On the Use of Deuterated Organic Solvents without TMS to Report <sup>1</sup>H/<sup>13</sup>C NMR Spectral Data of Organic Compounds: Current State of the Method, Its Pitfalls and Benefits, and Related Issues

On the Use of Deuterated Organic Solvents without TMS to Report <sup>1</sup>H/<sup>13</sup>C NMR Spectral Data of Organic Compounds: Current State of the Method, Its Pitfalls and Benefits, and Related Issues

The quite popular, simple but imperfect method of referencing NMR spectra to residual <sup>1</sup>H and <sup>13</sup>C signals of TMS-free deuterated organic solvents (referred to as Method A) is critically discussed for six commonly used NMR solvents with respect to their δ&...

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Bibliographic Details
Main Author: Ryszard B. Nazarski
Format: Article
Language:English
Published: MDPI AG 2023-05-01
Series:Molecules
Subjects:
NMR spectroscopy
tetramethylsilane
internal reference standards
deuterated solvent signals
residual <sup>1</sup>H signals
the IUPAC unified <i>Ξ</i> scale of chemical shifts
Online Access:https://www.mdpi.com/1420-3049/28/11/4369

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