Crystal structure of bis(1,10-phenanthroline-κ2N,N′)(1,3-thiazole-2-thiolato-κ2S2,N)nickel(II) hexafluoridophosphate 1,4-dioxane sesquisolvate

Crystal structure of bis(1,10-phenanthroline-κ2N,N′)(1,3-thiazole-2-thiolato-κ2S2,N)nickel(II) hexafluoridophosphate 1,4-dioxane sesquisolvate

The title salt, [Ni(C3H2NS2)(C12H8N2)2]PF6·1.5C4H8O2, was the unexpected product on making an attempt to prepare an [Ni(2-mercaptothiazolate)(1,10-phenanthroline)]+ complex by reaction of [NiCl2(1,10-phenanthroline)] with 2-mercaptothiazolate. In the resulting complex, the 2-mercaptothiazolate anion...

Full description

Bibliographic Details
Main Authors:	Keisuke Kai, Tomohiko Hamaguchi, Isao Ando
Format:	Article
Language:	English
Published:	International Union of Crystallography 2017-04-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure 2-mercaptothiazolate π–π stacking hydrogen bonding nickel(II) complex
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S205698901700456X

Similar Items

Bis[N-benzyl-N-(2-phenylethyl)dithiocarbamato-κ2S,S′](1,10-phenanthroline-κ2N,N′)zinc(II)
by: A. S. Sonia, et al.
Published: (2017-05-01)

Aqua(4-bromobenzoato-κO)bis(1,10-phenanthroline-κ2N,N′)manganese(II) 4-bromobenzoate dihydrate
by: Ling-Xia Hu, et al.
Published: (2016-05-01)

Tris(N-{bis[methyl(phenyl)amino]phosphoryl}benzenesulfonamidato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)lanthanum(III)
by: Angelina Yu. Prytula-Kurkunova, et al.
Published: (2017-07-01)

Crystal structure of (2-amino-7-methyl-4-oxidopteridine-6-carboxylato-κ3O4,N5,O6)aqua(1,10-phenanthroline-κ2N,N′)copper(II) trihydrate
by: Siddhartha S. Baisya, et al.
Published: (2014-11-01)

Synthesis and crystal structure of dichlorido(1,10-phenanthroline-κ2N,N′)gold(III) hexafluoridophosphate
by: Raphael Enoque Ferraz de Paiva, et al.
Published: (2017-07-01)

Crystal structure of catena-poly[[aquabis(4-formylbenzoato)-κ2O1,O1′;κO1-zinc]-μ-pyrazine-κ2N:N′]
by: Gülçin Şefiye Aşkın, et al.
Published: (2015-04-01)

Crystal structure of (2-amino-7-methyl-4-oxidopteridine-6-carboxylato-κ3O4,N5,O6)aqua(1,10-phenanthroline-κ2N,N′)zinc trihydrate
by: Siddhartha S. Baisya, et al.
Published: (2015-09-01)

4-(Benzo[d]thiazol-2-yl)-N,N-dimethylaniline
by: Yi-Wen Tang, et al.
Published: (2016-11-01)

catena-Poly[[diaquabis[1,4-bis(pyridin-4-yl)buta-1,3-diyne-κN]iron(II)]-μ-cyanido-κ2N:C-[dicyanido-κ2C-platinum(II)]-μ-cyanido-κ2C:N]
by: Lucia Piñeiro-López, et al.
Published: (2017-10-01)

Structural characterization and DFT study of bis{(S)-2-[(2-hydroxybenzyl)amino]-3-(4-hydroxyphenyl)propanoato-κ2N,O}(1,10-phenanthroline-κ2N,N′)cadmium(II) tetrahydrate
by: Md. Serajul Haque Faizi, et al.
Published: (2018-09-01)

Crystal structure of di-μ-hydroxido-bis[aqua(1,10-phenanthroline-κ2N,N′)copper(II)] naphthalene-2,6-dicarboxylate hexahydrate
by: Daniela Arias-Zárate, et al.
Published: (2015-04-01)

Crystal structure of {(S)-1-phenyl-N,N-bis[(pyridin-2-yl)methyl]ethanamine-κ3N,N′,N′′}bis(thiocyanato-κN)zinc from synchrotron data
by: Dong Won Lee, et al.
Published: (2017-01-01)

Crystal structure of bis{μ-4,4′-[1,3-phenylenebis(oxy)]dibenzoato-κ4O,O′:O′′,O′′′}bis[(1,10-phenanthroline-κ2N,N′)zinc(II)] dihydrate
by: Ya-Ping Li, et al.
Published: (2014-10-01)

Aquabis(2,2′-bipyridine-κ2N,N′)(isonicotinamide-κN)ruthenium(II) bis(trifluoromethanesulfonate)
by: Liam Faubert, et al.
Published: (2024-02-01)

Crystal structure of catena-poly[[bis(acetato-κO)copper(II)]-bis[μ-4-(1H-imidazol-1-yl)phenol]-κ2N3:O;κ2O:N3]
by: Mehmet Poyraz, et al.
Published: (2017-02-01)

(4′-Phenyl-2,2′:6′,2′′-terpyridine-κ3N,N′,N′′)bis(thiocyanato-κN)zinc(II) unknown solvate
by: An-ran Wang, et al.
Published: (2016-11-01)

