Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy

In this study, the formation of a periodic microstructural pattern designed by laser powder bed fusion (LPBF), commonly called selective laser melting (SLM), of an AlSi10Mg alloy is revealed at high resolution using scanning transmission electron microscopy and atom probe tomography. Special attenti...

Full description

Bibliographic Details
Main Authors: Williams Lefebvre, Grégory Rose, Pauline Delroisse, Eric Baustert, Fabien Cuvilly, Aude Simar
Format: Article
Language:English
Published: Elsevier 2021-01-01
Series:Materials & Design
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0264127520307991
_version_ 1818930045231562752
author Williams Lefebvre
Grégory Rose
Pauline Delroisse
Eric Baustert
Fabien Cuvilly
Aude Simar
author_facet Williams Lefebvre
Grégory Rose
Pauline Delroisse
Eric Baustert
Fabien Cuvilly
Aude Simar
author_sort Williams Lefebvre
collection DOAJ
description In this study, the formation of a periodic microstructural pattern designed by laser powder bed fusion (LPBF), commonly called selective laser melting (SLM), of an AlSi10Mg alloy is revealed at high resolution using scanning transmission electron microscopy and atom probe tomography. Special attention is paid to the description of non-equilibrium structures and compositional fields resulting from the ultrafast cooling of the LPBF process. Observations reveal the existence of a glass state in eutectic areas, wherein short-range ordering of the diamond-Si structure is observed. The apparent very fast solidification of eutectic regions is found to involve a local strain in adjacent Al cells, which extends up to 100 nm on average. In the supersaturated aluminium solid solution retained by the LPBF process, two populations of clusters are identified, for which the potential role of the selection of hardening phases is discussed. It is proposed that the microstructure of former melt pools outside heat-affected areas is described by the repetition of a periodic microstructural pattern consisting of eutectic regions /strain-hardened Al-crystals /strain-free Al-crystals with a high density of solute-rich clusters.
first_indexed 2024-12-20T03:54:27Z
format Article
id doaj.art-690171609ce94801ba292aeb25870b4a
institution Directory Open Access Journal
issn 0264-1275
language English
last_indexed 2024-12-20T03:54:27Z
publishDate 2021-01-01
publisher Elsevier
record_format Article
series Materials & Design
spelling doaj.art-690171609ce94801ba292aeb25870b4a2022-12-21T19:54:22ZengElsevierMaterials & Design0264-12752021-01-01197109264Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloyWilliams Lefebvre0Grégory Rose1Pauline Delroisse2Eric Baustert3Fabien Cuvilly4Aude Simar5Normandie University, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, France; Corresponding author.Normandie University, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, France; Volum-e, 1 chemin de la fonderie, 76340 Blangy-sur-Bresle, FranceInstitute of Mechanics, Materials and Civil Engineering, UCLouvain, Louvain-la-Neuve, BelgiumVolum-e, 1 chemin de la fonderie, 76340 Blangy-sur-Bresle, FranceNormandie University, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, FranceInstitute of Mechanics, Materials and Civil Engineering, UCLouvain, Louvain-la-Neuve, BelgiumIn this study, the formation of a periodic microstructural pattern designed by laser powder bed fusion (LPBF), commonly called selective laser melting (SLM), of an AlSi10Mg alloy is revealed at high resolution using scanning transmission electron microscopy and atom probe tomography. Special attention is paid to the description of non-equilibrium structures and compositional fields resulting from the ultrafast cooling of the LPBF process. Observations reveal the existence of a glass state in eutectic areas, wherein short-range ordering of the diamond-Si structure is observed. The apparent very fast solidification of eutectic regions is found to involve a local strain in adjacent Al cells, which extends up to 100 nm on average. In the supersaturated aluminium solid solution retained by the LPBF process, two populations of clusters are identified, for which the potential role of the selection of hardening phases is discussed. It is proposed that the microstructure of former melt pools outside heat-affected areas is described by the repetition of a periodic microstructural pattern consisting of eutectic regions /strain-hardened Al-crystals /strain-free Al-crystals with a high density of solute-rich clusters.http://www.sciencedirect.com/science/article/pii/S0264127520307991Laser powder bed fusionSLMLPBFSelective laser meltingAdditive manufacturing powder bed fusionDesign
spellingShingle Williams Lefebvre
Grégory Rose
Pauline Delroisse
Eric Baustert
Fabien Cuvilly
Aude Simar
Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
Materials & Design
Laser powder bed fusion
SLM
LPBF
Selective laser melting
Additive manufacturing powder bed fusion
Design
title Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
title_full Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
title_fullStr Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
title_full_unstemmed Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
title_short Nanoscale periodic gradients generated by laser powder bed fusion of an AlSi10Mg alloy
title_sort nanoscale periodic gradients generated by laser powder bed fusion of an alsi10mg alloy
topic Laser powder bed fusion
SLM
LPBF
Selective laser melting
Additive manufacturing powder bed fusion
Design
url http://www.sciencedirect.com/science/article/pii/S0264127520307991
work_keys_str_mv AT williamslefebvre nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy
AT gregoryrose nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy
AT paulinedelroisse nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy
AT ericbaustert nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy
AT fabiencuvilly nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy
AT audesimar nanoscaleperiodicgradientsgeneratedbylaserpowderbedfusionofanalsi10mgalloy