The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent

Titanium is a key biomedical material due its good biocompatibility, mechanical properties and corrosion stability, but infections of the implantation site still pose serious threat. One approach to prevent infection is to improve antimicrobial ability of the coating material. Silver doped hydro...

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Main Authors: Mišković-Stanković Vesna, Janaćković Đorđe, Stevanović Tatjana, Veljović Đorđe, Dindune Antonija, Eraković Sanja, Janković Ana
Format: Article
Language:English
Published: Serbian Chemical Society 2012-01-01
Series:Journal of the Serbian Chemical Society
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/0352-5139/2012/0352-51391200086J.pdf
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author Mišković-Stanković Vesna
Janaćković Đorđe
Stevanović Tatjana
Veljović Đorđe
Dindune Antonija
Eraković Sanja
Janković Ana
author_facet Mišković-Stanković Vesna
Janaćković Đorđe
Stevanović Tatjana
Veljović Đorđe
Dindune Antonija
Eraković Sanja
Janković Ana
author_sort Mišković-Stanković Vesna
collection DOAJ
description Titanium is a key biomedical material due its good biocompatibility, mechanical properties and corrosion stability, but infections of the implantation site still pose serious threat. One approach to prevent infection is to improve antimicrobial ability of the coating material. Silver doped hydroxyapatite (Ag/HAP) nanoparticles were synthesized by new modified precipitation method. The synthesized powder was used for preparation of Ag/HAP coating on titanium by electrophoretic deposition. The coating was characterized in terms of phase composition and structure by Attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) and X-ray diffraction (XRD); surface morphology and chemical composition was assessed using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). Research focused on evaluation of the corrosion behaviour of Ag/HAP coating in simulated body fluid (SBF) at 37 ºC during prolonged immersion time by electrochemical impedance spectroscopy (EIS). Silver doped HAP coating provided good corrosion protection in SBF solution. [Acknowledgements. This research was financed by the Ministry of Education, Science and Technological Development of the Republic of Serbia, contracts No. III 45019 and by National Sciences and Engineering Research Council of Canada (NSERC). Dr Ana Jankovic was financed by the FP7 Nanotech FTM Grant Agreement 245916]
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spelling doaj.art-6364de3690ca40e5a143888a8f9c94032022-12-21T21:03:41ZengSerbian Chemical SocietyJournal of the Serbian Chemical Society0352-51392012-01-0177111609162310.2298/JSC120712086JThe electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agentMišković-Stanković VesnaJanaćković ĐorđeStevanović TatjanaVeljović ĐorđeDindune AntonijaEraković SanjaJanković AnaTitanium is a key biomedical material due its good biocompatibility, mechanical properties and corrosion stability, but infections of the implantation site still pose serious threat. One approach to prevent infection is to improve antimicrobial ability of the coating material. Silver doped hydroxyapatite (Ag/HAP) nanoparticles were synthesized by new modified precipitation method. The synthesized powder was used for preparation of Ag/HAP coating on titanium by electrophoretic deposition. The coating was characterized in terms of phase composition and structure by Attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) and X-ray diffraction (XRD); surface morphology and chemical composition was assessed using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). Research focused on evaluation of the corrosion behaviour of Ag/HAP coating in simulated body fluid (SBF) at 37 ºC during prolonged immersion time by electrochemical impedance spectroscopy (EIS). Silver doped HAP coating provided good corrosion protection in SBF solution. [Acknowledgements. This research was financed by the Ministry of Education, Science and Technological Development of the Republic of Serbia, contracts No. III 45019 and by National Sciences and Engineering Research Council of Canada (NSERC). Dr Ana Jankovic was financed by the FP7 Nanotech FTM Grant Agreement 245916]http://www.doiserbia.nb.rs/img/doi/0352-5139/2012/0352-51391200086J.pdfelectrochemical impedancehydroxyapatitesilverelectrophoretic depositionsimulated body fluid
spellingShingle Mišković-Stanković Vesna
Janaćković Đorđe
Stevanović Tatjana
Veljović Đorđe
Dindune Antonija
Eraković Sanja
Janković Ana
The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
Journal of the Serbian Chemical Society
electrochemical impedance
hydroxyapatite
silver
electrophoretic deposition
simulated body fluid
title The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
title_full The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
title_fullStr The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
title_full_unstemmed The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
title_short The electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
title_sort electrochemical impedance spectroscopy of silver doped hydroxyapatite coating in simulated body fluid used as corrosive agent
topic electrochemical impedance
hydroxyapatite
silver
electrophoretic deposition
simulated body fluid
url http://www.doiserbia.nb.rs/img/doi/0352-5139/2012/0352-51391200086J.pdf
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