5-Amino-3-methyl-1,2,4-thiadiazole
An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction w...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
MDPI AG
2018-01-01
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| Series: | Molbank |
| Subjects: | |
| Online Access: | http://www.mdpi.com/1422-8599/2018/1/M977 |
| _version_ | 1818303762928762880 |
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| author | R. Alan Aitken Alexandra M. Z. Slawin |
| author_facet | R. Alan Aitken Alexandra M. Z. Slawin |
| author_sort | R. Alan Aitken |
| collection | DOAJ |
| description | An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules. |
| first_indexed | 2024-12-13T05:59:58Z |
| format | Article |
| id | doaj.art-6de85acabab0457dbb99a9e20b9f40bb |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-12-13T05:59:58Z |
| publishDate | 2018-01-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-6de85acabab0457dbb99a9e20b9f40bb2022-12-21T23:57:21ZengMDPI AGMolbank1422-85992018-01-0120181M97710.3390/M977M9775-Amino-3-methyl-1,2,4-thiadiazoleR. Alan Aitken0Alexandra M. Z. Slawin1EaStCHEM School of Chemistry, University of St Andrews, North Haugh, St Andrews, Fife KY16 9ST, UKEaStCHEM School of Chemistry, University of St Andrews, North Haugh, St Andrews, Fife KY16 9ST, UKAn improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules.http://www.mdpi.com/1422-8599/2018/1/M9771,2,4-thiadiazoleNMR spectraIR spectrumX-ray structure |
| spellingShingle | R. Alan Aitken Alexandra M. Z. Slawin 5-Amino-3-methyl-1,2,4-thiadiazole Molbank 1,2,4-thiadiazole NMR spectra IR spectrum X-ray structure |
| title | 5-Amino-3-methyl-1,2,4-thiadiazole |
| title_full | 5-Amino-3-methyl-1,2,4-thiadiazole |
| title_fullStr | 5-Amino-3-methyl-1,2,4-thiadiazole |
| title_full_unstemmed | 5-Amino-3-methyl-1,2,4-thiadiazole |
| title_short | 5-Amino-3-methyl-1,2,4-thiadiazole |
| title_sort | 5 amino 3 methyl 1 2 4 thiadiazole |
| topic | 1,2,4-thiadiazole NMR spectra IR spectrum X-ray structure |
| url | http://www.mdpi.com/1422-8599/2018/1/M977 |
| work_keys_str_mv | AT ralanaitken 5amino3methyl124thiadiazole AT alexandramzslawin 5amino3methyl124thiadiazole |