Electrochemical synthesis of urania coin-like nanoparticles in aqueous media

Urania nanostructures were synthesized by a facile, which is a simple and clean and straightforward deposition method, for two different deposition time durations. The morphology and structures of the products were characterized by the X-ray diffraction analysis (XRD) and Scanning Electronic Microsc...

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Main Authors: T Yousefi, R Yavari, M Ghannadi Maragheh, S.J Ahmadi, H Malek Mohammad, A Gharib, H Ghasemi Mobtaker
Format: Article
Language:fas
Published: Nuclear Science and Technology Research Institute 2020-02-01
Series:مجله علوم و فنون هسته‌ای
Subjects:
Online Access:https://jonsat.nstri.ir/article_1066_e6e6a09005ab60f5a1c3a9e594ec3f24.pdf
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author T Yousefi
R Yavari
M Ghannadi Maragheh
S.J Ahmadi
H Malek Mohammad
A Gharib
H Ghasemi Mobtaker
author_facet T Yousefi
R Yavari
M Ghannadi Maragheh
S.J Ahmadi
H Malek Mohammad
A Gharib
H Ghasemi Mobtaker
author_sort T Yousefi
collection DOAJ
description Urania nanostructures were synthesized by a facile, which is a simple and clean and straightforward deposition method, for two different deposition time durations. The morphology and structures of the products were characterized by the X-ray diffraction analysis (XRD) and Scanning Electronic Microscopy (SEM). The SEM images indicated that the morphology of the synthesized samples for 10 minutes was composed of a coin-like structure with a nano-scale dimension in a narrow- size distribution. The results indicated that the deposition time affects the morphology while it does not affect the structure. The XRD results identified the sample structures as UO2 crystal. The chemical composition of different points of the sample surface was determined by the energy dispersive spectroscopy (EDS) technique and the results clarified that the samples have a homogeneous composition of uranium oxide. The synergistic properties of the substrate surface, and uranium ions are responsible for the formation of an outstanding and a novel structure.
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spelling doaj.art-637dceb221be4009a2256ff038ea5a182023-05-02T10:15:41ZfasNuclear Science and Technology Research Instituteمجله علوم و فنون هسته‌ای1735-18712676-58612020-02-01404212710.24200/nst.2020.10661066Electrochemical synthesis of urania coin-like nanoparticles in aqueous mediaT Yousefi0R Yavari1M Ghannadi Maragheh2S.J Ahmadi3H Malek Mohammad4A Gharib5H Ghasemi Mobtaker61. پژوهشکده‌ی مواد و سوخت هسته‌ای، پژوهشگاه علوم و فنون هسته‌ای، سازمان انرژی اتمی ایران، صندوق پستی: 8486-11365، تهران ـ ایران1. پژوهشکده‌ی مواد و سوخت هسته‌ای، پژوهشگاه علوم و فنون هسته‌ای، سازمان انرژی اتمی ایران، صندوق پستی: 8486-11365، تهران ـ ایران1. پژوهشکده‌ی مواد و سوخت هسته‌ای، پژوهشگاه علوم و فنون هسته‌ای، سازمان انرژی اتمی ایران، صندوق پستی: 8486-11365، تهران ـ ایران1. پژوهشکده‌ی مواد و سوخت هسته‌ای، پژوهشگاه علوم و فنون هسته‌ای، سازمان انرژی اتمی ایران، صندوق پستی: 8486-11365، تهران ـ ایران2. گروه فیزیک و مهندسی انرژی، دانشگاه صنعتی امیرکبیر، صندوق پستی: 1591634311، تهران ـ ایران2. گروه فیزیک و مهندسی انرژی، دانشگاه صنعتی امیرکبیر، صندوق پستی: 1591634311، تهران ـ ایران1. پژوهشکده‌ی مواد و سوخت هسته‌ای، پژوهشگاه علوم و فنون هسته‌ای، سازمان انرژی اتمی ایران، صندوق پستی: 8486-11365، تهران ـ ایرانUrania nanostructures were synthesized by a facile, which is a simple and clean and straightforward deposition method, for two different deposition time durations. The morphology and structures of the products were characterized by the X-ray diffraction analysis (XRD) and Scanning Electronic Microscopy (SEM). The SEM images indicated that the morphology of the synthesized samples for 10 minutes was composed of a coin-like structure with a nano-scale dimension in a narrow- size distribution. The results indicated that the deposition time affects the morphology while it does not affect the structure. The XRD results identified the sample structures as UO2 crystal. The chemical composition of different points of the sample surface was determined by the energy dispersive spectroscopy (EDS) technique and the results clarified that the samples have a homogeneous composition of uranium oxide. The synergistic properties of the substrate surface, and uranium ions are responsible for the formation of an outstanding and a novel structure.https://jonsat.nstri.ir/article_1066_e6e6a09005ab60f5a1c3a9e594ec3f24.pdfcoin- like nanostructureuraniadeposition
spellingShingle T Yousefi
R Yavari
M Ghannadi Maragheh
S.J Ahmadi
H Malek Mohammad
A Gharib
H Ghasemi Mobtaker
Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
مجله علوم و فنون هسته‌ای
coin- like nanostructure
urania
deposition
title Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
title_full Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
title_fullStr Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
title_full_unstemmed Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
title_short Electrochemical synthesis of urania coin-like nanoparticles in aqueous media
title_sort electrochemical synthesis of urania coin like nanoparticles in aqueous media
topic coin- like nanostructure
urania
deposition
url https://jonsat.nstri.ir/article_1066_e6e6a09005ab60f5a1c3a9e594ec3f24.pdf
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AT ryavari electrochemicalsynthesisofuraniacoinlikenanoparticlesinaqueousmedia
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AT sjahmadi electrochemicalsynthesisofuraniacoinlikenanoparticlesinaqueousmedia
AT hmalekmohammad electrochemicalsynthesisofuraniacoinlikenanoparticlesinaqueousmedia
AT agharib electrochemicalsynthesisofuraniacoinlikenanoparticlesinaqueousmedia
AT hghasemimobtaker electrochemicalsynthesisofuraniacoinlikenanoparticlesinaqueousmedia