γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy

In present work, a novel γ′′-strengthened Nb-alloyed medium-entropy alloy (MEA) was successfully fabricated and systematically investigated. Our results evidence that the γ′′ phase brings out significant precipitation hardening effect (∼10.2 %volume fraction contributes ∼ 685 MPa strength enhancemen...

Full description

Bibliographic Details
Main Authors: Wenjie Lu, Xian Luo, Yafeng Wang, Bin Huang, Zhijun Wang, Yanqing Yang
Format: Article
Language:English
Published: Elsevier 2023-01-01
Series:Materials & Design
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0264127522011005
_version_ 1811175478004809728
author Wenjie Lu
Xian Luo
Yafeng Wang
Bin Huang
Zhijun Wang
Yanqing Yang
author_facet Wenjie Lu
Xian Luo
Yafeng Wang
Bin Huang
Zhijun Wang
Yanqing Yang
author_sort Wenjie Lu
collection DOAJ
description In present work, a novel γ′′-strengthened Nb-alloyed medium-entropy alloy (MEA) was successfully fabricated and systematically investigated. Our results evidence that the γ′′ phase brings out significant precipitation hardening effect (∼10.2 %volume fraction contributes ∼ 685 MPa strength enhancement). The metastable γ′′ phase could abnormally transform to ε phase, and the morphology and distribution of ε phase shows great impacts on mechanical properties. A hetero-lamellae grain coupling with dual-precipitation (HLG + dual-P) structure was successfully constructed in this Nb-alloyed MEA, which could effectively combine precipitation hardening and hetero-deformation induced (HDI) hardening effects. Deformation characters investigations reveals that the absence of mechanical twinning in γ′′-strengthened MEA originates from the improved critical twinning stress related to the fine dislocation source size and the difficulty of high-energy complex SFs reordering. The combination of massive stacking-faults, Lomer-Cottrell locks and dynamically reinforced HDI hardening contribute to the excellent ductility and work-hardening capacity at high-level strength in the HLG + dual-P structural alloy. Our work provides a useful insight and helpful guidance for developing high-performance precipitation-hardened multi-principal element alloys.
first_indexed 2024-04-10T19:37:40Z
format Article
id doaj.art-658758fbc4464aaa9e3dfe48d7f0bdaa
institution Directory Open Access Journal
issn 0264-1275
language English
last_indexed 2024-04-10T19:37:40Z
publishDate 2023-01-01
publisher Elsevier
record_format Article
series Materials & Design
spelling doaj.art-658758fbc4464aaa9e3dfe48d7f0bdaa2023-01-30T04:12:07ZengElsevierMaterials & Design0264-12752023-01-01225111477γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloyWenjie Lu0Xian Luo1Yafeng Wang2Bin Huang3Zhijun Wang4Yanqing Yang5State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR China; Langu Institute for Materials Analysis Co. Ltd, Weihai 264207, PR ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR China; Corresponding authors.State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR ChinaState Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, PR China; Langu Institute for Materials Analysis Co. Ltd, Weihai 264207, PR China; Corresponding authors.In present work, a novel γ′′-strengthened Nb-alloyed medium-entropy alloy (MEA) was successfully fabricated and systematically investigated. Our results evidence that the γ′′ phase brings out significant precipitation hardening effect (∼10.2 %volume fraction contributes ∼ 685 MPa strength enhancement). The metastable γ′′ phase could abnormally transform to ε phase, and the morphology and distribution of ε phase shows great impacts on mechanical properties. A hetero-lamellae grain coupling with dual-precipitation (HLG + dual-P) structure was successfully constructed in this Nb-alloyed MEA, which could effectively combine precipitation hardening and hetero-deformation induced (HDI) hardening effects. Deformation characters investigations reveals that the absence of mechanical twinning in γ′′-strengthened MEA originates from the improved critical twinning stress related to the fine dislocation source size and the difficulty of high-energy complex SFs reordering. The combination of massive stacking-faults, Lomer-Cottrell locks and dynamically reinforced HDI hardening contribute to the excellent ductility and work-hardening capacity at high-level strength in the HLG + dual-P structural alloy. Our work provides a useful insight and helpful guidance for developing high-performance precipitation-hardened multi-principal element alloys.http://www.sciencedirect.com/science/article/pii/S0264127522011005Medium-entropy alloyγ′′ phasePrecipitation behaviorPrecipitation hardeningHetero-deformation induced hardening
spellingShingle Wenjie Lu
Xian Luo
Yafeng Wang
Bin Huang
Zhijun Wang
Yanqing Yang
γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
Materials & Design
Medium-entropy alloy
γ′′ phase
Precipitation behavior
Precipitation hardening
Hetero-deformation induced hardening
title γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
title_full γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
title_fullStr γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
title_full_unstemmed γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
title_short γ′′ Phase transformation, precipitation hardening, hetero-deformation induced hardening and deformation mechanisms in a Nb-alloyed medium-entropy alloy
title_sort γ phase transformation precipitation hardening hetero deformation induced hardening and deformation mechanisms in a nb alloyed medium entropy alloy
topic Medium-entropy alloy
γ′′ phase
Precipitation behavior
Precipitation hardening
Hetero-deformation induced hardening
url http://www.sciencedirect.com/science/article/pii/S0264127522011005
work_keys_str_mv AT wenjielu gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy
AT xianluo gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy
AT yafengwang gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy
AT binhuang gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy
AT zhijunwang gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy
AT yanqingyang gphasetransformationprecipitationhardeningheterodeformationinducedhardeninganddeformationmechanismsinanballoyedmediumentropyalloy