Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases
In this study, zinc oxide nanoparticles (ZnONPs) were synthesised using royal jelly. The prepared NPs were characterised through transmission electron microscopy, field-emission scanning electron microscopy, X-ray diffraction and Fourier transform infrared analysis. The size of the ZnONPs was 31.75 ...
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Elsevier
2023-12-01
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Series: | Results in Chemistry |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S221171562300303X |
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author | Mouhaned Y. Al-darwesh Sattar S. Ibrahim Mohammed Faiad Naief Ahmed Mishaal Mohammed Hammouda Chebbi |
author_facet | Mouhaned Y. Al-darwesh Sattar S. Ibrahim Mohammed Faiad Naief Ahmed Mishaal Mohammed Hammouda Chebbi |
author_sort | Mouhaned Y. Al-darwesh |
collection | DOAJ |
description | In this study, zinc oxide nanoparticles (ZnONPs) were synthesised using royal jelly. The prepared NPs were characterised through transmission electron microscopy, field-emission scanning electron microscopy, X-ray diffraction and Fourier transform infrared analysis. The size of the ZnONPs was 31.75 nm. The produced ZnONPs were evaluated as gas sensors for O2 and NH3 gases at various temperatures and time intervals. The highest sensitivity response to O2 (i.e. 11.1%) was recorded at 100 °C. The highest sensitivity response to NH3 (i.e. 12%) was observed at 25 °C. The sensor exhibited the shortest response and recovery times at different temperatures for O2 and NH3 gases, respectively. At 100 °C, the response time for O2 gas was 18 s, and the recovery time was 23 s. For NH3 gas, the response time was 25 s at 100 °C, and the recovery time was 22 s at 25 °C. These findings demonstrate the unique response and recovery features of the sensor. |
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id | doaj.art-6c2239e6b44c4d18a10e6add79fea03d |
institution | Directory Open Access Journal |
issn | 2211-7156 |
language | English |
last_indexed | 2024-03-09T01:28:16Z |
publishDate | 2023-12-01 |
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series | Results in Chemistry |
spelling | doaj.art-6c2239e6b44c4d18a10e6add79fea03d2023-12-10T06:15:07ZengElsevierResults in Chemistry2211-71562023-12-016101064Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gasesMouhaned Y. Al-darwesh0Sattar S. Ibrahim1Mohammed Faiad Naief2Ahmed Mishaal Mohammed3Hammouda Chebbi4Department of Chemistry, College of Science, University Of Anbar, Ramadi, IraqDepartment of Chemistry, College of Science, University Of Anbar, Ramadi, IraqDepartment of Agricultural Machines and Equipment, College of Agricultural Engineering Science, University of Baghdad, Baghdad, IraqDepartment of Chemistry, College of Science, University Of Anbar, Ramadi, Iraq; Corresponding author.University of Tunis El Manar, Faculty of Sciences of Tunis, Laboratory of Materials, Crystal Chemistry and Applied Thermodynamics, 2092 El Manar II, Tunis, TunisiaIn this study, zinc oxide nanoparticles (ZnONPs) were synthesised using royal jelly. The prepared NPs were characterised through transmission electron microscopy, field-emission scanning electron microscopy, X-ray diffraction and Fourier transform infrared analysis. The size of the ZnONPs was 31.75 nm. The produced ZnONPs were evaluated as gas sensors for O2 and NH3 gases at various temperatures and time intervals. The highest sensitivity response to O2 (i.e. 11.1%) was recorded at 100 °C. The highest sensitivity response to NH3 (i.e. 12%) was observed at 25 °C. The sensor exhibited the shortest response and recovery times at different temperatures for O2 and NH3 gases, respectively. At 100 °C, the response time for O2 gas was 18 s, and the recovery time was 23 s. For NH3 gas, the response time was 25 s at 100 °C, and the recovery time was 22 s at 25 °C. These findings demonstrate the unique response and recovery features of the sensor.http://www.sciencedirect.com/science/article/pii/S221171562300303XZnONPsGas sensorOxygenAmmoniaFE-SEM |
spellingShingle | Mouhaned Y. Al-darwesh Sattar S. Ibrahim Mohammed Faiad Naief Ahmed Mishaal Mohammed Hammouda Chebbi Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases Results in Chemistry ZnONPs Gas sensor Oxygen Ammonia FE-SEM |
title | Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases |
title_full | Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases |
title_fullStr | Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases |
title_full_unstemmed | Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases |
title_short | Synthesis and characterizations of zinc oxide nanoparticles and its ability to detect O2 and NH3 gases |
title_sort | synthesis and characterizations of zinc oxide nanoparticles and its ability to detect o2 and nh3 gases |
topic | ZnONPs Gas sensor Oxygen Ammonia FE-SEM |
url | http://www.sciencedirect.com/science/article/pii/S221171562300303X |
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