Investigation of Crystallization Kinetics of Fe36Cr12Mo10 and α-Fe Phases in Devitrification of Fe51Cr18Mo7B16C4Nb4 Amorphous Alloy
In this research, crystallization of Fe36Cr12Mo10 and α-Fe phases in devitrification of Fe51Cr18Mo7B16C4Nb4 amorphous alloy was studied using X-ray diffraction and transmission electron microscopy. For evaluation of crystallization kinetics, differential scanning calorimetric tests were carried out...
Main Authors: | , , |
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Format: | Article |
Language: | fas |
Published: |
Isfahan University of Technology
2015-05-01
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Series: | Journal of Advanced Materials in Engineering |
Subjects: | |
Online Access: | http://jame.iut.ac.ir/article-1-640-en.html |
Summary: | In this research, crystallization of Fe36Cr12Mo10 and α-Fe phases in devitrification of Fe51Cr18Mo7B16C4Nb4 amorphous alloy was studied using X-ray diffraction and transmission electron microscopy. For evaluation of crystallization kinetics, differential scanning calorimetric tests were carried out at different heating rates. Results showed that two-step crystallization led to the formation of Fe36Cr12Mo10 and α-Fe phases in the structure of alloy. Activation energy of crystallization of Fe36Cr12Mo10 and α-Fe phases measured according to Kissinger-Starink model were 747 and 880 kJ/mol, respectively. Results growth mechanism along with the decreasing nucleation rate in crystallization of Fe36Cr12Mo10 and α-Fe phases. |
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ISSN: | 2251-600X 2423-5733 |