Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process

The current study focuses on an alternative strategy for producing nanoparticles (NPs) using one-step electrochemical discharge process (ECDP) in different electrolyte mediums. Current and plasma discharge effects on morphology and mass output rate were examined in detail. FE-SEM and TEM results sho...

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Main Authors: Harish Bishwakarma, Alok Kumar Das, Pankaj Kumar, Purushottam Kumar Singh, Mohamed M. Awad
Format: Article
Language:English
Published: Taylor & Francis Group 2023-12-01
Series:Journal of Taibah University for Science
Subjects:
Online Access:https://www.tandfonline.com/doi/10.1080/16583655.2023.2188017
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author Harish Bishwakarma
Alok Kumar Das
Pankaj Kumar
Purushottam Kumar Singh
Mohamed M. Awad
author_facet Harish Bishwakarma
Alok Kumar Das
Pankaj Kumar
Purushottam Kumar Singh
Mohamed M. Awad
author_sort Harish Bishwakarma
collection DOAJ
description The current study focuses on an alternative strategy for producing nanoparticles (NPs) using one-step electrochemical discharge process (ECDP) in different electrolyte mediums. Current and plasma discharge effects on morphology and mass output rate were examined in detail. FE-SEM and TEM results show dimensional control materials such as rod, flower and rice shapes are produced. The XRD, EDS, UV-vis and Raman characterization techniques confirm the formation of CuO-ZnO NPs with different morphology. The use of two semiconductors (n-type ZnO and p-type CuO) in combination have two different band energies may boost electrochemical performance. From the electrochemical study, the flower-shaped structure has high specific capacity (313 F/g at 2 A/g current density), with 84.1% retention capacitance after 5000 cycles. This study allows us to study the discharge-based composite formation, which could be used in supercapacitors.
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spelling doaj.art-6332580974694a479df6dadb0b3a328a2024-04-10T20:17:48ZengTaylor & Francis GroupJournal of Taibah University for Science1658-36552023-12-0117110.1080/16583655.2023.2188017Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge processHarish Bishwakarma0Alok Kumar Das1Pankaj Kumar2Purushottam Kumar Singh3Mohamed M. Awad4Advanced Manufacturing Laboratory, IIT (ISM), Dhanbad, Jharkhand, IndiaAdvanced Manufacturing Laboratory, IIT (ISM), Dhanbad, Jharkhand, IndiaCenter for Materials and Manufacturing, Department of Mechanical Engineering, SR University, Warangal, Telangana, IndiaMechanical Engineering Department, NIT Silchar, Silchar, Assam, IndiaMechanical Power Engineering Department, Faculty of Engineering, Mansoura University, Mansoura, EgyptThe current study focuses on an alternative strategy for producing nanoparticles (NPs) using one-step electrochemical discharge process (ECDP) in different electrolyte mediums. Current and plasma discharge effects on morphology and mass output rate were examined in detail. FE-SEM and TEM results show dimensional control materials such as rod, flower and rice shapes are produced. The XRD, EDS, UV-vis and Raman characterization techniques confirm the formation of CuO-ZnO NPs with different morphology. The use of two semiconductors (n-type ZnO and p-type CuO) in combination have two different band energies may boost electrochemical performance. From the electrochemical study, the flower-shaped structure has high specific capacity (313 F/g at 2 A/g current density), with 84.1% retention capacitance after 5000 cycles. This study allows us to study the discharge-based composite formation, which could be used in supercapacitors.https://www.tandfonline.com/doi/10.1080/16583655.2023.2188017CuO-ZnOdimensional structureECDPflower shapesupercapacitor
spellingShingle Harish Bishwakarma
Alok Kumar Das
Pankaj Kumar
Purushottam Kumar Singh
Mohamed M. Awad
Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
Journal of Taibah University for Science
CuO-ZnO
dimensional structure
ECDP
flower shape
supercapacitor
title Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
title_full Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
title_fullStr Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
title_full_unstemmed Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
title_short Structure and electrochemical properties of CuO-ZnO nanocomposite produced by the one-step novel discharge process
title_sort structure and electrochemical properties of cuo zno nanocomposite produced by the one step novel discharge process
topic CuO-ZnO
dimensional structure
ECDP
flower shape
supercapacitor
url https://www.tandfonline.com/doi/10.1080/16583655.2023.2188017
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