3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity

Binder Jetting (BJT) is a non-fusion-based Additive Manufacturing (AM) technique. It consists of the selective deposition of a liquid binder to join powder particles, thereby enabling the creation of near-net-shaped parts.In this study, the main printing parameters correlated to the binder distribut...

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Main Authors: Francesco Bertolini, Marco Mariani, Elisa Mercadelli, Carlo Baldisserri, Carmen Galassi, Claudio Capiani, Raffaele Ardito, Nora Lecis
Format: Article
Language:English
Published: Elsevier 2024-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424004381
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author Francesco Bertolini
Marco Mariani
Elisa Mercadelli
Carlo Baldisserri
Carmen Galassi
Claudio Capiani
Raffaele Ardito
Nora Lecis
author_facet Francesco Bertolini
Marco Mariani
Elisa Mercadelli
Carlo Baldisserri
Carmen Galassi
Claudio Capiani
Raffaele Ardito
Nora Lecis
author_sort Francesco Bertolini
collection DOAJ
description Binder Jetting (BJT) is a non-fusion-based Additive Manufacturing (AM) technique. It consists of the selective deposition of a liquid binder to join powder particles, thereby enabling the creation of near-net-shaped parts.In this study, the main printing parameters correlated to the binder distribution and infiltration (binder saturation, binder set time, drying time, and target bed temperature) were optimised to improve the precision of green parts printed with potassium sodium niobate (KNN) powder. The optimisation procedure was conducted using the Taguchi statistical method. An L9 orthogonal array with four factors of control at three levels each was employed. The analysis showed that the drying time had the greatest influence on the precision of green parts, followed by binder saturation and target bed temperature. Binder set time did not seem to affect the results.Dimensional analysis, microstructural and piezoelectric characterisation of parts densified by pressureless sintering were conducted. The highest average relative density exceeded 80% for the specimens printed with the lower binder saturation. Piezoelectric properties exhibit more complex behaviour. The prolonged infiltration of larger binder volumes is correlated to higher g33, thus FOMh and FOM33, and lower values for ε33T. On the other hand, d33 does not display a specific dependence on density or printing parameters.The results of this study indicate that BJT can be used to fabricate high-precision KNN components with good piezoelectric properties. The optimisation of printing parameters is essential to achieve the desired results.
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spelling doaj.art-66f6ce5e6c004a0d8cb1fb23965fe4e12024-03-24T06:58:29ZengElsevierJournal of Materials Research and Technology2238-78542024-03-0129459746063D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosityFrancesco Bertolini0Marco Mariani1Elisa Mercadelli2Carlo Baldisserri3Carmen Galassi4Claudio Capiani5Raffaele Ardito6Nora Lecis7Department of Mechanical Engineering, Politecnico di Milano, Milano, 20156, Italy; Corresponding author.Department of Mechanical Engineering, Politecnico di Milano, Milano, 20156, ItalyNational Research Council of Italy, Institute of Science, Technology and Sustainability for Ceramics (CNR-ISSMC, Former ISTEC), Faenza, 48018, ItalyNational Research Council of Italy, Institute of Science, Technology and Sustainability for Ceramics (CNR-ISSMC, Former ISTEC), Faenza, 48018, ItalyDepartment of Mechanical Engineering, Politecnico di Milano, Milano, 20156, Italy; National Research Council of Italy, Institute of Science, Technology and Sustainability for Ceramics (CNR-ISSMC, Former ISTEC), Faenza, 48018, ItalyNational Research Council of Italy, Institute of Science, Technology and Sustainability for Ceramics (CNR-ISSMC, Former ISTEC), Faenza, 48018, ItalyDepartment of Civil and Environmental Engineering, Politecnico di Milano, Milano, 20133, ItalyDepartment of Mechanical Engineering, Politecnico di Milano, Milano, 20156, ItalyBinder Jetting (BJT) is a non-fusion-based Additive Manufacturing (AM) technique. It consists of the selective deposition of a liquid binder to join powder particles, thereby enabling the creation of near-net-shaped parts.In this study, the main printing parameters correlated to the binder distribution and infiltration (binder saturation, binder set time, drying time, and target bed temperature) were optimised to improve the precision of green parts printed with potassium sodium niobate (KNN) powder. The optimisation procedure was conducted using the Taguchi statistical method. An L9 orthogonal array with four factors of control at three levels each was employed. The analysis showed that the drying time had the greatest influence on the precision of green parts, followed by binder saturation and target bed temperature. Binder set time did not seem to affect the results.Dimensional analysis, microstructural and piezoelectric characterisation of parts densified by pressureless sintering were conducted. The highest average relative density exceeded 80% for the specimens printed with the lower binder saturation. Piezoelectric properties exhibit more complex behaviour. The prolonged infiltration of larger binder volumes is correlated to higher g33, thus FOMh and FOM33, and lower values for ε33T. On the other hand, d33 does not display a specific dependence on density or printing parameters.The results of this study indicate that BJT can be used to fabricate high-precision KNN components with good piezoelectric properties. The optimisation of printing parameters is essential to achieve the desired results.http://www.sciencedirect.com/science/article/pii/S2238785424004381Binder jettingAdditive manufacturingPorous piezoceramicPotassium sodium niobateDesign of experimentTaguchi method
spellingShingle Francesco Bertolini
Marco Mariani
Elisa Mercadelli
Carlo Baldisserri
Carmen Galassi
Claudio Capiani
Raffaele Ardito
Nora Lecis
3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
Journal of Materials Research and Technology
Binder jetting
Additive manufacturing
Porous piezoceramic
Potassium sodium niobate
Design of experiment
Taguchi method
title 3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
title_full 3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
title_fullStr 3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
title_full_unstemmed 3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
title_short 3D printing of potassium sodium niobate by binder jetting: Printing parameters optimisation and correlation to final porosity
title_sort 3d printing of potassium sodium niobate by binder jetting printing parameters optimisation and correlation to final porosity
topic Binder jetting
Additive manufacturing
Porous piezoceramic
Potassium sodium niobate
Design of experiment
Taguchi method
url http://www.sciencedirect.com/science/article/pii/S2238785424004381
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