Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy

Thermal desorption spectroscopy (TDS) of tungsten implanted with D2+ ions was performed after irradiation with 8 MeV-electrons, 5.0keV-D2+, and 6.0 MeV-Fe3+. The release peak temperatures of the TDS spectra are discussed. Positron annihilation lifetime (PAL) measurements of electron-irradiated tungs...

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Main Authors: K. Sato, R. Tamiya, Q. Xu, H. Tsuchida, T. Yoshiie
Format: Article
Language:English
Published: Elsevier 2016-12-01
Series:Nuclear Materials and Energy
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179115300764
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author K. Sato
R. Tamiya
Q. Xu
H. Tsuchida
T. Yoshiie
author_facet K. Sato
R. Tamiya
Q. Xu
H. Tsuchida
T. Yoshiie
author_sort K. Sato
collection DOAJ
description Thermal desorption spectroscopy (TDS) of tungsten implanted with D2+ ions was performed after irradiation with 8 MeV-electrons, 5.0keV-D2+, and 6.0 MeV-Fe3+. The release peak temperatures of the TDS spectra are discussed. Positron annihilation lifetime (PAL) measurements of electron-irradiated tungsten were also performed, showing that single vacancies migrate a sufficient distance to arrive at a sink or meet interstitial-type defects during annealing at 673K. A decrease in the PAL was detected for single vacancies that contain deuterium atoms. The peak temperature of deuterium release from dislocations was lower than that from single vacancies. In samples irradiated with 6.0 MeV-Fe3+, the effect of Fe contamination on deuterium trapping and the deuterium release from voids were detected. These tendencies correspond to previous works.
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spelling doaj.art-6befb3cacb85438da501d80d77618b8b2022-12-21T17:59:53ZengElsevierNuclear Materials and Energy2352-17912016-12-019C55455910.1016/j.nme.2016.09.014Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopyK. Sato0R. Tamiya1Q. Xu2H. Tsuchida3T. Yoshiie4Graduate School of Science and Engineering, Kagoshima University, Kagoshima-shi, Kagoshima, 890-0065 JapanResearch Reactor Institute, Kyoto University, Kumatori-cho, Sennan-gun, Osaka, 590-0494 JapanResearch Reactor Institute, Kyoto University, Kumatori-cho, Sennan-gun, Osaka, 590-0494 JapanQuantum Science and Engineering Center, Kyoto University, Uji-shi, Kyoto, 611-0011 JapanResearch Reactor Institute, Kyoto University, Kumatori-cho, Sennan-gun, Osaka, 590-0494 JapanThermal desorption spectroscopy (TDS) of tungsten implanted with D2+ ions was performed after irradiation with 8 MeV-electrons, 5.0keV-D2+, and 6.0 MeV-Fe3+. The release peak temperatures of the TDS spectra are discussed. Positron annihilation lifetime (PAL) measurements of electron-irradiated tungsten were also performed, showing that single vacancies migrate a sufficient distance to arrive at a sink or meet interstitial-type defects during annealing at 673K. A decrease in the PAL was detected for single vacancies that contain deuterium atoms. The peak temperature of deuterium release from dislocations was lower than that from single vacancies. In samples irradiated with 6.0 MeV-Fe3+, the effect of Fe contamination on deuterium trapping and the deuterium release from voids were detected. These tendencies correspond to previous works.http://www.sciencedirect.com/science/article/pii/S2352179115300764TungstenHydrogen isotopesThermal desorption spectroscopyPositron annihilationDefectsIon implantation
spellingShingle K. Sato
R. Tamiya
Q. Xu
H. Tsuchida
T. Yoshiie
Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
Nuclear Materials and Energy
Tungsten
Hydrogen isotopes
Thermal desorption spectroscopy
Positron annihilation
Defects
Ion implantation
title Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
title_full Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
title_fullStr Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
title_full_unstemmed Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
title_short Detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
title_sort detection of deuterium trapping sites in tungsten by thermal desorption spectroscopy and positron annihilation spectroscopy
topic Tungsten
Hydrogen isotopes
Thermal desorption spectroscopy
Positron annihilation
Defects
Ion implantation
url http://www.sciencedirect.com/science/article/pii/S2352179115300764
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AT qxu detectionofdeuteriumtrappingsitesintungstenbythermaldesorptionspectroscopyandpositronannihilationspectroscopy
AT htsuchida detectionofdeuteriumtrappingsitesintungstenbythermaldesorptionspectroscopyandpositronannihilationspectroscopy
AT tyoshiie detectionofdeuteriumtrappingsitesintungstenbythermaldesorptionspectroscopyandpositronannihilationspectroscopy