The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process
Among the recently developed compositions tailored for the power bed fusion-laser beam process (PBF-LB), the novel Al-Mn-Cr-Zr alloy stands out. This composition exploits high solid solution strengthening, achieving a high hardness value in the as-built condition. The produced samples are inherently...
Main Authors: | , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
MDPI AG
2022-08-01
|
Series: | Metals |
Subjects: | |
Online Access: | https://www.mdpi.com/2075-4701/12/8/1387 |
_version_ | 1797408847247179776 |
---|---|
author | Alessandra Martucci Bharat Mehta Mariangela Lombardi Lars Nyborg |
author_facet | Alessandra Martucci Bharat Mehta Mariangela Lombardi Lars Nyborg |
author_sort | Alessandra Martucci |
collection | DOAJ |
description | Among the recently developed compositions tailored for the power bed fusion-laser beam process (PBF-LB), the novel Al-Mn-Cr-Zr alloy stands out. This composition exploits high solid solution strengthening, achieving a high hardness value in the as-built condition. The produced samples are inherently crack-free and have a good level of densification (~99.5%). The goal of this study is to investigate how this quaternary system is affected by the laser power while retaining a similar volumetric energy density. A comparison between the microstructural features and the mechanical performance was performed on a set of samples processed with power values ranging from 100 to 170 W. Microstructural features were investigated through optical microscopy, Electron Back Scattered Diffraction (EBSD) investigation and feature analysis using advanced microscopy to examine the amount, distribution, and shape of precipitates in the different process conditions. Although the quantitative feature analysis permitted analysis of more than 60 k precipitates for each power condition, all samples demonstrated a low level of precipitation (below 0.3%) with nanometric size (around 75 nm). The mechanical performances of this quaternary system as a function of the laser power value were evaluated with a microhardness test, recording very similar values for the different process conditions with a mean value of approximately 104 HV. The results suggested a very stable system over the tested range of process parameters. In addition, considering the low level of precipitation of nanometric phases enriched in Al-Mn, a supersaturated state could be established in each process condition. |
first_indexed | 2024-03-09T04:05:29Z |
format | Article |
id | doaj.art-631f2c8a0e5a4aeab54ea86833741047 |
institution | Directory Open Access Journal |
issn | 2075-4701 |
language | English |
last_indexed | 2024-03-09T04:05:29Z |
publishDate | 2022-08-01 |
publisher | MDPI AG |
record_format | Article |
series | Metals |
spelling | doaj.art-631f2c8a0e5a4aeab54ea868337410472023-12-03T14:07:24ZengMDPI AGMetals2075-47012022-08-01128138710.3390/met12081387The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam ProcessAlessandra Martucci0Bharat Mehta1Mariangela Lombardi2Lars Nyborg3Department of Applied Science and Technology, Politecnico di Torino, 10129 Turin, ItalyDepartment of Industrial and Materials Science, Chalmers University of Technology, 412 96 Gothenburg, SwedenDepartment of Applied Science and Technology, Politecnico di Torino, 10129 Turin, ItalyDepartment of Industrial and Materials Science, Chalmers University of Technology, 412 96 Gothenburg, SwedenAmong the recently developed compositions tailored for the power bed fusion-laser beam process (PBF-LB), the novel Al-Mn-Cr-Zr alloy stands out. This composition exploits high solid solution strengthening, achieving a high hardness value in the as-built condition. The produced samples are inherently crack-free and have a good level of densification (~99.5%). The goal of this study is to investigate how this quaternary system is affected by the laser power while retaining a similar volumetric energy density. A comparison between the microstructural features and the mechanical performance was performed on a set of samples processed with power values ranging from 100 to 170 W. Microstructural features were investigated through optical microscopy, Electron Back Scattered Diffraction (EBSD) investigation and feature analysis using advanced microscopy to examine the amount, distribution, and shape of precipitates in the different process conditions. Although the quantitative feature analysis permitted analysis of more than 60 k precipitates for each power condition, all samples demonstrated a low level of precipitation (below 0.3%) with nanometric size (around 75 nm). The mechanical performances of this quaternary system as a function of the laser power value were evaluated with a microhardness test, recording very similar values for the different process conditions with a mean value of approximately 104 HV. The results suggested a very stable system over the tested range of process parameters. In addition, considering the low level of precipitation of nanometric phases enriched in Al-Mn, a supersaturated state could be established in each process condition.https://www.mdpi.com/2075-4701/12/8/1387PBF-LBAl-Mn-Cr-ZrAl-based alloysfeature analysisAl-Mn precipitates |
spellingShingle | Alessandra Martucci Bharat Mehta Mariangela Lombardi Lars Nyborg The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process Metals PBF-LB Al-Mn-Cr-Zr Al-based alloys feature analysis Al-Mn precipitates |
title | The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process |
title_full | The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process |
title_fullStr | The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process |
title_full_unstemmed | The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process |
title_short | The Influence of Processing Parameters on the Al-Mn Enriched Nano-Precipitates Formation in a Novel Al-Mn-Cr-Zr Alloy Tailored for Power Bed Fusion-Laser Beam Process |
title_sort | influence of processing parameters on the al mn enriched nano precipitates formation in a novel al mn cr zr alloy tailored for power bed fusion laser beam process |
topic | PBF-LB Al-Mn-Cr-Zr Al-based alloys feature analysis Al-Mn precipitates |
url | https://www.mdpi.com/2075-4701/12/8/1387 |
work_keys_str_mv | AT alessandramartucci theinfluenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT bharatmehta theinfluenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT mariangelalombardi theinfluenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT larsnyborg theinfluenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT alessandramartucci influenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT bharatmehta influenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT mariangelalombardi influenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess AT larsnyborg influenceofprocessingparametersonthealmnenrichednanoprecipitatesformationinanovelalmncrzralloytailoredforpowerbedfusionlaserbeamprocess |