Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN

The effect of induction heating on the surface properties of hot-pressed ceramics based on plasma chemical nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN (additives: Al<sub>2</sub>O<sub>3</sub>, AlN, and Y<sub>2</sub>O<sub>3</sub&...

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Main Author: Lina L. Sartinska
Format: Article
Language:English
Published: MDPI AG 2023-10-01
Series:Powders
Subjects:
Online Access:https://www.mdpi.com/2674-0516/2/4/43
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author Lina L. Sartinska
author_facet Lina L. Sartinska
author_sort Lina L. Sartinska
collection DOAJ
description The effect of induction heating on the surface properties of hot-pressed ceramics based on plasma chemical nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN (additives: Al<sub>2</sub>O<sub>3</sub>, AlN, and Y<sub>2</sub>O<sub>3</sub>) has been studied. The research demonstrates the formation of a modified layer on the surface of the hot-pressed material. The study examines the porosity, hardness, fracture toughness, brittleness, distribution of elements, and wear of hot-pressed ceramics on the surface before and after additional grinding. Removal of the surface porous layer results in increased density and hardness, leading to a higher number of acoustic emission signals during scratching with a Vickers indenter. A different response to scratching indicates a transgranular or intergranular fracture of the structure. The presence of porosity and carbon contamination on the surface layer of materials negatively impacts the properties of TiN-reinforced ceramics based on Si<sub>3</sub>N<sub>4</sub>-Al<sub>2</sub>O<sub>3</sub>-AlN (SIALON). However, the addition of Y<sub>2</sub>O<sub>3</sub> effectively prevents carbon penetration and reduces the effect of grinding. Additionally, the dark-colored tone observed on the outer volume of the samples suggests a non-thermal microwave effect of the induction furnace.
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spelling doaj.art-6aee663bf48d4e2f8e25c9d1a22f4c3a2023-12-22T14:36:59ZengMDPI AGPowders2674-05162023-10-012469770810.3390/powders2040043Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiNLina L. Sartinska0Frantsevich Institute for Problems of Materials Science of NAS of Ukraine, 3 Krzhyzhanovsky Str., 03142 Kiev, UkraineThe effect of induction heating on the surface properties of hot-pressed ceramics based on plasma chemical nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN (additives: Al<sub>2</sub>O<sub>3</sub>, AlN, and Y<sub>2</sub>O<sub>3</sub>) has been studied. The research demonstrates the formation of a modified layer on the surface of the hot-pressed material. The study examines the porosity, hardness, fracture toughness, brittleness, distribution of elements, and wear of hot-pressed ceramics on the surface before and after additional grinding. Removal of the surface porous layer results in increased density and hardness, leading to a higher number of acoustic emission signals during scratching with a Vickers indenter. A different response to scratching indicates a transgranular or intergranular fracture of the structure. The presence of porosity and carbon contamination on the surface layer of materials negatively impacts the properties of TiN-reinforced ceramics based on Si<sub>3</sub>N<sub>4</sub>-Al<sub>2</sub>O<sub>3</sub>-AlN (SIALON). However, the addition of Y<sub>2</sub>O<sub>3</sub> effectively prevents carbon penetration and reduces the effect of grinding. Additionally, the dark-colored tone observed on the outer volume of the samples suggests a non-thermal microwave effect of the induction furnace.https://www.mdpi.com/2674-0516/2/4/43nitridesplasma chemical nanopowdershot-pressingsurface propertiesmechanical propertieswear
spellingShingle Lina L. Sartinska
Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
Powders
nitrides
plasma chemical nanopowders
hot-pressing
surface properties
mechanical properties
wear
title Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
title_full Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
title_fullStr Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
title_full_unstemmed Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
title_short Effect of Induction Heating on Surface Properties of Hot-Pressed Ceramics Based on Nanopowders Si<sub>3</sub>N<sub>4</sub> and TiN
title_sort effect of induction heating on surface properties of hot pressed ceramics based on nanopowders si sub 3 sub n sub 4 sub and tin
topic nitrides
plasma chemical nanopowders
hot-pressing
surface properties
mechanical properties
wear
url https://www.mdpi.com/2674-0516/2/4/43
work_keys_str_mv AT linalsartinska effectofinductionheatingonsurfacepropertiesofhotpressedceramicsbasedonnanopowderssisub3subnsub4subandtin