Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite

Sono-chemical is a fast procedure for preparing monodisperse nanoparticles. Magnetite nanoparticles were prepared via a sono-chemical reaction at a room temperature. Fe3O4 nanostructures were then added to acrylonitrile-butadiene-styrene (ABS) copolymer. Nanocomposites are very attractive due to the...

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Main Authors: Farhad Heidary, Davood Ghanbari
Format: Article
Language:English
Published: Iranian Chemical Society 2021-06-01
Series:Nanochemistry Research
Subjects:
Online Access:http://www.nanochemres.org/article_138041_822acc438b1dc0bf8c4615f805675a06.pdf
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author Farhad Heidary
Davood Ghanbari
author_facet Farhad Heidary
Davood Ghanbari
author_sort Farhad Heidary
collection DOAJ
description Sono-chemical is a fast procedure for preparing monodisperse nanoparticles. Magnetite nanoparticles were prepared via a sono-chemical reaction at a room temperature. Fe3O4 nanostructures were then added to acrylonitrile-butadiene-styrene (ABS) copolymer. Nanocomposites are very attractive due to the fact that small amount of nanostructure can lead to great improvement in many properties, such as mechanical and thermal property. Nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and vibrating sample magnetometer (VSM). The XRD pattern of nanoparticles is indexed as a cubic phase (space group: Fd-3m). Fe3O4 nanostructures exhibit a super paramagnetic behaviour with a saturation magnetization of 54 emu/g and a coercivity of 11 Oe at room temperature. The effect of ultrasonic power on the shape and particle size was investigated and the result showed at 150W by increasing power growth stage overcome to nucleation stage and nanoparticles with bigger diameters were obtained. The flame retardancy behavior of ABS-Fe3O4 was studied by UL-94 analysis.
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spelling doaj.art-644b941b7e2f4850b124567a78217bc92023-02-05T07:27:31ZengIranian Chemical SocietyNanochemistry Research2538-42792423-818X2021-06-016111712110.22036/ncr.2021.01.011138041Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocompositeFarhad Heidary0Davood Ghanbari1Department of Chemistry, Faculty of Science, Arak University, Arak 38156-8-8349, IranDepartment of Science, Arak University of Technology, Arak, IranSono-chemical is a fast procedure for preparing monodisperse nanoparticles. Magnetite nanoparticles were prepared via a sono-chemical reaction at a room temperature. Fe3O4 nanostructures were then added to acrylonitrile-butadiene-styrene (ABS) copolymer. Nanocomposites are very attractive due to the fact that small amount of nanostructure can lead to great improvement in many properties, such as mechanical and thermal property. Nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and vibrating sample magnetometer (VSM). The XRD pattern of nanoparticles is indexed as a cubic phase (space group: Fd-3m). Fe3O4 nanostructures exhibit a super paramagnetic behaviour with a saturation magnetization of 54 emu/g and a coercivity of 11 Oe at room temperature. The effect of ultrasonic power on the shape and particle size was investigated and the result showed at 150W by increasing power growth stage overcome to nucleation stage and nanoparticles with bigger diameters were obtained. The flame retardancy behavior of ABS-Fe3O4 was studied by UL-94 analysis.http://www.nanochemres.org/article_138041_822acc438b1dc0bf8c4615f805675a06.pdfnanoparticlesnanocompositesono-chemicalmagnetite
spellingShingle Farhad Heidary
Davood Ghanbari
Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
Nanochemistry Research
nanoparticles
nanocomposite
sono-chemical
magnetite
title Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
title_full Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
title_fullStr Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
title_full_unstemmed Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
title_short Sono-chemical synthesis of Fe3O4 nanostructures and its application in acrylonitrile-butadiene-styrene polymeric nanocomposite
title_sort sono chemical synthesis of fe3o4 nanostructures and its application in acrylonitrile butadiene styrene polymeric nanocomposite
topic nanoparticles
nanocomposite
sono-chemical
magnetite
url http://www.nanochemres.org/article_138041_822acc438b1dc0bf8c4615f805675a06.pdf
work_keys_str_mv AT farhadheidary sonochemicalsynthesisoffe3o4nanostructuresanditsapplicationinacrylonitrilebutadienestyrenepolymericnanocomposite
AT davoodghanbari sonochemicalsynthesisoffe3o4nanostructuresanditsapplicationinacrylonitrilebutadienestyrenepolymericnanocomposite