Microstructure Characterization and Hardening Evaluation of Ferrite/Martensitic Steels Induced by He<sup>2+</sup> Irradiation

Two ferrite/martensitic (F/M) steels with different Si concentrations (0 and 0.4 wt.%) were irradiated by 250 keV He<sup>2+</sup> ions with different fluences of 2 × 10<sup>16</sup> ions/cm<sup>2</sup> and 1 × 10<sup>17</sup> ions/cm<sup>2</su...

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Bibliographic Details
Main Authors: Guangjie Zhang, Junfeng Yang, Zhuoming Xie, Linchao Zhang, Rui Liu, Meng Sun, Gang Li, Hui Wang, Yi Hu, Xuebang Wu, Qianfeng Fang, Changsong Liu, Xianping Wang
Format: Article
Language:English
Published: MDPI AG 2023-08-01
Series:Crystals
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Online Access:https://www.mdpi.com/2073-4352/13/9/1308
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Summary:Two ferrite/martensitic (F/M) steels with different Si concentrations (0 and 0.4 wt.%) were irradiated by 250 keV He<sup>2+</sup> ions with different fluences of 2 × 10<sup>16</sup> ions/cm<sup>2</sup> and 1 × 10<sup>17</sup> ions/cm<sup>2</sup>. Transmission electron microscopy and a nanoindenter were employed to investigate their microstructure evolution and irradiation hardening effects induced by high-energy He<sup>2+</sup> ions. A large number of He bubbles formed in the Si-free and Si-containing F/M steels, which preferentially nucleated and grew at the lath and phase boundaries. Owing to the inhibiting effect of Si addition on He bubble growth, the He bubbles in the Si-containing sample exhibited smaller size and higher density at the same He<sup>2+</sup> fluence. Nanoindenter measurement revealed that typical irradiation hardening was observed in the F/M steel, and 1/2<111> and <100> type dislocation loops formed by He<sup>2+</sup> irradiation was recognized as the dominant mechanism. The addition of Si induced an increase in the number density of dislocation loops, leading to the exacerbation of the irradiation hardening, and the results are basically in agreement with the theoretical analysis based on the dispersion barrier hardening (DBH) and Friedel–Kroupa–Hirsch (FKH) models.
ISSN:2073-4352