Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings
In this study, we present a fractional factorial design approach for exploring the effects and interactions of key synthesis and electrochemical transfer parameters on the roughness and wettability of hexagonal boron nitride (h-BN) coatings, due to their essential role in biofilm formation. The stud...
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| Format: | Article |
| Language: | English |
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MDPI AG
2023-11-01
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| Series: | Nanomaterials |
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| Online Access: | https://www.mdpi.com/2079-4991/13/23/2992 |
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| author | Helen Figueroa Juliet Aristizabal Elías Reinoso-Guerra Bárbara Arce María José Vargas-Straube Dana Gentil Cristian Ramírez José Cordero Nelson P. Barrera Carolina Parra |
| author_facet | Helen Figueroa Juliet Aristizabal Elías Reinoso-Guerra Bárbara Arce María José Vargas-Straube Dana Gentil Cristian Ramírez José Cordero Nelson P. Barrera Carolina Parra |
| author_sort | Helen Figueroa |
| collection | DOAJ |
| description | In this study, we present a fractional factorial design approach for exploring the effects and interactions of key synthesis and electrochemical transfer parameters on the roughness and wettability of hexagonal boron nitride (h-BN) coatings, due to their essential role in biofilm formation. The studied parameters for the synthesis process include precursor mass, growth time, and substrate conditioning, whereas for the transfer process, applied voltage and aqueous medium concentration were studied. Through this polynomial model, we confirmed the strong influence of precursor mass and medium concentration parameters on h-BN surface roughness and its resulting antibiofilm properties. |
| first_indexed | 2024-03-09T01:45:59Z |
| format | Article |
| id | doaj.art-6b7da73e72ae48faa45a55083ec4bfd6 |
| institution | Directory Open Access Journal |
| issn | 2079-4991 |
| language | English |
| last_indexed | 2024-03-09T01:45:59Z |
| publishDate | 2023-11-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Nanomaterials |
| spelling | doaj.art-6b7da73e72ae48faa45a55083ec4bfd62023-12-08T15:22:50ZengMDPI AGNanomaterials2079-49912023-11-011323299210.3390/nano13232992Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN CoatingsHelen Figueroa0Juliet Aristizabal1Elías Reinoso-Guerra2Bárbara Arce3María José Vargas-Straube4Dana Gentil5Cristian Ramírez6José Cordero7Nelson P. Barrera8Carolina Parra9Laboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileDepartamento de Ingeniería Química y Ambiental, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileFacultad de Ciencias Biológicas, Pontificia Universidad Católica de Chile, Alameda 340, Santiago 7820436, ChileFacultad de Ciencias Biológicas, Pontificia Universidad Católica de Chile, Alameda 340, Santiago 7820436, ChileLaboratorio de Nanobiomateriales, Departamento de Ingeniería Mecánica, Universidad Técnica Federico Santa María, Avenida España 1680, Valparaíso 2390123, ChileIn this study, we present a fractional factorial design approach for exploring the effects and interactions of key synthesis and electrochemical transfer parameters on the roughness and wettability of hexagonal boron nitride (h-BN) coatings, due to their essential role in biofilm formation. The studied parameters for the synthesis process include precursor mass, growth time, and substrate conditioning, whereas for the transfer process, applied voltage and aqueous medium concentration were studied. Through this polynomial model, we confirmed the strong influence of precursor mass and medium concentration parameters on h-BN surface roughness and its resulting antibiofilm properties.https://www.mdpi.com/2079-4991/13/23/2992h-BNfractional experiment designCVD synthesiselectrochemical transfer |
| spellingShingle | Helen Figueroa Juliet Aristizabal Elías Reinoso-Guerra Bárbara Arce María José Vargas-Straube Dana Gentil Cristian Ramírez José Cordero Nelson P. Barrera Carolina Parra Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings Nanomaterials h-BN fractional experiment design CVD synthesis electrochemical transfer |
| title | Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings |
| title_full | Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings |
| title_fullStr | Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings |
| title_full_unstemmed | Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings |
| title_short | Fractional Factorial Design to Evaluate the Synthesis and Electrochemical Transfer Parameters of h-BN Coatings |
| title_sort | fractional factorial design to evaluate the synthesis and electrochemical transfer parameters of h bn coatings |
| topic | h-BN fractional experiment design CVD synthesis electrochemical transfer |
| url | https://www.mdpi.com/2079-4991/13/23/2992 |
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