Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method
Plate-like single-crystalline BaBi4Ti4[Formula: see text] particles were synthesized by the molten salt synthesis (MSS) method. The effects of sintering temperature, holding time, and NaCl–KCl molten salt content on the phase structure and morphology of plate-like BaBi4-Ti4[Formula: see text] partic...
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| Format: | Article |
| Language: | English |
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World Scientific Publishing
2023-04-01
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| Series: | Journal of Advanced Dielectrics |
| Subjects: | |
| Online Access: | https://www.worldscientific.com/doi/10.1142/S2010135X22500229 |
| _version_ | 1797832971724521472 |
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| author | Xiaoying Feng Bei Xu Xiaoyu Xu Penghui Chen Zhuozhao Wu Duo Teng Jie Xu Feng Gao |
| author_facet | Xiaoying Feng Bei Xu Xiaoyu Xu Penghui Chen Zhuozhao Wu Duo Teng Jie Xu Feng Gao |
| author_sort | Xiaoying Feng |
| collection | DOAJ |
| description | Plate-like single-crystalline BaBi4Ti4[Formula: see text] particles were synthesized by the molten salt synthesis (MSS) method. The effects of sintering temperature, holding time, and NaCl–KCl molten salt content on the phase structure and morphology of plate-like BaBi4-Ti4[Formula: see text] particles were investigated. The results show that plate-like BaBi4Ti4[Formula: see text] particles can be synthesized when the sintering temperature is above 800[Formula: see text]C. The size of particles increases with increasing sintering temperature and molten salt content. Largely anisotropic plate-like BaBi4Ti4[Formula: see text] particles with diameter [Formula: see text]10[Formula: see text]m and thickness of [Formula: see text]0.3 [Formula: see text]m can be obtained under the optimum process parameters. The crystal structure of BaBi4Ti4[Formula: see text] was determined as A21am by TEM, which should be attributed to the Bi[Formula: see text] and Ba[Formula: see text] diffusing into [TiO6] octahedrons. |
| first_indexed | 2024-04-09T14:17:20Z |
| format | Article |
| id | doaj.art-617bd9a7481e42e3ab559cf43dd2f32a |
| institution | Directory Open Access Journal |
| issn | 2010-135X 2010-1368 |
| language | English |
| last_indexed | 2024-04-09T14:17:20Z |
| publishDate | 2023-04-01 |
| publisher | World Scientific Publishing |
| record_format | Article |
| series | Journal of Advanced Dielectrics |
| spelling | doaj.art-617bd9a7481e42e3ab559cf43dd2f32a2023-05-05T06:34:35ZengWorld Scientific PublishingJournal of Advanced Dielectrics2010-135X2010-13682023-04-01130210.1142/S2010135X22500229Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis methodXiaoying Feng0Bei Xu1Xiaoyu Xu2Penghui Chen3Zhuozhao Wu4Duo Teng5Jie Xu6Feng Gao7State Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaState Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaState Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaState Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaQueen Mary University of London Engineering School, Northwestern Polytechnical University, Xi’ an 710072, P. R. ChinaSchool of Marine Science and Technology, Northwestern Polytechnical University, Xi’ an 710072, P. R. ChinaState Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaState Key Laboratory of Solidification Processing, MIIT Key Laboratory of Radiation Detection, Materials and Devices, USI Institute of Intelligence Materials and Structure, NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, P. R. ChinaPlate-like single-crystalline BaBi4Ti4[Formula: see text] particles were synthesized by the molten salt synthesis (MSS) method. The effects of sintering temperature, holding time, and NaCl–KCl molten salt content on the phase structure and morphology of plate-like BaBi4-Ti4[Formula: see text] particles were investigated. The results show that plate-like BaBi4Ti4[Formula: see text] particles can be synthesized when the sintering temperature is above 800[Formula: see text]C. The size of particles increases with increasing sintering temperature and molten salt content. Largely anisotropic plate-like BaBi4Ti4[Formula: see text] particles with diameter [Formula: see text]10[Formula: see text]m and thickness of [Formula: see text]0.3 [Formula: see text]m can be obtained under the optimum process parameters. The crystal structure of BaBi4Ti4[Formula: see text] was determined as A21am by TEM, which should be attributed to the Bi[Formula: see text] and Ba[Formula: see text] diffusing into [TiO6] octahedrons.https://www.worldscientific.com/doi/10.1142/S2010135X22500229Molten salt synthesis methodcalcining conditionsalts contentmicroplateletsanisotropy |
| spellingShingle | Xiaoying Feng Bei Xu Xiaoyu Xu Penghui Chen Zhuozhao Wu Duo Teng Jie Xu Feng Gao Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method Journal of Advanced Dielectrics Molten salt synthesis method calcining condition salts content microplatelets anisotropy |
| title | Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method |
| title_full | Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method |
| title_fullStr | Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method |
| title_full_unstemmed | Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method |
| title_short | Fabrication plate-like BaBi4Ti4 single-crystalline particles by the molten salt synthesis method |
| title_sort | fabrication plate like babi4ti4 single crystalline particles by the molten salt synthesis method |
| topic | Molten salt synthesis method calcining condition salts content microplatelets anisotropy |
| url | https://www.worldscientific.com/doi/10.1142/S2010135X22500229 |
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