Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition
Solid state transformation of supersaturated solid solution to anomalous Ni-Sn eutectic has been studied. The metastableNi-Sn solid solution was prepared via mechanical alloying of a mixed Ni+Sn powder containing 32.5 wt-% Sn powder.The milling conditions included ball to powder ratio (BPR) of 5:1 a...
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Format: | Article |
Language: | English |
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Prince of Songkla University
2011-04-01
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Series: | Songklanakarin Journal of Science and Technology (SJST) |
Subjects: | |
Online Access: | http://rdo.psu.ac.th/sjstweb/journal/33-2/0125-3395-33-2-209-214.pdf |
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author | Ruangdaj Tongsri Nattaya Tosangthum |
author_facet | Ruangdaj Tongsri Nattaya Tosangthum |
author_sort | Ruangdaj Tongsri |
collection | DOAJ |
description | Solid state transformation of supersaturated solid solution to anomalous Ni-Sn eutectic has been studied. The metastableNi-Sn solid solution was prepared via mechanical alloying of a mixed Ni+Sn powder containing 32.5 wt-% Sn powder.The milling conditions included ball to powder ratio (BPR) of 5:1 and milling speed of 300 rpm. Milling times were varied as5, 15, and 25 hours. Milling the mixed powder for longer than 15 hours resulted in formation of supersaturated Ni-Sn solidsolution. Differential thermal analysis of the supersaturated Ni-Sn solid solution revealed two reactions, namely peritectoidand peritectic reactions, occurring at 945 and 1,141°C, respectively. Heating of the supersaturated Ni-Sn solid solution todifferent temperatures such as 800, 850, 900, 950, 1,100, and 1,140°C with holding time of 10 minutes resulted in developmentof anomalous eutectic with Ni3Sn phase matrix embedded with Ni solution particles. Sintering and coarsening of the eutecticwas depending on heating temperatures. |
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id | doaj.art-67858e2013c74036920a3eb531458114 |
institution | Directory Open Access Journal |
issn | 0125-3395 |
language | English |
last_indexed | 2024-12-23T14:46:43Z |
publishDate | 2011-04-01 |
publisher | Prince of Songkla University |
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series | Songklanakarin Journal of Science and Technology (SJST) |
spelling | doaj.art-67858e2013c74036920a3eb5314581142022-12-21T17:43:05ZengPrince of Songkla UniversitySongklanakarin Journal of Science and Technology (SJST)0125-33952011-04-01332209214Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic compositionRuangdaj TongsriNattaya TosangthumSolid state transformation of supersaturated solid solution to anomalous Ni-Sn eutectic has been studied. The metastableNi-Sn solid solution was prepared via mechanical alloying of a mixed Ni+Sn powder containing 32.5 wt-% Sn powder.The milling conditions included ball to powder ratio (BPR) of 5:1 and milling speed of 300 rpm. Milling times were varied as5, 15, and 25 hours. Milling the mixed powder for longer than 15 hours resulted in formation of supersaturated Ni-Sn solidsolution. Differential thermal analysis of the supersaturated Ni-Sn solid solution revealed two reactions, namely peritectoidand peritectic reactions, occurring at 945 and 1,141°C, respectively. Heating of the supersaturated Ni-Sn solid solution todifferent temperatures such as 800, 850, 900, 950, 1,100, and 1,140°C with holding time of 10 minutes resulted in developmentof anomalous eutectic with Ni3Sn phase matrix embedded with Ni solution particles. Sintering and coarsening of the eutecticwas depending on heating temperatures.http://rdo.psu.ac.th/sjstweb/journal/33-2/0125-3395-33-2-209-214.pdfmechanical millinganomalous N-Sn eutecticsolid state transformation |
spellingShingle | Ruangdaj Tongsri Nattaya Tosangthum Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition Songklanakarin Journal of Science and Technology (SJST) mechanical milling anomalous N-Sn eutectic solid state transformation |
title | Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition |
title_full | Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition |
title_fullStr | Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition |
title_full_unstemmed | Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition |
title_short | Solid state transformation of non-equilibrium Ni-Sn powder with a eutectic composition |
title_sort | solid state transformation of non equilibrium ni sn powder with a eutectic composition |
topic | mechanical milling anomalous N-Sn eutectic solid state transformation |
url | http://rdo.psu.ac.th/sjstweb/journal/33-2/0125-3395-33-2-209-214.pdf |
work_keys_str_mv | AT ruangdajtongsri solidstatetransformationofnonequilibriumnisnpowderwithaeutecticcomposition AT nattayatosangthum solidstatetransformationofnonequilibriumnisnpowderwithaeutecticcomposition |