Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging

The potential formation and the size of microgaps at the material/dentin interface after various surface modifications of a resin-matrix computer-aided design/computer-aided manufacturing (CAD/CAM) ceramic following artificial aging was investigated. Fifty human third molars were used, and a resin-m...

Full description

Bibliographic Details
Main Authors: Alexandros Galanopoulos, Dimitrios Dionysopoulos, Constantinos Papadopoulos, Petros Mourouzis, Kosmas Tolidis
Format: Article
Language:English
Published: MDPI AG 2023-02-01
Series:Applied Sciences
Subjects:
Online Access:https://www.mdpi.com/2076-3417/13/4/2335
_version_ 1797622558401495040
author Alexandros Galanopoulos
Dimitrios Dionysopoulos
Constantinos Papadopoulos
Petros Mourouzis
Kosmas Tolidis
author_facet Alexandros Galanopoulos
Dimitrios Dionysopoulos
Constantinos Papadopoulos
Petros Mourouzis
Kosmas Tolidis
author_sort Alexandros Galanopoulos
collection DOAJ
description The potential formation and the size of microgaps at the material/dentin interface after various surface modifications of a resin-matrix computer-aided design/computer-aided manufacturing (CAD/CAM) ceramic following artificial aging was investigated. Fifty human third molars were used, and a resin-matrix CAD/CAM ceramic, Lava Ultimate, and a resin cement material, Rely X Ultimate, were tested. CAD/CAM blocks were sectioned, and each slab was luted on the tooth surface using the same resin cement. The surface material was modified using the following treatments: Group 1—no treatment (control); Group 2—hydrofluoric acid (HF) + silane; Group 3—air abrasion with Al<sub>2</sub>O<sub>3</sub> particles (29 μm); Group 4—air abrasion with Al<sub>2</sub>O<sub>3</sub> particles (53 μm); and Group 5—erbium, chromium:yttrium–scandium–gallium–garnet (Er,Cr:YSGG) (2780 nm) laser treatment. The specimens were submitted to thermocycling (5000 cycles: 5 °C–55 °C) and then transversely cut in the middle and examined using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). Larger microgaps were observed in the control and laser-treated groups, with no significant differences (<i>p</i> = 0.452). By contrast, the other three groups presented lower microgap formation, and in some cases, no microgaps were detected. Air-abrasion groups exhibited the lowest microgap formation (<i>p</i> < 0.05). Different surface modifications of the material presented significant differences in the formation of microgaps at the adhesive interface after artificial aging, implying differences in bond strengths among the groups. Air-abrasion pretreatments with Al<sub>2</sub>O<sub>3</sub> particles presented more beneficial results regarding microgap formation.
first_indexed 2024-03-11T09:13:01Z
format Article
id doaj.art-6766c3fcd89942a89aec35dd7a184507
institution Directory Open Access Journal
issn 2076-3417
language English
last_indexed 2024-03-11T09:13:01Z
publishDate 2023-02-01
publisher MDPI AG
record_format Article
series Applied Sciences
spelling doaj.art-6766c3fcd89942a89aec35dd7a1845072023-11-16T18:54:30ZengMDPI AGApplied Sciences2076-34172023-02-01134233510.3390/app13042335Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial AgingAlexandros Galanopoulos0Dimitrios Dionysopoulos1Constantinos Papadopoulos2Petros Mourouzis3Kosmas Tolidis4Department of Operative Dentistry, Faculty of Dentistry, School of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, GreeceDepartment of Operative Dentistry, Faculty of Dentistry, School of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, GreeceDepartment of Operative Dentistry, Faculty of Dentistry, School of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, GreeceDepartment of Operative Dentistry, Faculty of Dentistry, School of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, GreeceDepartment of Operative Dentistry, Faculty of Dentistry, School of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, GreeceThe potential formation and the size of microgaps at the material/dentin interface after various surface modifications of a resin-matrix computer-aided design/computer-aided manufacturing (CAD/CAM) ceramic following artificial aging was investigated. Fifty human third molars were used, and a resin-matrix CAD/CAM ceramic, Lava Ultimate, and a resin cement material, Rely X Ultimate, were tested. CAD/CAM blocks were sectioned, and each slab was luted on the tooth surface using the same resin cement. The surface material was modified using the following treatments: Group 1—no treatment (control); Group 2—hydrofluoric acid (HF) + silane; Group 3—air abrasion with Al<sub>2</sub>O<sub>3</sub> particles (29 μm); Group 4—air abrasion with Al<sub>2</sub>O<sub>3</sub> particles (53 μm); and Group 5—erbium, chromium:yttrium–scandium–gallium–garnet (Er,Cr:YSGG) (2780 nm) laser treatment. The specimens were submitted to thermocycling (5000 cycles: 5 °C–55 °C) and then transversely cut in the middle and examined using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). Larger microgaps were observed in the control and laser-treated groups, with no significant differences (<i>p</i> = 0.452). By contrast, the other three groups presented lower microgap formation, and in some cases, no microgaps were detected. Air-abrasion groups exhibited the lowest microgap formation (<i>p</i> < 0.05). Different surface modifications of the material presented significant differences in the formation of microgaps at the adhesive interface after artificial aging, implying differences in bond strengths among the groups. Air-abrasion pretreatments with Al<sub>2</sub>O<sub>3</sub> particles presented more beneficial results regarding microgap formation.https://www.mdpi.com/2076-3417/13/4/2335artificial agingEr,Cr:YSGG lasermicrogap formationresin-matrix CAD/CAM ceramicssurface treatments
spellingShingle Alexandros Galanopoulos
Dimitrios Dionysopoulos
Constantinos Papadopoulos
Petros Mourouzis
Kosmas Tolidis
Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
Applied Sciences
artificial aging
Er,Cr:YSGG laser
microgap formation
resin-matrix CAD/CAM ceramics
surface treatments
title Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
title_full Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
title_fullStr Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
title_full_unstemmed Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
title_short Microgap Formation between a Dental Resin-Matrix Computer-Aided Design/Computer-Aided Manufacturing Ceramic Restorative and Dentin after Various Surface Treatments and Artificial Aging
title_sort microgap formation between a dental resin matrix computer aided design computer aided manufacturing ceramic restorative and dentin after various surface treatments and artificial aging
topic artificial aging
Er,Cr:YSGG laser
microgap formation
resin-matrix CAD/CAM ceramics
surface treatments
url https://www.mdpi.com/2076-3417/13/4/2335
work_keys_str_mv AT alexandrosgalanopoulos microgapformationbetweenadentalresinmatrixcomputeraideddesigncomputeraidedmanufacturingceramicrestorativeanddentinaftervarioussurfacetreatmentsandartificialaging
AT dimitriosdionysopoulos microgapformationbetweenadentalresinmatrixcomputeraideddesigncomputeraidedmanufacturingceramicrestorativeanddentinaftervarioussurfacetreatmentsandartificialaging
AT constantinospapadopoulos microgapformationbetweenadentalresinmatrixcomputeraideddesigncomputeraidedmanufacturingceramicrestorativeanddentinaftervarioussurfacetreatmentsandartificialaging
AT petrosmourouzis microgapformationbetweenadentalresinmatrixcomputeraideddesigncomputeraidedmanufacturingceramicrestorativeanddentinaftervarioussurfacetreatmentsandartificialaging
AT kosmastolidis microgapformationbetweenadentalresinmatrixcomputeraideddesigncomputeraidedmanufacturingceramicrestorativeanddentinaftervarioussurfacetreatmentsandartificialaging