Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method

SrBi4Ti4O15 is one of four-layered Aurivillius compound family member that can be used as photocatalyst material that works in the violet light region. To expand its work function range can be conducted by doped with metal elements to SrBi4Ti4O15 as results reduced its band gap energy. In this resea...

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Main Authors: Puspa Sari, Suci Noerfaiqotul Himmah, Arie Hardian, Nur Aini, Anton Prasetyo
Format: Article
Language:English
Published: Komunitas Ilmuwan dan Profesional Muslim Indonesia 2022-12-01
Series:Communications in Science and Technology
Subjects:
Online Access:https://cst.kipmi.or.id/journal/article/view/940
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author Puspa Sari
Suci Noerfaiqotul Himmah
Arie Hardian
Nur Aini
Anton Prasetyo
author_facet Puspa Sari
Suci Noerfaiqotul Himmah
Arie Hardian
Nur Aini
Anton Prasetyo
author_sort Puspa Sari
collection DOAJ
description SrBi4Ti4O15 is one of four-layered Aurivillius compound family member that can be used as photocatalyst material that works in the violet light region. To expand its work function range can be conducted by doped with metal elements to SrBi4Ti4O15 as results reduced its band gap energy. In this research, we synthesized vanadium doped SrBi4Ti4O15 (SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15)) by molten salt method (used KCl salt). The diffractogram sample showed that the target compounds SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15) had been successfully synthesized with the space group A21am without impurities. The SEM micrographs showed the particle shape of SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15) was plate-like (sheets) and V dopant did not cause agglomeration. The result of Kubelka-Munk equation calculation showed that the V dopant can reduced the band gap energy value from 3.04 eV (408 nm) to 2.84 eV (437 nm)
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spelling doaj.art-6752fe159fd14446a6674017e84164e92022-12-31T17:02:10ZengKomunitas Ilmuwan dan Profesional Muslim IndonesiaCommunications in Science and Technology2502-92582502-92662022-12-017217518010.21924/cst.7.2.2022.940940Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt methodPuspa Sari0Suci Noerfaiqotul Himmah1Arie Hardian2Nur Aini3Anton Prasetyo4Department of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, 65144, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, 65144, IndonesiaDepartment of Chemistry, Faculty of Sciences and Informatics, Universitas Jenderal Achmad Yani, Jl. Jenderal Sudirman, Cimahi, 40531, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, 65144, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Universitas Islam Negeri Maulana Malik Ibrahim Malang, Malang, 65144, IndonesiaSrBi4Ti4O15 is one of four-layered Aurivillius compound family member that can be used as photocatalyst material that works in the violet light region. To expand its work function range can be conducted by doped with metal elements to SrBi4Ti4O15 as results reduced its band gap energy. In this research, we synthesized vanadium doped SrBi4Ti4O15 (SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15)) by molten salt method (used KCl salt). The diffractogram sample showed that the target compounds SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15) had been successfully synthesized with the space group A21am without impurities. The SEM micrographs showed the particle shape of SrBi4Ti4-nVnO15 (n= 0, 0.05, 0.1, and 0.15) was plate-like (sheets) and V dopant did not cause agglomeration. The result of Kubelka-Munk equation calculation showed that the V dopant can reduced the band gap energy value from 3.04 eV (408 nm) to 2.84 eV (437 nm)https://cst.kipmi.or.id/journal/article/view/940srbi4ti4o15v dopantmolten salt methodkcl
spellingShingle Puspa Sari
Suci Noerfaiqotul Himmah
Arie Hardian
Nur Aini
Anton Prasetyo
Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
Communications in Science and Technology
srbi4ti4o15
v dopant
molten salt method
kcl
title Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
title_full Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
title_fullStr Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
title_full_unstemmed Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
title_short Synthesis and characterization of plate-like vanadium doped SrBi4Ti4O15 prepared via KCl molten salt method
title_sort synthesis and characterization of plate like vanadium doped srbi4ti4o15 prepared via kcl molten salt method
topic srbi4ti4o15
v dopant
molten salt method
kcl
url https://cst.kipmi.or.id/journal/article/view/940
work_keys_str_mv AT puspasari synthesisandcharacterizationofplatelikevanadiumdopedsrbi4ti4o15preparedviakclmoltensaltmethod
AT sucinoerfaiqotulhimmah synthesisandcharacterizationofplatelikevanadiumdopedsrbi4ti4o15preparedviakclmoltensaltmethod
AT ariehardian synthesisandcharacterizationofplatelikevanadiumdopedsrbi4ti4o15preparedviakclmoltensaltmethod
AT nuraini synthesisandcharacterizationofplatelikevanadiumdopedsrbi4ti4o15preparedviakclmoltensaltmethod
AT antonprasetyo synthesisandcharacterizationofplatelikevanadiumdopedsrbi4ti4o15preparedviakclmoltensaltmethod