4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid
A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed c...
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
MDPI AG
2017-04-01
|
| Series: | Molbank |
| Subjects: | |
| Online Access: | http://www.mdpi.com/1422-8599/2017/2/M938 |
| _version_ | 1818893607822688256 |
|---|---|
| author | Hery Suwito Kautsar Ul Haq Nia Nur Dinia Rahmah Alfinda Novi Kristanti Ni Nyoman Tri Puspaningsih |
| author_facet | Hery Suwito Kautsar Ul Haq Nia Nur Dinia Rahmah Alfinda Novi Kristanti Ni Nyoman Tri Puspaningsih |
| author_sort | Hery Suwito |
| collection | DOAJ |
| description | A dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS, 1H- and 13C-NMR, and 2D-NMR spectral analysis. |
| first_indexed | 2024-12-19T18:15:18Z |
| format | Article |
| id | doaj.art-6c8d53b55e7a4856ad3f51f493376ea9 |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-12-19T18:15:18Z |
| publishDate | 2017-04-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-6c8d53b55e7a4856ad3f51f493376ea92022-12-21T20:11:07ZengMDPI AGMolbank1422-85992017-04-0120172M93810.3390/M938M9384-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic AcidHery Suwito0Kautsar Ul Haq1Nia Nur Dinia Rahmah2Alfinda Novi Kristanti3Ni Nyoman Tri Puspaningsih4Department of Chemistry, Faculty of Science and Technology, Airlangga University, Surabaya 60115, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Airlangga University, Surabaya 60115, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Airlangga University, Surabaya 60115, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Airlangga University, Surabaya 60115, IndonesiaDepartment of Chemistry, Faculty of Science and Technology, Airlangga University, Surabaya 60115, IndonesiaA dimethoxy amide chalcone has been synthesized in a two-step reaction. First, an amine chalcone was synthesized by the reaction of 4′-aminoacetophenone and 2,5-dimethoxybenzaldehyde using 40% NaOH solution as a catalyst in ethanol, and then followed by amidation through the reaction of the formed chalcone and succinic anhydride. The structure of the target compound was established by FTIR, HR-MS, 1H- and 13C-NMR, and 2D-NMR spectral analysis.http://www.mdpi.com/1422-8599/2017/2/M938amino chalconesamide chalconessuccinic anhydride |
| spellingShingle | Hery Suwito Kautsar Ul Haq Nia Nur Dinia Rahmah Alfinda Novi Kristanti Ni Nyoman Tri Puspaningsih 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid Molbank amino chalcones amide chalcones succinic anhydride |
| title | 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid |
| title_full | 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid |
| title_fullStr | 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid |
| title_full_unstemmed | 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid |
| title_short | 4-({4-[(2E)-3-(2,5-Dimethoxyphenyl)prop-2-enoyl]phenyl}amino)-4-oxobutanoic Acid |
| title_sort | 4 4 2e 3 2 5 dimethoxyphenyl prop 2 enoyl phenyl amino 4 oxobutanoic acid |
| topic | amino chalcones amide chalcones succinic anhydride |
| url | http://www.mdpi.com/1422-8599/2017/2/M938 |
| work_keys_str_mv | AT herysuwito 442e325dimethoxyphenylprop2enoylphenylamino4oxobutanoicacid AT kautsarulhaq 442e325dimethoxyphenylprop2enoylphenylamino4oxobutanoicacid AT nianurdiniarahmah 442e325dimethoxyphenylprop2enoylphenylamino4oxobutanoicacid AT alfindanovikristanti 442e325dimethoxyphenylprop2enoylphenylamino4oxobutanoicacid AT ninyomantripuspaningsih 442e325dimethoxyphenylprop2enoylphenylamino4oxobutanoicacid |