Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt

In this study, the low-temperature reduction-diffusion (LTRD) process using a Li-Ca reductant, which has a low eutectic point of about 230 °C, was demonstrated. The RD reaction was possible at a very low temperature of 400 °C significantly less than 850 °C, which is the lowest practicable temperatur...

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Main Authors: Jungryang Kim, Shusuke Okada, Kenta Takagi
Format: Article
Language:English
Published: AIP Publishing LLC 2023-02-01
Series:AIP Advances
Online Access:http://dx.doi.org/10.1063/9.0000458
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author Jungryang Kim
Shusuke Okada
Kenta Takagi
author_facet Jungryang Kim
Shusuke Okada
Kenta Takagi
author_sort Jungryang Kim
collection DOAJ
description In this study, the low-temperature reduction-diffusion (LTRD) process using a Li-Ca reductant, which has a low eutectic point of about 230 °C, was demonstrated. The RD reaction was possible at a very low temperature of 400 °C significantly less than 850 °C, which is the lowest practicable temperature of the conventional RD process, by identifying the production of the SmFe2 phase. The LTRD process in this study also made it possible to investigate the Sm-Fe binary phases synthesized at the low temperature and the Sm-Fe phase transitions depending on the temperatures with the compositions of Sm and Fe.
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spelling doaj.art-6795d62776b8484c8949ed5759e78bf62023-03-10T17:26:20ZengAIP Publishing LLCAIP Advances2158-32262023-02-01132025124025124-510.1063/9.0000458Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic meltJungryang Kim0Shusuke Okada1Kenta Takagi2Magnetic Powder Metallurgy Research Center, National Institute of Advanced Industrial Science and Technology (AIST), 2266-98 Anagahora, Shimoshidami, Moriyama-ku, Nagoya 463-8560, Aichi, JapanMagnetic Powder Metallurgy Research Center, National Institute of Advanced Industrial Science and Technology (AIST), 2266-98 Anagahora, Shimoshidami, Moriyama-ku, Nagoya 463-8560, Aichi, JapanMagnetic Powder Metallurgy Research Center, National Institute of Advanced Industrial Science and Technology (AIST), 2266-98 Anagahora, Shimoshidami, Moriyama-ku, Nagoya 463-8560, Aichi, JapanIn this study, the low-temperature reduction-diffusion (LTRD) process using a Li-Ca reductant, which has a low eutectic point of about 230 °C, was demonstrated. The RD reaction was possible at a very low temperature of 400 °C significantly less than 850 °C, which is the lowest practicable temperature of the conventional RD process, by identifying the production of the SmFe2 phase. The LTRD process in this study also made it possible to investigate the Sm-Fe binary phases synthesized at the low temperature and the Sm-Fe phase transitions depending on the temperatures with the compositions of Sm and Fe.http://dx.doi.org/10.1063/9.0000458
spellingShingle Jungryang Kim
Shusuke Okada
Kenta Takagi
Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
AIP Advances
title Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
title_full Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
title_fullStr Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
title_full_unstemmed Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
title_short Low temperature synthesis of Sm-Fe alloy powder by reduction-diffusion process using new reductant of Li-Ca eutectic melt
title_sort low temperature synthesis of sm fe alloy powder by reduction diffusion process using new reductant of li ca eutectic melt
url http://dx.doi.org/10.1063/9.0000458
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AT kentatakagi lowtemperaturesynthesisofsmfealloypowderbyreductiondiffusionprocessusingnewreductantoflicaeutecticmelt