Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot
This research paper dealt with the synthesis and characterization of pure and metal-doped hydroxyapatite covering an in-depth crystallographic analysis. The Scherrer equation, Linear Straight-Line Model, Munshi Scherrer Model, Uniform Deformation Model, Uniform Stress Deformation Model, Uniform Defo...
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| Format: | Article |
| Language: | English |
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Elsevier
2024-03-01
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| Series: | Results in Materials |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S2590048X23001346 |
| _version_ | 1797261840974086144 |
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| author | Sanjana Afrin Disha Md. Sahadat Hossain Md. Lawshan Habib Samina Ahmed |
| author_facet | Sanjana Afrin Disha Md. Sahadat Hossain Md. Lawshan Habib Samina Ahmed |
| author_sort | Sanjana Afrin Disha |
| collection | DOAJ |
| description | This research paper dealt with the synthesis and characterization of pure and metal-doped hydroxyapatite covering an in-depth crystallographic analysis. The Scherrer equation, Linear Straight-Line Model, Munshi Scherrer Model, Uniform Deformation Model, Uniform Stress Deformation Model, Uniform Deformation Energy Density Model, Size Strain Model, Halder Wagner Model, and Sahadat Scherrer Model were engaged to estimate crystallite size as well as strain, stress, and energy density from few models. All the models were evaluated with their merits and demerits along with usefulness. All the mentioned models showed acceptable results as the crystallite size ranges were from 22 to 77 nm except Linear Straight-Line Model (revealed invalid results for all the synthesized samples). The modified Williamson-Hall model (Uniform Deformation Model, Uniform Stress Deformation Model, Uniform Deformation Energy Density Model) exerted strain, stress and energy density positive and negative. But Size Strain Model, and Halder Wagner Model resulted in only positive values. |
| first_indexed | 2024-03-09T01:26:23Z |
| format | Article |
| id | doaj.art-6e6a32c1156e49828f5fb245da6e1a90 |
| institution | Directory Open Access Journal |
| issn | 2590-048X |
| language | English |
| last_indexed | 2024-04-24T23:47:37Z |
| publishDate | 2024-03-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Results in Materials |
| spelling | doaj.art-6e6a32c1156e49828f5fb245da6e1a902024-03-15T04:44:21ZengElsevierResults in Materials2590-048X2024-03-0121100496Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plotSanjana Afrin Disha0Md. Sahadat Hossain1Md. Lawshan Habib2Samina Ahmed3Institute of Glass and Ceramic Research and Testing, Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhanmondi, Dhaka-1205, Bangladesh; Department of Applied Chemistry and Chemical Engineering, Faculty of Engineering, Bangabandhu Sheikh Mujibur Rahman Science and Technology University, Gopalganj-8100, BangladeshInstitute of Glass and Ceramic Research and Testing, Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhanmondi, Dhaka-1205, BangladeshDepartment of Applied Chemistry and Chemical Engineering, Faculty of Engineering, Bangabandhu Sheikh Mujibur Rahman Science and Technology University, Gopalganj-8100, Bangladesh; Corresponding author.Department of Applied Chemistry and Chemical Engineering, Faculty of Engineering, Bangabandhu Sheikh Mujibur Rahman Science and Technology University, Gopalganj-8100, Bangladesh.Institute of Glass and Ceramic Research and Testing, Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhanmondi, Dhaka-1205, Bangladesh; BCSIR Laboratories Dhaka, Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh; Corresponding author. Institute of Glass and Ceramic Research and Testing, Bangladesh Council of Scientific and Industrial Research (BCSIR), Dhanmondi, Dhaka-1205, Bangladesh.This research paper dealt with the synthesis and characterization of pure and metal-doped hydroxyapatite covering an in-depth crystallographic analysis. The Scherrer equation, Linear Straight-Line Model, Munshi Scherrer Model, Uniform Deformation Model, Uniform Stress Deformation Model, Uniform Deformation Energy Density Model, Size Strain Model, Halder Wagner Model, and Sahadat Scherrer Model were engaged to estimate crystallite size as well as strain, stress, and energy density from few models. All the models were evaluated with their merits and demerits along with usefulness. All the mentioned models showed acceptable results as the crystallite size ranges were from 22 to 77 nm except Linear Straight-Line Model (revealed invalid results for all the synthesized samples). The modified Williamson-Hall model (Uniform Deformation Model, Uniform Stress Deformation Model, Uniform Deformation Energy Density Model) exerted strain, stress and energy density positive and negative. But Size Strain Model, and Halder Wagner Model resulted in only positive values.http://www.sciencedirect.com/science/article/pii/S2590048X23001346X-ray diffractionCrystallite sizeStrainStressEnergy density |
| spellingShingle | Sanjana Afrin Disha Md. Sahadat Hossain Md. Lawshan Habib Samina Ahmed Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot Results in Materials X-ray diffraction Crystallite size Strain Stress Energy density |
| title | Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot |
| title_full | Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot |
| title_fullStr | Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot |
| title_full_unstemmed | Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot |
| title_short | Calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging Scherrer method, Halder-Wagner method, Williamson-Hall model, and size-strain plot |
| title_sort | calculation of crystallite sizes of pure and metals doped hydroxyapatite engaging scherrer method halder wagner method williamson hall model and size strain plot |
| topic | X-ray diffraction Crystallite size Strain Stress Energy density |
| url | http://www.sciencedirect.com/science/article/pii/S2590048X23001346 |
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