addiriyah Chair for Environmental Studies, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi ArabiaDepartment of Botany and Microbiology, Addiriyah Chair for Environmental Studies, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi ArabiaDepartment of Physics, Khadir Mohideen College, Adirampattinam 614701, India; Corresponding authors.Chemistry of Heterocycles and Natural Product Research Laboratory, Department of Chemistry, School of Advanced Sciences, VIT University, Vellore 632014, Tamil Nadu, IndiaChemistry of Heterocycles and Natural Product Research Laboratory, Department of Chemistry, School of Advanced Sciences, VIT University, Vellore 632014, Tamil Nadu, India; Corresponding authors.Department of Physics, Sree Sevugan Annamalai College, Devakottai, 630303, IndiaNickel oxides nanoparticles (NiO NPs) were synthesized by biosynthesis method with the help of phytoconstituents present in the neem leaf. Further the synthesized NiO NPs were subjected for structural, optical, morphological and magnetic properties. The XRD patterns clearly infer the presence of polycrystalline nature of samples (0 1 0), (0 1 1) and (0 1 2) with hexagonal crystal phase. Morphological studies using Transmission Electron Microscope (TEM) reveals that the biosynthesized NiO NPs were in shape of oblong with 12 nm in size. Elemental analysis (EDAX) confirms the quantity of Ni is present at 51% and remaining O as 49% as well as the mass magnetization values of 61 emu/g are also recorded for NiO NPs and its coercivity values in the range of 0.2–0.4 of nanoparticles respectively. Finally the NiO NPs was studied for bacterial activity against Staphylococcus aureus (MTCC 1430) and followed by Escherichia coli (MTCC 739) by agar diffusion assay. Keywords: Neem seed, NiO NPs, Coercivity, Magnetic properties, Bacterial activitieshttp://www.sciencedirect.com/science/article/pii/S2211379716302455 |
spellingShingle | V. Helan J. Joseph Prince Naif Abdullah Al-Dhabi Mariadhas Valan Arasu A. Ayeshamariam G. Madhumitha Selvaraj Mohana Roopan M. Jayachandran Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis Results in Physics |
title | Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis |
title_full | Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis |
title_fullStr | Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis |
title_full_unstemmed | Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis |
title_short | Neem leaves mediated preparation of NiO nanoparticles and its magnetization, coercivity and antibacterial analysis |
title_sort | neem leaves mediated preparation of nio nanoparticles and its magnetization coercivity and antibacterial analysis |
url | http://www.sciencedirect.com/science/article/pii/S2211379716302455 |
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