Crystal structure of tetraaqua[2-(pyridin-2-yl)-1H-imidazole-κ2N2,N3]iron(II) sulfate
by: Zouaoui Setifi, et al.
Published: (2015-04-01)

Di-μ-chlorido-bis[(2,2′:6′,2′′-terpyridine-κ3N,N′,N′′)copper(II)] bis(trifluoromethanesulfonate)
by: Rafael A. Adrian, et al.
Published: (2021-10-01)

Crystal structure of trans-bis{4-bromo-N-[(pyridin-2-yl)methylidene]aniline-κ2N,N′}dichloridoruthenium(II)
by: Kittipong Chainok, et al.
Published: (2015-09-01)

Crystal structure of dichlorido(2,2′:6′,2′′-terpyridine-κ3N,N′,N′′)zinc: a redetermination
by: Cheng-Cheng Kong, et al.
Published: (2014-11-01)

2,3-Dihydrobenz[4,5]imidazo[2,1-b]thiazole
by: Ahmed Moussaif, et al.
Published: (2016-12-01)

Crystal structure of bis(3-bromopyridine-κN)bis(O-ethyl dithiocarbonato-κ2S,S′)nickel(II)
by: Rajni Kant, et al.
Published: (2015-01-01)

Synthesis, crystal structure and Hirshfeld surface analysis of di-μ2-iodido-bis[(2,2′-biquinoline-κ2N,N′)copper(I)]
by: Ayalew W. Temesgen, et al.
Published: (2023-03-01)

Crystal structure of an AgI intercalation compound: catena-poly[[silver(I)-μ-N-(pyridin-3-ylmethyl)pyridin-3-amine-κ2N:N′] hexafluoridophosphate acetonitrile disolvate]
by: Suk-Hee Moon, et al.
Published: (2017-10-01)

Crystal structure of bis[2-(benzothiazol-2-yl)phenolato-κ2N,O]copper(II)
by: Namhun Kim, et al.
Published: (2015-09-01)

Crystal structure of trans-(1,8-dibutyl-1,3,6,8,10,13-hexaazacyclotetradecane-κ4N3,N6,N10,N13)bis(isonicotinato-κO)nickel(II) determined from synchrotron data
by: Jong Won Shin, et al.
Published: (2016-02-01)

Crystal structure of fac-[2-(4-methyl-5-phenylpyridin-2-yl)phenyl-κ2C1,N]bis[2-(pyridin-2-yl)phenyl-κ2C1,N]iridium(III)
by: Chi-Heon Lee, et al.
Published: (2016-12-01)

2-(5-Methyl-1-benzofuran-3-yl)-N-(2-phenylethyl)acetamide
by: N. Ramprasad, et al.
Published: (2017-02-01)

Crystal structure of (μ-N-allylthiourea-κ2S:S)bis[μ-bis(diphenylphosphanyl)methane-κ2P:P′]bis[bromidocopper(I)] acetonitrile disolvate
by: Mareeya Hemman, et al.
Published: (2015-09-01)

4-[5-(Benzofuran-2-yl)-1-phenyl-1H-pyrazol-3-yl]-N,N-dimethylaniline
by: G. S. Lingaraju, et al.
Published: (2016-08-01)

Crystal structure of N-[3-(benzo[d]thiazol-2-yl)-6-bromo-2H-chromen-2-ylidene]-4-methylbenzenamine
by: Amira E. M. Abdallah, et al.
Published: (2023-05-01)

N-[(3-Bromo-1-phenylsulfonyl-1H-indol-2-yl)methyl]-4-fluoroaniline
by: C. Suresh Yadav, et al.
Published: (2017-02-01)

Crystal structure of 1-benzyl-3-methyl-1H-imidazolium hexafluoridophosphate
by: Patrick C. Hillesheim, et al.
Published: (2014-12-01)

5-(2-Methylfuran-3-yl)-N-phenyl-1,3,4-oxadiazol-2-amine
by: Santosh Paswan, et al.
Published: (2016-11-01)

4-(4-Bromophenyl)-2-(3-(4-chlorophenyl)-5-{3-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazol-4-yl]-1-phenyl-1H-pyrazol-4-yl}-4,5-dihydro-1H-pyrazol-1-yl)thiazole
by: Gamal A. El-Hiti, et al.
Published: (2018-01-01)

N′-[(1E)-2,5-Dimethoxybenzylidene]pyridine-2-carbohydrazide
by: Mustafa R.Albayati, et al.
Published: (2018-01-01)

Crystal structure of tetraaqua(5,5′-dimethyl-2,2′-bipyridyl-κ2N,N′)iron(II) sulfate
by: Yamine Belamri, et al.
Published: (2014-12-01)

Benzo[4,5]imidazo[2,1-b]thiazole-2-carbaldehyde
by: Basappa Yallur, et al.
Published: (2016-05-01)

N-(4-Methoxy-2-nitrophenyl)-2-(3-methyl-2-oxo-1,2-dihydroquinoxalin-1-yl)acetamide
by: Mohcine Missioui, et al.
Published: (2023-03-01)

Crystal structure of 2-hydroxyimino-2-(pyridin-2-yl)-N′-[1-(pyridin-2-yl)ethylidene]acetohydrazide
by: Maxym O. Plutenko, et al.
Published: (2014-12-01)