In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature

Calcite twinning is a dominant deformation mechanism at low temperatures. It is often used to reconstruct paleostresses: orientations of the principal stress axes, stress ratios and differential stress. Despite numerous studies, on single crystals and aggregates, questions remain about the initiatio...

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Main Authors: Camille Parlangeau, Alexandre Dimanov, Simon Hallais
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Geosciences
Subjects:
Online Access:https://www.mdpi.com/2076-3263/12/6/233
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author Camille Parlangeau
Alexandre Dimanov
Simon Hallais
author_facet Camille Parlangeau
Alexandre Dimanov
Simon Hallais
author_sort Camille Parlangeau
collection DOAJ
description Calcite twinning is a dominant deformation mechanism at low temperatures. It is often used to reconstruct paleostresses: orientations of the principal stress axes, stress ratios and differential stress. Despite numerous studies, on single crystals and aggregates, questions remain about the initiation and evolution of the twinning. In particular, the existence of a critical value for the activation of twin planes is debated. In this study, Carrara marble samples were uniaxially deformed at low temperature. The experiments were monitored in situ in an SEM (Scanning Electron Microscope) and a deformation analysis was performed at regular intervals using image correlation. Image correlation analysis shows the link between the overconcentration of strains and the appearance of the first twinned planes. This is followed by a densification and a gradual thickening of the twin lamellae. Fracturing only appears in a third stage as a precursor to the collapse of the sample. The inversion, using the CSIT-2 technique, showed that the twinned planes are globally related to the applied macroscopic stress. The inversion allows one to retrieve the macroscopic stress tensor. Schmid factors were extracted from this analysis and correlated to the loading curves. For crystals of about 200 µm diameter, the threshold value is in between 6.75 and 8.25 MPa.
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spelling doaj.art-6775278762be480598f4aa24c792123b2023-11-23T16:49:51ZengMDPI AGGeosciences2076-32632022-05-0112623310.3390/geosciences12060233In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room TemperatureCamille Parlangeau0Alexandre Dimanov1Simon Hallais2Laboratoire de Mécanique des Solides, CNRS UMR 7649, École Polytechnique, 91128 Palaiseau, FranceLaboratoire de Mécanique des Solides, CNRS UMR 7649, École Polytechnique, 91128 Palaiseau, FranceLaboratoire de Mécanique des Solides, CNRS UMR 7649, École Polytechnique, 91128 Palaiseau, FranceCalcite twinning is a dominant deformation mechanism at low temperatures. It is often used to reconstruct paleostresses: orientations of the principal stress axes, stress ratios and differential stress. Despite numerous studies, on single crystals and aggregates, questions remain about the initiation and evolution of the twinning. In particular, the existence of a critical value for the activation of twin planes is debated. In this study, Carrara marble samples were uniaxially deformed at low temperature. The experiments were monitored in situ in an SEM (Scanning Electron Microscope) and a deformation analysis was performed at regular intervals using image correlation. Image correlation analysis shows the link between the overconcentration of strains and the appearance of the first twinned planes. This is followed by a densification and a gradual thickening of the twin lamellae. Fracturing only appears in a third stage as a precursor to the collapse of the sample. The inversion, using the CSIT-2 technique, showed that the twinned planes are globally related to the applied macroscopic stress. The inversion allows one to retrieve the macroscopic stress tensor. Schmid factors were extracted from this analysis and correlated to the loading curves. For crystals of about 200 µm diameter, the threshold value is in between 6.75 and 8.25 MPa.https://www.mdpi.com/2076-3263/12/6/233calcite twincritical resolved shear stressin-situ deformation experiment
spellingShingle Camille Parlangeau
Alexandre Dimanov
Simon Hallais
In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
Geosciences
calcite twin
critical resolved shear stress
in-situ deformation experiment
title In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
title_full In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
title_fullStr In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
title_full_unstemmed In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
title_short In-Situ Evolution of Calcite Twinning during Uniaxial Compression of Carrara Marble at Room Temperature
title_sort in situ evolution of calcite twinning during uniaxial compression of carrara marble at room temperature
topic calcite twin
critical resolved shear stress
in-situ deformation experiment
url https://www.mdpi.com/2076-3263/12/6/233
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