Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material

Over the last decade, zirconia (ZrO<sub>2</sub>)-based ceramic materials have become more applicable to modern dental medicine due to the sustained development of diverse computer-aided design/computer-aided manufacturing (CAD/CAM) systems. However, before the cementation and clinical ap...

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Main Authors: Marko Jakovac, Teodoro Klaser, Borna Radatović, Arijeta Bafti, Željko Skoko, Luka Pavić, Mark Žic
Format: Article
Language:English
Published: MDPI AG 2021-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/11/2834
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author Marko Jakovac
Teodoro Klaser
Borna Radatović
Arijeta Bafti
Željko Skoko
Luka Pavić
Mark Žic
author_facet Marko Jakovac
Teodoro Klaser
Borna Radatović
Arijeta Bafti
Željko Skoko
Luka Pavić
Mark Žic
author_sort Marko Jakovac
collection DOAJ
description Over the last decade, zirconia (ZrO<sub>2</sub>)-based ceramic materials have become more applicable to modern dental medicine due to the sustained development of diverse computer-aided design/computer-aided manufacturing (CAD/CAM) systems. However, before the cementation and clinical application, the freshly prepared zirconia material (e.g., crowns) has to be processed by sandblasting in the dental laboratory. In this work, the impact of the sandblasting on the zirconia is monitored as changes in morphology (i.e., grains and cracks), and the presence of impurities might result in a poor adhesive bonding with cement. The sandblasting is conducted by using Al<sub>2</sub>O<sub>3</sub> powder (25, 50, 110 and 125 µm) under various amounts of air-abrasion pressure (0.1, 0.2, 0.4 and 0.6 MPa). There has been much interest in both the determination of the impact of the sandblasting on the zirconia phase transformations and conductivity. Morphology changes are observed by using Scanning Electron Microscope (SEM), the conductivity is measured by Impedance Spectroscopy (IS), and the phase transformation is observed by using Powder X-Ray Diffraction (PXRD). The results imply that even the application of the lowest amount of air-abrasion pressure and the smallest Al<sub>2</sub>O<sub>3</sub> powder size yields a morphology change, a phase transformation and a material contamination.
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spelling doaj.art-67a96628a452466bbde407b81ba499552023-11-21T21:22:15ZengMDPI AGMaterials1996-19442021-05-011411283410.3390/ma14112834Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics MaterialMarko Jakovac0Teodoro Klaser1Borna Radatović2Arijeta Bafti3Željko Skoko4Luka Pavić5Mark Žic6Department of Prosthodontics, School of Dental Medicine, University Zagreb, Gundulićeva 5, 10000 Zagreb, CroatiaDepartment of Physics, Faculty of Science, University of Zagreb, Bijenička, c. 32, 10000 Zagreb, CroatiaCenter for Excellence for Advanced Materials and Sensing Devices, Institute of Physics, 10000 Zagreb, CroatiaFaculty of Chemical Engineering and Technology, University of Zagreb, Marulićev trg 19, 10000 Zagreb, CroatiaDepartment of Physics, Faculty of Science, University of Zagreb, Bijenička, c. 32, 10000 Zagreb, CroatiaRuđer Bošković Institute, P.O. Box 180, 10000 Zagreb, CroatiaRuđer Bošković Institute, P.O. Box 180, 10000 Zagreb, CroatiaOver the last decade, zirconia (ZrO<sub>2</sub>)-based ceramic materials have become more applicable to modern dental medicine due to the sustained development of diverse computer-aided design/computer-aided manufacturing (CAD/CAM) systems. However, before the cementation and clinical application, the freshly prepared zirconia material (e.g., crowns) has to be processed by sandblasting in the dental laboratory. In this work, the impact of the sandblasting on the zirconia is monitored as changes in morphology (i.e., grains and cracks), and the presence of impurities might result in a poor adhesive bonding with cement. The sandblasting is conducted by using Al<sub>2</sub>O<sub>3</sub> powder (25, 50, 110 and 125 µm) under various amounts of air-abrasion pressure (0.1, 0.2, 0.4 and 0.6 MPa). There has been much interest in both the determination of the impact of the sandblasting on the zirconia phase transformations and conductivity. Morphology changes are observed by using Scanning Electron Microscope (SEM), the conductivity is measured by Impedance Spectroscopy (IS), and the phase transformation is observed by using Powder X-Ray Diffraction (PXRD). The results imply that even the application of the lowest amount of air-abrasion pressure and the smallest Al<sub>2</sub>O<sub>3</sub> powder size yields a morphology change, a phase transformation and a material contamination.https://www.mdpi.com/1996-1944/14/11/2834zirconiasandblastingPXRDimpedanceequivalent electrical circuit (EEC)conductivity
spellingShingle Marko Jakovac
Teodoro Klaser
Borna Radatović
Arijeta Bafti
Željko Skoko
Luka Pavić
Mark Žic
Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
Materials
zirconia
sandblasting
PXRD
impedance
equivalent electrical circuit (EEC)
conductivity
title Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
title_full Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
title_fullStr Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
title_full_unstemmed Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
title_short Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material
title_sort impact of sandblasting on morphology structure and conductivity of zirconia dental ceramics material
topic zirconia
sandblasting
PXRD
impedance
equivalent electrical circuit (EEC)
conductivity
url https://www.mdpi.com/1996-1944/14/11/2834
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