The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment

In this work, we study the effect of high-temperature thermomechanical treatment (HTMT) with deformation in the austenite region on the microstructure, tensile properties, impact toughness, and fracture features of advanced low-activation 12% chromium ferritic-martensitic reactor steel EK-181. HTMT...

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Main Authors: Nadezhda Polekhina, Valeria Linnik, Igor Litovchenko, Kseniya Almaeva, Sergey Akkuzin, Evgeny Moskvichev, Vyacheslav Chernov, Mariya Leontyeva-Smirnova, Nikolay Degtyarev, Kirill Moroz
Format: Article
Language:English
Published: MDPI AG 2022-11-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/12/11/1928
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author Nadezhda Polekhina
Valeria Linnik
Igor Litovchenko
Kseniya Almaeva
Sergey Akkuzin
Evgeny Moskvichev
Vyacheslav Chernov
Mariya Leontyeva-Smirnova
Nikolay Degtyarev
Kirill Moroz
author_facet Nadezhda Polekhina
Valeria Linnik
Igor Litovchenko
Kseniya Almaeva
Sergey Akkuzin
Evgeny Moskvichev
Vyacheslav Chernov
Mariya Leontyeva-Smirnova
Nikolay Degtyarev
Kirill Moroz
author_sort Nadezhda Polekhina
collection DOAJ
description In this work, we study the effect of high-temperature thermomechanical treatment (HTMT) with deformation in the austenite region on the microstructure, tensile properties, impact toughness, and fracture features of advanced low-activation 12% chromium ferritic-martensitic reactor steel EK-181. HTMT more significantly modifies the steel structural-phase state than the traditional heat treatment (THT). As a result of HTMT, the hierarchically organized structure of steel is refined. The forming grains and subgrains are elongated in the rolling direction and flattened in the rolling plane (so-called pancake structure) and have a high density of dislocations pinned by stable nanosized particles of the MX type. This microstructure provides a simultaneous increase, relative to THT, in the yield strength and impact toughness of steel EK-181 and does not practically change its ductile-brittle transition temperature. The most important reasons for the increase in impact toughness are a decrease in the effective grain size of steel (martensite blocks and ferrite grains) and the appearance of a crack-arrester type delamination perpendicular to the main crack propagation direction. This causes branching of the main crack and an increase in the absorbed impact energy.
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spelling doaj.art-6b3767f74c784cc99f2da94e25dfa5872023-11-24T09:14:00ZengMDPI AGMetals2075-47012022-11-011211192810.3390/met12111928The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical TreatmentNadezhda Polekhina0Valeria Linnik1Igor Litovchenko2Kseniya Almaeva3Sergey Akkuzin4Evgeny Moskvichev5Vyacheslav Chernov6Mariya Leontyeva-Smirnova7Nikolay Degtyarev8Kirill Moroz9Institute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaInstitute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaInstitute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaInstitute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaInstitute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaInstitute of Strength Physics and Materials Science SB RAS, 2/4 Pr. Akademicheskii, 634055 Tomsk, RussiaJSC “A. A. Bochvar High-Technology Research Institute of Inorganic Materials”, 5 Rogov St., 123060 Moscow, RussiaJSC “A. A. Bochvar High-Technology Research Institute of Inorganic Materials”, 5 Rogov St., 123060 Moscow, RussiaJSC “A. A. Bochvar High-Technology Research Institute of Inorganic Materials”, 5 Rogov St., 123060 Moscow, RussiaJSC “A. A. Bochvar High-Technology Research Institute of Inorganic Materials”, 5 Rogov St., 123060 Moscow, RussiaIn this work, we study the effect of high-temperature thermomechanical treatment (HTMT) with deformation in the austenite region on the microstructure, tensile properties, impact toughness, and fracture features of advanced low-activation 12% chromium ferritic-martensitic reactor steel EK-181. HTMT more significantly modifies the steel structural-phase state than the traditional heat treatment (THT). As a result of HTMT, the hierarchically organized structure of steel is refined. The forming grains and subgrains are elongated in the rolling direction and flattened in the rolling plane (so-called pancake structure) and have a high density of dislocations pinned by stable nanosized particles of the MX type. This microstructure provides a simultaneous increase, relative to THT, in the yield strength and impact toughness of steel EK-181 and does not practically change its ductile-brittle transition temperature. The most important reasons for the increase in impact toughness are a decrease in the effective grain size of steel (martensite blocks and ferrite grains) and the appearance of a crack-arrester type delamination perpendicular to the main crack propagation direction. This causes branching of the main crack and an increase in the absorbed impact energy.https://www.mdpi.com/2075-4701/12/11/1928ferritic-martensitic steel EK-181microstructuremechanical propertiesductile-brittle transition temperatureimpact toughnessfracture
spellingShingle Nadezhda Polekhina
Valeria Linnik
Igor Litovchenko
Kseniya Almaeva
Sergey Akkuzin
Evgeny Moskvichev
Vyacheslav Chernov
Mariya Leontyeva-Smirnova
Nikolay Degtyarev
Kirill Moroz
The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
Metals
ferritic-martensitic steel EK-181
microstructure
mechanical properties
ductile-brittle transition temperature
impact toughness
fracture
title The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
title_full The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
title_fullStr The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
title_full_unstemmed The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
title_short The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
title_sort microstructure tensile and impact properties of low activation ferritic martensitic steel ek 181 after high temperature thermomechanical treatment
topic ferritic-martensitic steel EK-181
microstructure
mechanical properties
ductile-brittle transition temperature
impact toughness
fracture
url https://www.mdpi.com/2075-4701/12/11/1928
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