Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions

Magnetic nanoparticles (MNPs) of iron oxide (Fe3O4) represent the most promising materials in many applications. MNPs have been synthesized by co-precipitation of ferric and ferrous ions in alkaline solution. Two methods of synthesis were conducted with different parameters, such as temperature (25...

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Main Authors: Ahmed Faiq Al-Alawy, Entisar Eliwi Al-Abodi, Raya Mohammed Kadhim
Format: Article
Language:English
Published: University of Baghdad 2018-10-01
Series:Journal of Engineering
Subjects:
Online Access:http://joe.uobaghdad.edu.iq/index.php/main/article/view/647
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author Ahmed Faiq Al-Alawy
Entisar Eliwi Al-Abodi
Raya Mohammed Kadhim
author_facet Ahmed Faiq Al-Alawy
Entisar Eliwi Al-Abodi
Raya Mohammed Kadhim
author_sort Ahmed Faiq Al-Alawy
collection DOAJ
description Magnetic nanoparticles (MNPs) of iron oxide (Fe3O4) represent the most promising materials in many applications. MNPs have been synthesized by co-precipitation of ferric and ferrous ions in alkaline solution. Two methods of synthesis were conducted with different parameters, such as temperature (25 and 80 ̊C), adding a base to the reactants and the opposite process, and using nitrogen as an inert gas. The product of the first method (MNPs-1) and the second method (MNPs-2) were characterized by x-ray diffractometer (XRD), Zeta Potential, atomic force microscope (AFM) and scanning electron microscope (SEM). AFM results showed convergent particle size of (MNPs-1) and (MNPs-2) with (86.01) and (74.14) nm respectively. Also, the zeta potential values of (MNPs-1) and (MNPs-2) were (2.77) and (-12.48) mV, respectively, which indicates more stability of (MNP-2).
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spelling doaj.art-649ed567d096462aa766ce0c5cd9f5cf2023-09-03T00:07:35ZengUniversity of BaghdadJournal of Engineering1726-40732520-33392018-10-01241010.31026/j.eng.2018.10.05Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different ConditionsAhmed Faiq Al-Alawy0Entisar Eliwi Al-Abodi1Raya Mohammed Kadhim2College of Engineering-University of BaghdadCollege of Education Ibn Al-Haitham-University of BaghdadMinistry of health and environment-Department of International Environment RelationshipsMagnetic nanoparticles (MNPs) of iron oxide (Fe3O4) represent the most promising materials in many applications. MNPs have been synthesized by co-precipitation of ferric and ferrous ions in alkaline solution. Two methods of synthesis were conducted with different parameters, such as temperature (25 and 80 ̊C), adding a base to the reactants and the opposite process, and using nitrogen as an inert gas. The product of the first method (MNPs-1) and the second method (MNPs-2) were characterized by x-ray diffractometer (XRD), Zeta Potential, atomic force microscope (AFM) and scanning electron microscope (SEM). AFM results showed convergent particle size of (MNPs-1) and (MNPs-2) with (86.01) and (74.14) nm respectively. Also, the zeta potential values of (MNPs-1) and (MNPs-2) were (2.77) and (-12.48) mV, respectively, which indicates more stability of (MNP-2).http://joe.uobaghdad.edu.iq/index.php/main/article/view/647magnetic nanoparticles, iron oxide, co-precipitation.
spellingShingle Ahmed Faiq Al-Alawy
Entisar Eliwi Al-Abodi
Raya Mohammed Kadhim
Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
Journal of Engineering
magnetic nanoparticles, iron oxide, co-precipitation.
title Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
title_full Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
title_fullStr Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
title_full_unstemmed Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
title_short Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions
title_sort synthesis and characterization of magnetic iron oxide nanoparticles by co precipitation method at different conditions
topic magnetic nanoparticles, iron oxide, co-precipitation.
url http://joe.uobaghdad.edu.iq/index.php/main/article/view/647
work_keys_str_mv AT ahmedfaiqalalawy synthesisandcharacterizationofmagneticironoxidenanoparticlesbycoprecipitationmethodatdifferentconditions
AT entisareliwialabodi synthesisandcharacterizationofmagneticironoxidenanoparticlesbycoprecipitationmethodatdifferentconditions
AT rayamohammedkadhim synthesisandcharacterizationofmagneticironoxidenanoparticlesbycoprecipitationmethodatdifferentconditions