Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)

Flower-like AuPtPd-Fe3O4 new nanohybrid prepared through a scalable synthetic approach was tested for the effective and simultaneous removal of Humic Acids and Cr (VI). Field emission scanning electron microscopy (FESEM) equipped with an energy dispersive X-ray (EDX) probe, X-ray diffractometer (XRD...

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Main Authors: Maria Sarno, Carmela Scudieri, Eleonora Ponticorvo
Format: Article
Language:English
Published: AIDIC Servizi S.r.l. 2019-04-01
Series:Chemical Engineering Transactions
Online Access:https://www.cetjournal.it/index.php/cet/article/view/9649
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author Maria Sarno
Carmela Scudieri
Eleonora Ponticorvo
author_facet Maria Sarno
Carmela Scudieri
Eleonora Ponticorvo
author_sort Maria Sarno
collection DOAJ
description Flower-like AuPtPd-Fe3O4 new nanohybrid prepared through a scalable synthetic approach was tested for the effective and simultaneous removal of Humic Acids and Cr (VI). Field emission scanning electron microscopy (FESEM) equipped with an energy dispersive X-ray (EDX) probe, X-ray diffractometer (XRD) and thermogravimetric analysis (TG-DTG) were used for characterization. The nanocatalyst, at the end of the preparation process, results dispersible in water. Calibration equations were plotted for the removal evaluation of Cr(VI) and Humic Acids in water samples. Electrochemical tests were carried out at pH 3.0 and 30 mA. Humic Acids were highly mineralized with TOC removal efficiency of 95%. In 3 h, 99 % of total Cr was removed.
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spelling doaj.art-636ed037c8d649cab3d4726bad3ab9e32022-12-21T22:49:38ZengAIDIC Servizi S.r.l.Chemical Engineering Transactions2283-92162019-04-017310.3303/CET1973039Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)Maria SarnoCarmela ScudieriEleonora PonticorvoFlower-like AuPtPd-Fe3O4 new nanohybrid prepared through a scalable synthetic approach was tested for the effective and simultaneous removal of Humic Acids and Cr (VI). Field emission scanning electron microscopy (FESEM) equipped with an energy dispersive X-ray (EDX) probe, X-ray diffractometer (XRD) and thermogravimetric analysis (TG-DTG) were used for characterization. The nanocatalyst, at the end of the preparation process, results dispersible in water. Calibration equations were plotted for the removal evaluation of Cr(VI) and Humic Acids in water samples. Electrochemical tests were carried out at pH 3.0 and 30 mA. Humic Acids were highly mineralized with TOC removal efficiency of 95%. In 3 h, 99 % of total Cr was removed.https://www.cetjournal.it/index.php/cet/article/view/9649
spellingShingle Maria Sarno
Carmela Scudieri
Eleonora Ponticorvo
Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
Chemical Engineering Transactions
title Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
title_full Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
title_fullStr Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
title_full_unstemmed Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
title_short Flower-like Auptpd-fe3o4 Nanocatalyst for Electrochemical Removal of Humic Acids and Cr(vi)
title_sort flower like auptpd fe3o4 nanocatalyst for electrochemical removal of humic acids and cr vi
url https://www.cetjournal.it/index.php/cet/article/view/9649
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AT eleonoraponticorvo flowerlikeauptpdfe3o4nanocatalystforelectrochemicalremovalofhumicacidsandcrvi